A method for producing wax medium for thermostat with f-t synthetic product
A synthetic product, F-T technology, applied in the direction of petroleum wax recovery, etc., can solve the problems of low product yield, low production cycle, inability to produce wax media for thermostats, and environmental pollution.
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Embodiment 1
[0059] This embodiment includes: (1) hydrogenation, (2) distillation and (3) sweating.
[0060] (1) Hydrogenation
[0061] Using the wax oil product (n-paraffin content of 95.5wt%) of the low-temperature F-T synthesis experimental device of China Petrochemical Corporation as raw material, the FHJ-2 catalyst (a Ni / Al 2 o 3 Commercial catalyst, developed and produced by Fushun Petrochemical Research Institute, the content of active metal nickel in terms of oxides is 40%, and the catalyst is subjected to conventional reduction treatment before use), under the action of reaction pressure 5.0MPa, reaction temperature 200°C, volume space velocity 1.0 h -1 Hydrogenation is carried out under the condition of 500:1 volume ratio of hydrogen to liquid to convert olefins and oxygenates in it. The weight content of normal paraffins in the hydrogenation product is 97.36%.
[0062] (2) Distillation
[0063] The product obtained by the above hydrogenation conversion is prepared in a vacu...
Embodiment 2
[0083] This embodiment includes: (1) hydroconversion, (2) distillation, and (3) sweating.
[0084] (1) Hydrogenation
[0085] With embodiment 1.
[0086] (2) Distillation
[0087] With embodiment 1.
[0088] (3) sweating
[0089] This part includes: (1) preparation work, (2) cooling - high temperature constant temperature - cooling - low temperature constant temperature crystallization (3) heating - constant temperature - heating - constant temperature sweating, (4) product refining and other processes.
[0090] (1) Preparation
[0091] Connect the jacket of the sweating dish and the movable coil to the circulation system, and fix the coil on the sweating dish; use water as the medium; start the heating function of the circulation system to raise the temperature of the circulating water to 74°C.
[0092]Put water under the sweating dish plate. Install the sealing system on the upper part of the sweating dish and connect it with the pressurized buffer tank and the compres...
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