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A kind of preparation method of high-performance anti-reflection film

An anti-reflection film, high-performance technology, applied in the direction of climate sustainability, final product manufacturing, sustainable manufacturing/processing, etc. Problems such as poor friction ability, achieve the effects of orderliness and low packing density, low production cost, and anti-reflection effect

Active Publication Date: 2018-07-13
常州海辰装饰材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the existing products, the surface hardness of the anti-reflection film is not high enough, the scratch resistance is poor, and it is easy to scratch during use, thus affecting the performance and life of the product

Method used

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  • A kind of preparation method of high-performance anti-reflection film

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] A method for preparing a high-performance antireflection film, the preparation steps of which are as follows:

[0031] Step 1, adding ethyl silicate to absolute ethanol, stirring evenly, adding a stabilizer to form a stable sol;

[0032] Step 2, slowly adding ethylene-vinyl acetate copolymer and curing agent into the sol solution, and ultrasonically dispersing for 10 minutes to form a viscous dispersion;

[0033] Step 3, soak the silicon wafer in the viscous dispersion liquid, then seal the micro-boiling reaction for 1 hour, and take out the silicon wafer after natural cooling;

[0034] Step 4, putting the coated silicon wafer into a muffle furnace for drying, and then cooling naturally to form a uniform film layer;

[0035] Step 5, adding polyvinylpyrrolidone to distilled water, stirring until completely dissolved, then adding nano-silicon carbide, penetrating agent and foaming agent to form a suspension;

[0036] In step 6, put the silicon wafer in step 4 into the s...

Embodiment 2

[0049] A method for preparing a high-performance antireflection film, the preparation steps of which are as follows:

[0050] Step 1, adding ethyl silicate to absolute ethanol, stirring evenly, adding a stabilizer to form a stable sol;

[0051] Step 2, slowly adding ethylene-vinyl acetate copolymer and curing agent into the sol solution, and ultrasonically dispersing for 15 minutes to form a viscous dispersion;

[0052] Step 3, soak the silicon chip in the viscous dispersion liquid, then seal the micro-boiling reaction for 2 hours, and take out the silicon chip after natural cooling;

[0053] Step 4, putting the coated silicon wafer into a muffle furnace for drying, and then cooling naturally to form a uniform film layer;

[0054] Step 5, adding polyvinylpyrrolidone to distilled water, stirring until completely dissolved, then adding nano-silicon carbide, penetrating agent and foaming agent to form a suspension;

[0055] In step 6, put the silicon wafer in step 4 into the su...

Embodiment 3

[0068] A method for preparing a high-performance antireflection film, the preparation steps of which are as follows:

[0069] Step 1, adding ethyl silicate to absolute ethanol, stirring evenly, adding a stabilizer to form a stable sol;

[0070] Step 2, slowly adding ethylene-vinyl acetate copolymer and curing agent into the sol solution, and ultrasonically dispersing for 15 minutes to form a viscous dispersion;

[0071] Step 3, soak the silicon chip in the viscous dispersion liquid, then seal the micro-boiling reaction for 2 hours, and take out the silicon chip after natural cooling;

[0072] Step 4, putting the coated silicon wafer into a muffle furnace for drying, and then cooling naturally to form a uniform film layer;

[0073] Step 5, adding polyvinylpyrrolidone to distilled water, stirring until completely dissolved, then adding nano-silicon carbide, penetrating agent and foaming agent to form a suspension;

[0074] Step 6, put the silicon wafer in step 4 into the suspe...

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Abstract

The invention relates to a high performance antireflection film preparation method. Ethyl silicate and silicon carbide are used as raw materials for preparing an antireflection film. The method comprises the following steps: a stabilizing agent and an ethane-vinyl acetate copolymer are added in the ethyl silicate, a stable sol solution is formed, the silicon carbide and polyvinylpyrrolidone are used for forming a suspending liquid, films are orderly coated on a silicon chip, slight boiling and pull-through modes are used for film coating, finally sintering operation is conducted, and the antireflection film is obtained. The method disclosed in the invention is small in intermolecular Van der Waals active force and low in orderliness and bulk density, surface hardness of the antireflection film can be improved, transmissivity of the antireflection film can be improved, and obvious reflection reducing effects are exerted.

Description

technical field [0001] The invention belongs to the technical field of thin film materials and relates to a preparation method of a high-performance anti-reflection film. Background technique [0002] In the field of solar cells, the conversion efficiency of solar cells can be effectively improved by increasing the light transmittance of the glass substrate, which has always been a hot and difficult point in industry research. Coating an anti-reflection coating on the glass substrate of the solar cell can minimize the reflectivity and increase the transmittance. Developed nano anti-reflection coating glass for solar photovoltaics with high transmittance within the response spectrum range of solar cells, which can improve the conversion efficiency of solar cells to the same extent, reduce power generation costs, improve the market competitiveness of solar cell power generation, and shorten the time for grid-connected power generation. The cost recovery period has very good e...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01L31/18H01L31/0216
CPCH01L31/02168H01L31/18Y02P70/50
Inventor 焦秀双
Owner 常州海辰装饰材料有限公司