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Soundless wax-penetrating polishing agent for synthetic leather and preparation method thereof

A synthetic leather and treatment agent technology, applied in fiber treatment, textiles and papermaking, etc., can solve the problems of incompatibility between hand feeling and light feeling, easy oil slick, etc.

Inactive Publication Date: 2017-11-24
福建鸣鸿树脂有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Polishing treatment agent is a finishing agent for garment leather, shoe leather and bag leather. Traditional synthetic leather polishing products basically use nitrocellulose as a carrier and epoxy soybean oil as a throwing aid system. Therefore, it is easy to slick oil, and the hand feeling and light feeling are difficult to be compatible.

Method used

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  • Soundless wax-penetrating polishing agent for synthetic leather and preparation method thereof
  • Soundless wax-penetrating polishing agent for synthetic leather and preparation method thereof
  • Soundless wax-penetrating polishing agent for synthetic leather and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] A preparation method for synthetic leather with silent wax polishing treatment agent, comprising the steps of:

[0021] 1. Synthesis of silicone-modified polyurethane resin with 30% solid content: put 194kg of reactive silicone with a molecular weight of 2000 into a 3.8-ton reactor, add 242kg of PPG1000, add 145kg of PCL1000, add 107kg of IPDI, and add 128kg of H12MDI. Add 300kg of DMF, stir for 20 minutes, raise the temperature to 90°C-95°C for 2h, add 0.45kg of organic bismuth catalyst after 2h, keep warm and continue the reaction for 2.5h, cool down to 60°C by cooling cycle, add 1000kg of cyclohexanone, continue to cool down to 40 ℃, gradually add 82kgIPDI dropwise to increase the viscosity to 9000-10000CPS / 25℃, stop the reaction with morphine and stir for 30min, add 800kg ethyl ester and stir for 30min to unload;

[0022] 2, compounding of treatment agent: in 3 cubic meters of biaxial dispersing kettles, add 135kg of organosilicon-modified polyurethane resins with 3...

Embodiment 2

[0025] A preparation method for synthetic leather with silent wax polishing treatment agent, comprising the steps of:

[0026] 1. Synthesis of silicone-modified polyurethane resin with 30% solid content: put 190kg of reactive silicone with a molecular weight of 2000 into a 3.8-ton reactor, add 230kg of PPG1000, add 150kg of PCL1000, add 110kg of IPDI, and add 120kg of H12MDI. Add 280kg of DMF, stir for 20 minutes, raise the temperature to 90°C-95°C for 2h, add 0.4kg of organic bismuth catalyst after 2h, keep warm and continue the reaction for 2.5h, cool down to 60°C by cooling cycle, add 1100kg of cyclohexanone, continue to cool down to 40°C ℃, gradually add 70kg of IPDI dropwise to increase the viscosity to 9000-10000CPS / 25℃, stop the reaction with morphine and stir for 30min, add 750kg of ethyl ester and stir for 30min to unload;

[0027] 2. Treatment agent compounding: add 100kg of organosilicon-modified polyurethane resin with 30% solid content synthesized in the first ste...

Embodiment 3

[0030] A preparation method for synthetic leather with silent wax polishing treatment agent, comprising the steps of:

[0031] 1. Synthesis of silicone-modified polyurethane resin with 30% solid content: put 200kg of reactive silicone with a molecular weight of 2000 into a 3.8-ton reactor, add 250kg of PPG1000, add 140kg of PCL1000, add 100kg of IPDI, and add 140kg of H12MDI. Add 320kg of DMF, stir for 20 minutes, raise the temperature to 90°C-95°C for 2h, add 0.5kg of organic bismuth catalyst after 2h, keep warm and continue the reaction for 2.5h, cool down to 60°C by cooling cycle, add 900kg of cyclohexanone, continue to cool down to 40 ℃, gradually add 90kg IPDI dropwise to increase the viscosity to 9000-10000CPS / 25℃, stop the reaction with morphine and stir for 30min, add 850kg ethyl ester and stir for 30min to unload;

[0032]2, compounding of treatment agent: add the organic silicon modified polyurethane resin 150kg of the 30% solid content synthesized in the first step ...

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Abstract

The invention provides a soundless wax-penetrating polishing agent for synthetic leather and a preparation method thereof. The soundless wax-penetrating polishing agent comprises the following components by weight percent: 10%-15% of organic silicon modified polyurethane resin containing 30% of solids, 5%-10% of cellulose nitrocellulose wetted with 30% ethyl alcohol, 10%-15% of cyclohexanone, 5%-12% of ethylene glycol butyl ether, 40%-45% of n-butyl acetate, 5%-6% of nanometer gaseous silica, 0.2%-0.5% of an extinction powder dispersing agent, 2%-4% of acetyl tributyl citrate and 2%-3% of polyether modified simethicone. After the synthetic leather treated with the treating agent provided by the invention is polished by a polishing wheel, the synthetic leather has high surface luster, feels smooth, is soundless in the process of rubbing the leather surface and has strong fur-stimulated feel.

Description

technical field [0001] The invention belongs to the field of leather treatment, in particular to a silent wax polishing treatment agent for synthetic leather and a preparation method thereof. Background technique [0002] Synthetic leather is a plastic product that simulates the composition and structure of natural leather and can be used as its substitute material. Usually, the impregnated non-woven fabric is used as the mesh layer, and the microporous polyurethane layer is used as the grain layer. Its front and back are very similar to leather, and has a certain degree of air permeability, which is closer to natural leather than ordinary artificial leather. Widely used in making shoes, boots, bags and ball games. Polishing treatment agent is a finishing agent for garment leather, shoe leather and bag leather. Traditional synthetic leather polishing products basically use nitrocellulose as a carrier and epoxy soybean oil as a throwing aid system. Therefore, it is easy to...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/572D06M15/07D06M13/12D06M13/165D06M13/224D06M11/79D06M15/647
Inventor 伊华盛
Owner 福建鸣鸿树脂有限公司
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