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Pd quantum dot-containing MoO3 nanofiber paper H2 sensor and preparation method thereof

A nanofiber, quantum dot technology, applied in instruments, measuring devices, scientific instruments, etc., can solve the problems of hydrogen leakage and diffusion, poor detection accuracy, hydrogen leakage, etc., and achieve short response time, short recovery time, and small initial resistance. Effect

Inactive Publication Date: 2017-09-08
HUBEI UNIV
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  • Summary
  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

However, hydrogen is a colorless, odorless, small molecular weight, flammable and explosive gas. During production, transportation and use, hydrogen leakage is very easy to occur and diffuses quickly, and it is difficult to be detected by human senses. High sensitivity must be used Detection device, fast, safe and reliable detection of hydrogen leaks
Existing hydrogen sensors based on bubble testing, catalytic combustion, mass spectrometer detection, electrochemical methods, ultrasonic methods, etc., all have shortcomings such as low safety and poor detection accuracy

Method used

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  • Pd quantum dot-containing MoO3 nanofiber paper H2 sensor and preparation method thereof
  • Pd quantum dot-containing MoO3 nanofiber paper H2 sensor and preparation method thereof
  • Pd quantum dot-containing MoO3 nanofiber paper H2 sensor and preparation method thereof

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Embodiment Construction

[0041] The embodiments of the present invention will be further described below in conjunction with the accompanying drawings. In order to make the purpose, technical solutions and advantages of the present invention clearer, the technical solutions in the present invention will be clearly and completely described below. Obviously, the described embodiments are the embodiment of the present invention. Some, but not all, embodiments. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the protection scope of the present invention.

[0042] MoO containing Pd quantum dots of the present invention 3 Nanofiber Paper H 2 The hydrogen sensitive element of the sensing head of the sensor is made of MoO modified with Pd quantum dots 3 Nanofiber paper production;

[0043] The MoO modified with Pd quantum dots 3 The fiber paper is prepared by hydrothermal synthesis and self-...

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Abstract

The invention discloses a Pd quantum dot-containing MoO3 nanofiber paper H2 sensor and a preparation method thereof. According to the Pd quantum dot-containing MoO3 nanofiber paper, in the process of preparing the pure MoO3 nanofiber paper, a right amount of Pd quantum dots (also called Pd nanoparticles) are doped for carrying out modification to obtain the Pd quantum dot modified MoO3 nanofiber paper. According to the hydrogen sensor produced by adopting the Pd quantum dot modified MoO3 nanofiber paper, in an environment with relatively low hydrogen concentration, the initial resistance of the sensor is smaller, both the response time and the recovery time of the sensor become shorter, the sensitivity is higher, the sensor can work at ordinary temperature, has stable properties and is reusable, and the integrated hydrogen-sensitive elements also can be integrated conveniently in various flexible circuits. The preparation method disclosed by the invention has a simple process, low energy consumption and no pollution of the manufacturing process.

Description

technical field [0001] The present invention relates to Pd-containing quantum dot MoO 3 Nanofiber Paper H 2 The sensor and its preparation method belong to the technical field of inorganic nano functional material and hydrogen sensor. Background technique [0002] As an efficient and clean fuel, reducing gas, and carrier gas, hydrogen has been widely used in many fields such as medical treatment, medicine, petrochemical, and metallurgy. However, hydrogen is a colorless, odorless, small molecular weight, flammable and explosive gas. During production, transportation and use, hydrogen leakage is very easy to occur and diffuses quickly, and it is difficult to be detected by human senses. High sensitivity must be used The detection device realizes hydrogen leakage detection quickly, safely and reliably. Existing hydrogen sensors based on bubble test, catalytic combustion, mass spectrometer detection, electrochemical method, ultrasonic method, etc. all have disadvantages such ...

Claims

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Application Information

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IPC IPC(8): G01N27/00
CPCG01N27/00
Inventor 胡永明罗显涛王钊顾豪爽
Owner HUBEI UNIV
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