A kind of polyvinyl alcohol-based film and its production method and polarizing film prepared therefrom
A polyvinyl alcohol-based film and film technology, applied in the field of polarizing film, can solve the problems of low self-sufficiency of PVA film, and achieve the effects of ensuring optical consistency, reducing dimensional changes, and good optical consistency
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Embodiment 1
[0042] This implementation discloses a polyvinyl alcohol-based film. The raw materials for preparation include the following components in parts by mass: 80-95 parts of PVA, 5-20 parts of EVOH, 5-25 parts of plasticizer, and 0.001-0.1 part of surfactant , 0.001-0.1 part of antioxidant; The degree of polymerization of PVA is 1500~3000, and the degree of alcoholysis is 97-100mol%l; The plasticizer is a polyhydroxy compound, preferably glycerin, purity ≥ 99.5%, and the antioxidant is selected from 1010 / 168 is a composition of 1:1; the polyvinyl alcohol film is annealed at 80°C, 50-95%RH for 2 hours, the crystallinity change of any area of the polyvinyl alcohol film is less than or equal to 5%, and its size is stable. The dimensional change in any direction of the film during swelling can be reduced, the processing performance of the polyvinyl alcohol film can be improved, and the optical consistency of the obtained polyvinyl alcohol film is good.
[0043] Preferably, the prepa...
Embodiment 2
[0056] The difference between this embodiment and embodiment 1 is:
[0057] Step (3), followed by peeling and entering 18 drying rollers, the speed of the first 9 drying rollers is constant at 8m / min, the speed of the tenth roller is 8.1m / min, and the speed of the eleventh roller is 8.3m / min, Afterwards, the rotational speed of the rollers increases sequentially, and between adjacent drying rollers, the rotational speed increases by no more than 105%; the temperature of the roller surface is controlled at 80-95°C, and in this embodiment, the temperature of the roller surface is selected to be 90°C. From the beginning of one drying roll to the end of the last drying roll, the drying temperature of the roll surface remains constant.
Embodiment 3
[0059] The difference between this embodiment and embodiment 1 is:
[0060] Step (3), followed by peeling and entering 20 drying rolls, the speed of the first 10 drying rolls is constant at 6m / min, the speed of the 11th roll is 6.2m / min, and the speed of the 12th roll is 6.3m / min, After that, the rotation speed of the subsequent rollers increases sequentially, and the speed increase between adjacent drying rollers is not higher than 105%; the temperature of the roller surface is controlled at 80-95°C, starting from the first drying roller to the end of the last drying roller, The drying temperature of the roll surface decreases gradually, and the temperature difference between adjacent rolls is ≤1°C.
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