A preparation method of long-acting magnetic therapy thermal underwear
A thermal underwear, long-lasting technology, applied in magnetic therapy, underwear, electrotherapy and other directions, can solve the problems of discomfort, air permeability, water absorption, softness that cannot catch up with cotton fibers, no research reports, etc. Good effect, strong water absorption effect
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Embodiment 1
[0032] In step (1), the mass fraction of the acetone solution is 10%, the soaking time is 1h, and the liquid squeeze rate is 80%; the pH value of the strong alkali solution is 14, and it is reacted at 80°C for 2h; wherein, the The strong alkali solution mainly includes one of sodium hydroxide and potassium hydroxide, and the acid is one of dilute hydrochloric acid, dilute nitric acid and dilute sulfuric acid;
[0033] In step (2), the concentration of the graphene oxide is 10g / L, Fe 2+ The concentration is 1g / L, Fe 3+ The concentration is 2g / L;
[0034] In step (4), the extruded water is 80% of the total water absorption of cotton fibers;
[0035] In step (5), the pH value of the alkaline solution is 9, and the volume ratio of the cotton fiber processed in the step (4) to the alkaline solution is 1:0.8; the alkaline solution is mainly composed of ammonia, hydrogen One or more of sodium, sodium hydroxide, sodium carbonate, sodium bicarbonate, preferably, the alkaline solutio...
Embodiment 2
[0041] In the step (1), the mass fraction of the acetone solution is 15%, the soaking time is 50min, and the squeeze rate is 78%; the pH value of the strong alkali solution is 13.5, and the reaction is carried out at 82°C for 1h45min; wherein, the The strong alkali solution mainly includes one of sodium hydroxide and potassium hydroxide, and the acid is one of dilute hydrochloric acid, dilute nitric acid and dilute sulfuric acid;
[0042] In step (2), the concentration of the graphene oxide is 20g / L, Fe 2+ The concentration is 3g / L, Fe 3+ The concentration is 6g / L;
[0043] In step (4), the extruded water is 75% of the total water absorption of cotton fibers;
[0044] In step (5), the pH value of the alkaline solution is 9.5, and the volume ratio of the cotton fiber processed in the step (4) to the alkaline solution is 1:1; the alkaline solution is mainly composed of ammonia, hydrogen One or more of sodium, sodium hydroxide, sodium carbonate, sodium bicarbonate;
[0045] In ...
Embodiment 3
[0050] In step (1), the mass fraction of the acetone solution is 20%, the soaking time is 40min, and the liquid squeeze rate is 75%; the pH value of the strong alkali solution is 13, and it is reacted at 85°C for 1h30min; wherein, the The strong alkali solution mainly includes one of sodium hydroxide and potassium hydroxide, and the acid is one of dilute hydrochloric acid, dilute nitric acid and dilute sulfuric acid;
[0051] In step (2), the concentration of described graphene oxide is 30g / L, Fe 2+ The concentration is 5g / L, Fe 3+ The concentration is 10g / L;
[0052] In step (4), the extruded water is 70% of the total water absorption of cotton fibers;
[0053] In step (5), the pH value of the alkaline solution is 10, and the volume ratio of the cotton fiber processed in the step (4) to the alkaline solution is 1:1.2; the alkaline solution is mainly composed of ammonia, hydrogen One or more of sodium, sodium hydroxide, sodium carbonate, sodium bicarbonate;
[0054] In ste...
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