A kind of layered potassium magnesium phosphate complex lithium base grease composition and preparation method thereof
A potassium-magnesium phosphate composite lithium-based lubricating grease and base lubricating grease technology, applied in the field of lubrication, to achieve the effects of abundant raw material sources, cost reduction, and easy industrialization
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0027] Add 31.32 g of PAO8 and 4.0 g of 12-hydroxystearic acid to the fat-making kettle, heat up and melt, and slowly add lithium hydroxide aqueous solution (containing 0.5 g of lithium hydroxide) at a temperature of 115 °C. After the lithium hydroxide solution was added, the temperature rose rapidly to 180 °C to completely dehydrate the soap base, and the material was quickly cooled to 115 °C, and 1.0 g of azelaic acid was added, stirred for 10 min, and lithium hydroxide aqueous solution (containing Lithium 0.5 g) to saponify azelaic acid, the temperature was raised to 180 °C and kept for 1 h to complete the dehydration, the temperature was rapidly raised to 200 °C and kept for 20 min, and 62.63 g of PAO8 was added to rapidly cool the lipid base, and continued to stir and cooled to 66 °C , add 0.05 g of diphenylamine, and grind evenly with a high-pressure homogenizer to obtain the basic complex lithium-based grease A.
[0028] Add raw materials into a 30 mL polytetrafluoroeth...
Embodiment 2
[0033]Add 27 g of 100 SN and 8.0 g of stearic acid to the fat-making kettle, heat up and melt, and slowly add lithium hydroxide aqueous solution (containing 2.0 g of lithium hydroxide) at a temperature of 80 °C. After the lithium hydroxide solution is added, the temperature rises rapidly to 130 °C to completely dehydrate the soap base, the material is quickly cooled to 90 °C, 4.0 g of adipic acid is added, stirred for 10 min, and lithium hydroxide aqueous solution (containing Lithium 2.0 g) to saponify adipic acid, raise the temperature to 130 °C and keep for 1 h to complete the dehydration, then rapidly raise the temperature to 220 °C and keep for 20 min, add 54 g of 100 SN to rapidly cool the lipid base, continue to stir and cool to 66 ℃, add 3 g of phenothiazine, and grind evenly with a three-roll machine to obtain the basic complex lithium-based grease B.
[0034] Add raw materials into a 30 mL polytetrafluoroethylene stainless steel kettle: 0.6 g magnesium sulfate, 3.73 g...
Embodiment 3
[0039] Add 28 g of liquid paraffin and 8.0 g of stearic acid to the fat-making kettle, heat up and melt, and slowly add lithium hydroxide aqueous solution (containing 1.5 g of lithium hydroxide) at a temperature of 90 °C. After the lithium hydroxide solution was added, the temperature rose rapidly to 140 °C to completely dehydrate the soap base, and the material was quickly cooled to 100 °C, and 3.0 g of sebacic acid was added, stirred for 10 min, and then lithium hydroxide aqueous solution (containing Lithium 1.5 g) to saponify sebacic acid, raise the temperature to 140 °C and keep for 1 h to complete the dehydration, then rapidly raise the temperature to 205 °C and keep for 20 min, add 54 g of liquid paraffin to rapidly cool the fat base, continue to stir and cool to 66 ℃, add 2.0 g of 2,6-di-tert-butyl-p-cresol, and grind it evenly with a three-roll machine to obtain the basic complex lithium-based grease C.
[0040] Add raw materials into a 30 mL polytetrafluoroethylene st...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More