A kind of lithium ion battery negative electrode material binder and negative electrode material and lithium battery
A lithium-ion battery and negative electrode material technology, applied in battery electrodes, secondary batteries, circuits, etc., can solve the problem of small specific capacity of the battery and achieve the effect of increasing the specific capacity
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specific Embodiment 1
[0026] Step 1: dissolving N-n-propylmaleamide in an organic solvent to form a maleamide solution, and then preheating to between 40-50 degrees Celsius;
[0027] Step 2: Add 1,3-propanedithiol to the solution after step 1, adjust the pH value of the solution between 5-7 with acetic acid, and add an initiator, wherein the initiator uses an existing initiator, such as Azobisisobutyronitrile, azobisisoheptanonitrile, etc.
[0028] Step 3: By raising the temperature to 80 degrees Celsius, stirring the reaction, and maintaining reflux, the reaction is completed when the refractive index is 1.498-1.479;
[0029] Step 4: Cool down to below 60 degrees Celsius, depressurize, remove the solvent until the viscosity is 1.5PA·S, stop the solvent removal, and stir evenly.
specific Embodiment 2
[0031] Step 1: Dissolving N-methylmaleamide in an organic solvent to form a maleamide solution, and then preheating to 40-50 degrees Celsius;
[0032] Step 2: Add n-dodecyl mercaptan to the solution after step 1, adjust the pH value of the solution between 5-7 by acetic acid, and add an initiator, wherein the initiator uses an existing initiator, such as azo Diisobutyronitrile, azobisisoheptanonitrile, etc.
[0033] Step 3: By raising the temperature to 80 degrees Celsius, stirring the reaction, and maintaining reflux, the reaction is completed when the refractive index is 1.498-1.479;
[0034] Step 4: Cool down to below 60 degrees Celsius, depressurize, remove the solvent until the viscosity is 1.5PA·S, stop the solvent removal, and stir evenly.
specific Embodiment 3
[0036] Step 1: Dissolving N-phenylmaleamide in an organic solvent to form a maleamide solution, and then preheating to 40-50 degrees Celsius;
[0037] Step 2: Add 1,9-nonanedithiol to the solution after step 1, adjust the pH value of the solution between 5-7 with acetic acid, and add an initiator, wherein the initiator uses an existing initiator, such as even Azobisisobutyronitrile, azobisisoheptanonitrile, etc.
[0038] Step 3: By raising the temperature to 90 degrees Celsius, stirring the reaction, and maintaining reflux, the reaction is completed when the refractive index is 1.498-1.479;
[0039] Step 4: Cool down to below 60 degrees Celsius, depressurize, remove the solvent until the viscosity is 1.5PA·S, stop the solvent removal, and stir evenly.
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