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A method for producing wax medium for thermostat with f-t synthetic product

A synthetic product, F-T technology, applied in the direction of petroleum wax recovery, etc., can solve the problems of low product yield, low production cycle, inability to produce wax media for thermostats, and environmental pollution.

Active Publication Date: 2019-01-25
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0018] Compared with the solvent separation process, the sweating separation process is an intermittent operation, and the product yield is lower and the production cycle is longer, but the sweating process has the advantages of less investment, simple production process, low operating cost, safe production process, energy saving and no environmental impact. Pollution and other advantages, some manufacturers are still using this method to produce soap wax products
[0019] Over the years, the sweating method has been developed in terms of production equipment and technology, such as CN89214332 (vertical square multi-section sweating tank), CN94223980.6 (dish-type sweating device), CN98233254.8 (paraffin sweating tank), CN200920033500. X (new paraffin sweating tank), CN201210508905.0 (a high-efficiency paraffin sweating device), CN201320127680.4 (tubular paraffin deoiling device), etc., have made improvements in sweating production equipment; CN91206202 (a high-efficiency paraffin sweating tank ) has made improvements in the sweating process, but these improvements still cannot produce wax media for thermostats with a melting point of about 70 °C
[0020] The means of producing wax medium in the prior art, there are solvent methods, such as: DD 241,829, SU 1,084,289, RU 2,009,171, US 5,223,122 and other patents, the production methods introduced by these patents pollute the environment
[0021] The means of producing wax medium in the prior art also have (multi-stage) sweating or (distillation method) combined sweating, such as: CN02109670.8 (waxy temperature medium for shower automatic thermostat valve), CN02109668.6 (heating control Wax medium for temperature control valve and its preparation method), CN200310104909.3 (a wax temperature-sensitive medium for temperature control valve and its preparation method), etc., the melting points of the target products of these patents are all below 50°C; CN201110353409.8 ( A preparation method of waxy temperature medium for temperature control valve), CN201110353410.0 (a preparation method of thermal induction wax medium for automatic thickening valve of motorcycle), CN02109670.8 (waxy temperature medium for shower automatic temperature control valve) medium), etc. The target product of these patents has a melting point below 50°C and a wide temperature control range, so it is not suitable for use as a wax medium for thermostats

Method used

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  • A method for producing wax medium for thermostat with f-t synthetic product
  • A method for producing wax medium for thermostat with f-t synthetic product

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0059] This embodiment includes: (1) hydrogenation, (2) distillation and (3) sweating.

[0060] (1) Hydrogenation

[0061] Using the wax oil product (n-paraffin content of 95.5wt%) of the low-temperature F-T synthesis experimental device of China Petrochemical Corporation as raw material, the FHJ-2 catalyst (a Ni / Al 2 o 3 Commercial catalyst, developed and produced by Fushun Petrochemical Research Institute, the content of active metal nickel in terms of oxides is 40%, and the catalyst is subjected to conventional reduction treatment before use), under the action of reaction pressure 5.0MPa, reaction temperature 200°C, volume space velocity 1.0 h -1 Hydrogenation is carried out under the condition of 500:1 volume ratio of hydrogen to liquid to convert olefins and oxygenates in it. The weight content of normal paraffins in the hydrogenation product is 97.36%.

[0062] (2) Distillation

[0063] The product obtained by the above hydrogenation conversion is prepared in a vacu...

Embodiment 2

[0083] This embodiment includes: (1) hydroconversion, (2) distillation, and (3) sweating.

[0084] (1) Hydrogenation

[0085] With embodiment 1.

[0086] (2) Distillation

[0087] With embodiment 1.

[0088] (3) sweating

[0089] This part includes: (1) preparation work, (2) cooling - high temperature constant temperature - cooling - low temperature constant temperature crystallization (3) heating - constant temperature - heating - constant temperature sweating, (4) product refining and other processes.

[0090] (1) Preparation

[0091] Connect the jacket of the sweating dish and the movable coil to the circulation system, and fix the coil on the sweating dish; use water as the medium; start the heating function of the circulation system to raise the temperature of the circulating water to 74°C.

[0092]Put water under the sweating dish plate. Install the sealing system on the upper part of the sweating dish and connect it with the pressurized buffer tank and the compres...

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Abstract

The invention discloses a method for producing a wax medium for a thermostat from products synthesized by F-T. The method comprises the following steps: products synthesized by F-T whose weight percentage of n-alkanes is 85% or above are used as raw materials, and hydro-conversion is carried out under the effects of a catalyst; distillation is carried out for hydrogenated products in order to prepare components of proper distillation ranges; sweating is carried out in order to produce the target product. The method is based on common sweating process, in a sweating process, air-flow passes through a wax layer for carrying liquid state components, separating effect of solid components and liquid components is enhanced and separating speed is accelerated; at the same time, gas generated by decomposition of inorganic salt forms micro spaces in the wax layer for facilitating rapid discharge of liquid components. The method has the advantages of low production equipment investment, simple production process, low operation cost, safety, energy saving without solvent pollution, and the like; the product has a narrow temperature control range, and can be applied to wax temperature control valves, especially the wax type medium for the thermostat.

Description

technical field [0001] The invention belongs to the technical field of special wax production, in particular to a method for producing a wax medium for a thermostat with an F-T synthetic product. Background technique [0002] The wax temperature control valve uses wax as the medium for sensing temperature changes. When the ambient temperature changes, the volume of the wax will change, and then control the valve opening, thereby adjusting the flow rate and achieving the purpose of adjusting and controlling the temperature. The wax substance used in wax temperature control valve is called wax medium. Wax temperature control valve has many advantages and is widely used. [0003] The thermostat, also known as the thermostat, is used to automatically adjust the amount of water entering the radiator according to the temperature of the cooling water, change the water circulation range, and adjust the heat dissipation capacity of the cooling system to ensure that the engine works ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10G73/36
CPCC10G73/36
Inventor 孙剑锋姚春雷陈琳吴颖刘纾言赵威
Owner CHINA PETROLEUM & CHEM CORP