Phosphor compound, LED device, and production method of LED device
A technology of LED devices and phosphors, applied in chemical instruments and methods, semiconductor devices, electrical components, etc., can solve the problem of low fluorescence quantum efficiency of gibbsite ore nano-luminescent materials, which cannot meet the application requirements of UV-type LEDs, and the preparation method can be Poor controllability and other issues, to achieve significant luminous effect, increase color rendering index, and meet the requirements of wide spectrum
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Embodiment 1
[0117] (1) Preparation of blue phosphor
[0118] Take an appropriate amount of organoaluminum salt precursor basic aluminum acetate (Al(OH)(Ac) 2 ), fully ground. Weigh 0.5000g-2.0000g of the ground basic aluminum acetate powder.
[0119] Put the weighed basic aluminum acetate powder into the quartz boat, put the quartz boat into the quartz tube, and then put the quartz tube into the heating area of the tube furnace. Connect the exhaust system, check the airtightness of the system after sealing, and set the heating conditions after confirming that the airtightness is good.
[0120] Nitrogen gas was introduced into the quartz tube for 30 minutes to exhaust. After the exhaust was completed, nitrogen gas was continuously injected at a rate of 50 sccm, and the heating program of the tube furnace system was started. The starting temperature is room temperature, and the heating rate is 26°C / min. After the temperature was raised to 290°C, the system was kept at 290°C for 2 hour...
Embodiment 2
[0140] (1) Preparation of blue phosphor
[0141] Take an appropriate amount of organoaluminum salt precursor basic aluminum acetate (Al(OH)(Ac) 2 ), fully ground. Weigh 1.25 g of ground basic aluminum acetate powder.
[0142] Put the weighed basic aluminum acetate powder into the quartz boat, put the quartz boat into the quartz tube, and then put the quartz tube into the heating area of the tube furnace. Connect the exhaust system, check the airtightness of the system after sealing, and set the heating conditions after confirming that the airtightness is good.
[0143] Nitrogen gas was introduced into the quartz tube for 30 minutes to exhaust. After the exhaust was completed, nitrogen gas was continuously injected at a rate of 50 sccm, and the heating program of the tube furnace system was started. The initial temperature is room temperature, and the heating rate is 30°C / min. After heating up to 300°C, the system was kept at 300°C for 2.5h.
[0144] After the tube furna...
Embodiment 3
[0161] (1) Preparation of blue phosphor
[0162] Take an appropriate amount of organoaluminum salt precursor basic aluminum acetate (Al(OH)(Ac) 2 ), fully ground. Weigh 1.25 g of the ground basic aluminum acetate powder.
[0163] Put the weighed basic aluminum acetate powder into the quartz boat, put the quartz boat into the quartz tube, and then put the quartz tube into the heating area of the tube furnace. Connect the exhaust system, check the airtightness of the system after sealing, and set the heating conditions after confirming that the airtightness is good.
[0164] Nitrogen gas was introduced into the quartz tube for 30 minutes to exhaust. After the exhaust was completed, nitrogen gas was continuously injected at a rate of 100 sccm, and the heating program of the tube furnace system was started. The starting temperature is room temperature, and the heating rate is 32°C / min. After the temperature was raised to 320°C, the system was kept at 320°C for 2.5 hours.
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