Formation method of high-specific-volume, high-flexibility and low-electric-leakage electrode foil
A chemical formation method and low leakage technology, applied in circuits, capacitors, electrolytic capacitors, etc., can solve the problems of low electrode foil specific volume, low bending strength, high current density, etc. High volume effect
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Embodiment 1
[0020] A high specific volume, high bending, low leakage electrode foil formation method, the specific implementation steps are as follows:
[0021] (1) Pretreatment: Put the corroded aluminum foil with a purity of 99.99wt% in pure water at a temperature of 97°C for 12 minutes, then depolarize the aluminum foil in 5wt% fumaric acid aqueous solution, fumaric acid The temperature of the acid solution is 85°C;
[0022] (2) Primary formation: immerse the pretreated aluminum foil in an aqueous solution containing 1wt% azelaic acid and 5wt% ammonium azelate at 85°C and 10mA / cm 2 , 6min under 120V condition;
[0023] (3) Secondary formation: the aluminum foil after the primary formation is immersed in an aqueous solution containing 1wt% azelaic acid, 3wt% ammonium azelate and 3wt% boric acid, at 85°C, 10mA / cm 2 , 250V conditions into 6min;
[0024] (4) Tertiary formation: the aluminum foil after the secondary formation is immersed in an aqueous solution containing 3wt% citric acid...
Embodiment 2
[0030] A high specific volume, high bending, low leakage electrode foil formation method, the specific implementation steps are as follows:
[0031] (1) Pretreatment: put the corroded aluminum foil with a purity of 99.99wt% in pure water at a temperature of 98°C for 9 minutes, then depolarize the aluminum foil in 1wt% fumaric acid aqueous solution, fumaric acid The temperature of the acid solution is 83°C;
[0032] (2) Primary formation: immerse the pretreated aluminum foil in an aqueous solution containing 2wt% azelaic acid and 2wt% ammonium azelate at 86°C, 8mA / cm 2 , 6min under 120V condition;
[0033] (3) Secondary formation: the aluminum foil after the primary formation is immersed in an aqueous solution containing 2wt% azelaic acid, 1.5wt% ammonium azelate and 1wt% boric acid, at 86°C, 8mA / cm 2 , 250V conditions into 6min;
[0034] (4) Tertiary formation: the aluminum foil after the secondary formation is immersed in an aqueous solution containing 1wt% citric acid, 3w...
Embodiment 3
[0040] A high specific volume, high bending, low leakage electrode foil formation method, the specific implementation steps are as follows:
[0041] (1) Pretreatment: Put the corroded aluminum foil with a purity of 99.99wt% in pure water at a temperature of 98°C for 10 minutes, and then depolarize the aluminum foil in 4wt% fumaric acid aqueous solution. The temperature of the acid solution is 84°C;
[0042] (2) Primary formation: immerse the pretreated aluminum foil in an aqueous solution containing 2wt% azelaic acid and 3wt% ammonium azelate at 86°C and 9mA / cm 2 , 6min under 120V condition;
[0043] (3) Secondary formation: the aluminum foil after the primary formation is immersed in an aqueous solution containing 2wt% azelaic acid, 2wt% ammonium azelate and 2wt% boric acid, at 86°C, 9mA / cm 2 , 250V conditions into 6min;
[0044] (4) Tertiary formation: the aluminum foil after the secondary formation is immersed in an aqueous solution containing 2wt% citric acid, 2wt% ammo...
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