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A method for rapid determination of effective rubber powder content of rubber powder modified asphalt

A modified asphalt, rapid measurement technology, applied in the direction of removing a certain component and weighing, etc., can solve the problem that the effective rubber powder content of rubber powder modified asphalt cannot be effectively measured, so as to shorten the dissolution time, the compression test period, the The effect of saving solvent

Active Publication Date: 2020-08-14
HEBEI PROVINCIAL COMM PLANNING & DESIGN INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] In view of the above analysis, this application aims to provide a method for quickly determining the effective rubber powder content of rubber powder modified asphalt, in order to solve the problem that the existing technology cannot effectively measure the effective rubber powder content in rubber powder modified asphalt

Method used

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  • A method for rapid determination of effective rubber powder content of rubber powder modified asphalt
  • A method for rapid determination of effective rubber powder content of rubber powder modified asphalt
  • A method for rapid determination of effective rubber powder content of rubber powder modified asphalt

Examples

Experimental program
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Effect test

Embodiment 1

[0091] Select 20% rubber powder-modified asphalt, of which the viscosity at 180°C is 2.4Pa·S, the penetration is 48 (0.1mm), the softening point is 71.5°C, and the ductility at 5°C is 13cm; among them, 20% rubber powder is mixed in The raw materials in the modified asphalt are 100 parts by mass of asphalt, 25 parts of rubber powder, 0.25 parts of epoxy fatty acid methyl ester, 2 parts of reinforcing agent phenolic resin, and 0.5 parts of crosslinking agent sulfur.

[0092] The method for quickly measuring the effective rubber powder content of rubber powder modified asphalt in this embodiment is as follows:

[0093] Step 1. Put the 100mL round-bottom flask, glass rod, and 100mm-diameter Buchner funnel used in the test into an oven at 105°C to dry for 15 minutes, then transfer to a desiccator to cool for 30 minutes, and weigh the mass m1 of the round-bottom flask to be 95.474 g, taking the glass rod quality m2 is 14.271g, and taking the Buchner funnel quality m3 is 273.285g;

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Embodiment 2

[0115] Select 25% rubber powder-modified asphalt, which has a viscosity of 3.1Pa·S at 180°C, a penetration of 64 (0.1mm), a softening point of 73.0°C, and a ductility of 14cm at 5°C; 25% rubber powder is mixed in it The raw materials in the modified asphalt are 100 parts by mass of asphalt, 34 parts of rubber powder, 0.25 parts of epoxy fatty acid methyl ester, 0.1 part of activator 980, 2 parts of reinforcing resin, and 0.5 parts of crosslinking agent sulfur share.

[0116] The method for quickly measuring the effective rubber powder content of rubber powder modified asphalt in this embodiment is as follows:

[0117] Step 1. Put the 100mL round-bottom flask, glass rod, and 100mm diameter Buchner funnel used in the test into an oven at 105°C to dry for 15 minutes, then transfer it to a desiccator to cool for 30 minutes, and weigh the mass m1 of the round-bottom flask to be 95.480 g, taking the glass rod quality m2 is 14.273g, and taking the Buchner funnel quality m3 is 273.28...

Embodiment 3

[0140] Select 30% rubber powder-modified asphalt, of which the viscosity at 180°C is 3.2Pa·S, the penetration is 56 (0.1mm), the softening point is 71.5°C, and the ductility at 5°C is 17cm; among them, 30% rubber powder is mixed in The raw materials in the modified asphalt are 100 parts by mass ratio of asphalt, 43 parts of rubber powder, 0.25 parts of epoxy fatty acid methyl ester, 0.14 parts of activator 980, 3 parts of reinforcing phenolic resin, and 0.5 parts of crosslinking agent sulfur .

[0141] The method for quickly measuring the effective rubber powder content of rubber powder modified asphalt in this embodiment is as follows:

[0142] Step 1. Put the 100mL round-bottom flask, glass rod, and 100mm-diameter Buchner funnel used in the test into an oven at 105°C to dry for 15 minutes, and then transfer it to a desiccator to cool for 30 minutes. Weigh the mass m1 of the round-bottom flask to be 95.467 g, taking the glass rod quality m2 is 14.276g, and taking the Buchner...

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Abstract

This application relates to a method for quickly determining the effective rubber powder content of rubber powder modified asphalt, which mainly includes: step 1, processing the instrument used for testing; step 2, heating the rubber powder modified asphalt to a molten state; preparing rubber powder modified asphalt solution; step 3, insert the Buchner funnel into the suction filter bottle; step 4, put the filter paper into the Buchner funnel; step 5, pour the rubber powder modified asphalt solution into the Buchner funnel, and suction filter; step 6, Put the Buchner funnel together with the filter paper in a ventilated place; step 7, place the used instrument in an oven, dry and cool, weigh the Buchner funnel together with the filter paper, round bottom flask and glass rod; step 8, calculate the effective rubber powder content , according to the content of effective rubber powder to determine the comprehensive performance of rubber powder modified asphalt. The beneficial effects of the application are: the dissolution time of rubber powder modified asphalt is greatly shortened, the experiment cycle is shortened, and a large amount of solvent is saved; the performance and thermal performance of 20% or more rubber powder modified asphalt can be comprehensively evaluated. stability.

Description

technical field [0001] The present application relates to the technical field of determination of effective rubber powder content in rubber powder modified asphalt, in particular to a method for rapidly measuring the effective rubber powder content of rubber powder modified asphalt. Background technique [0002] With the blowout growth of the number of cars in modern society, as of June 2016, the number of motor vehicles in the country reached 285 million. At the same time, the number of heavy-duty trucks is also increasing, which makes my country's Road traffic is faced with many challenges such as large flow and axle load. Ordinary road petroleum asphalt refined by oil refineries can no longer meet the various requirements of high-grade highways, especially expressways, on the performance of asphalt binders. SBS has been widely used because it can greatly improve the road performance of road asphalt, but SBS is a high value-added material, and its application in the field ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N5/04
CPCG01N5/04
Inventor 蔡斌王国清秦禄生张忠民朱冀军王联芳王庆凯薛善光高海涛刘家辉李磊王洪涛高辉张文哲
Owner HEBEI PROVINCIAL COMM PLANNING & DESIGN INST