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546 results about "Potassium phosphate" patented technology

Potassium phosphate is a generic term for the salts of potassium and phosphate ions including...

Method for controlling setting time and early hydration speed of magnesium potassium phosphate cement

InactiveCN102234200AEffective adjustment of clotting timeEffective control of clotting timeControl setOperability
The invention relates to a method for controlling the setting time and early hydration speed of magnesium potassium phosphate cement, and belongs to an early strength quick hardening cement cementing material. A composite retarder can effectively adjust the setting time of magnesium potassium phosphate cement slurry, and the setting time of the magnesium potassium phosphate cement slurry can be effectively controlled in the range of 10 minutes to 6 hours by adjusting the content of chloride and disodium hydrogen phosphate dodecahydrate in the composite retarder, so that the problems of a limited retarding effect, low operability and the like are solved; the composite retarder can change the hydration heat release characteristic of the magnesium potassium phosphate cement, the magnesium potassium phosphate cement slurry doped with the conventional retarder borax has a hydration heat release peak at the initial reaction stage and has a high heat release speed and large heat release amount, and the magnesium potassium phosphate cement doped with the composite retarder has two hydration heat release peaks and has small hydration heat release amount at the initial hydration stage; and the doped composite retarder improves the microstructure and later strength of a hardened magnesium potassium phosphate cement body, so that enough construction operable time can be ensured while the magnesium potassium phosphate cement slurry has early strength and is quickly hardened.
Owner:苏州诚开新材料有限公司

Hole channel amplification method of porous ceramic microballoon sphere

The invention discloses a hole channel amplification method of a porous ceramic microballoon sphere for liquid chromatography, which enables silica, zirconium dioxide or titanium dioxide powder to serve as ceramic framework materials, enables nanometer powdered carbon, ammonium chloride, polyving akohol, urea, polyethylene glycol, sodium chloride, sodium sulfate, sodium phosphate, potassium phosphate, potassium chloride, potassium sulfate and the like to serve as porogen, and prepares macropore ceramic microballoon spheres through reversed phase suspension and high temperature sintering. The specific steps are as following: (1) preparing ceramic slurry, enabling the ceramic framework materials, the porogen and sodium alginate solution to be mixed; (2) preparing the porous ceramic microballoon sphere, enabling the ceramic slurry to be conducted reversed phase suspension and dispersion in an oil phase, adding saturation calcium chloride solution in a dropping mode, solidifying to from the sphere, and molding by high temperature sintering; and (3) removing residual porogen, enabling the ceramic microballoon sphere to be soaked in water, hydrochloric acid or sodium hydroxide solution, shaking to dissolve the residual porogen. The microballoon sphere developed by the method has the advantages of having rigidity, and being big in hole diameter and good in spherical degree, and the microballoon sphere can be used for substrates of large biological molecule chromatographic separation media.
Owner:嘉兴千纯生物科技有限公司

High-efficiency iron rust conversion agent

The utility model relates to a high-efficiency iron rust conversion agent, and belongs to the field of an antirust paint. The iron rust conversion agent comprises the following raw materials by weight: 0.1-10% of zinc oxide, 20-40% of phosphoric acid, 0.5-15% of dichromate, 0.5-10% of phosphate, 0.1-10% of corrosion inhibitor, and 50-70% of solvent, wherein the dichromate is potassium dichromate or sodium dichromate; the phosphate is sodium phosphate or potassium phosphate; the corrosion inhibitor is urotropine or urea; and the solvent is water or ethanol. The preparation method comprises the steps as follows: sequentially adding the solvent, the phosphoric acid, the dichromate, the phosphate, the corrosion inhibitor and the zinc oxide to a glass cup under persistently stirring according to the mass ratio, and dissolving for 10-20 min. The production method bases on the dissolving of the solid reactants in the phosphoric acid solution. The phosphorized film formed by iron rust conversion has the effects of preventing rust and fixing remnant rust, and the formed phosphorized layer protective film is long-acting, and stable in atmospheric environment, lubricating oil and organic solvent, has high adhesion, can be used as a primer, has dielectric properties, and can prevent electro-chemical corrosion on the metal surface.
Owner:ZHEJIANG OCEAN UNIV

Soil-improving continuous-cropping-resistant compound fertilizer for vegetables and preparation method thereof

The invention discloses a soil-improving continuous-cropping-resistant compound fertilizer for vegetables. Raw materials of the compound fertilizer comprise, by weight, 10-15 parts of urea, 10-12 parts of ammonium nitrate, 15-20 parts of potassium phosphate, 10-15 parts of calcium magnesium phosphate fertilizer, 3-5 parts of potassium sulfate, 1-3 parts of calcium chloride, 2-4 parts of carbonized rice husk, 3-5 parts of peat, 1-3 parts of attapulgite, 5-8 parts of guano, 15-20 parts of Chinese medicine residue, 10-15 parts of soybean meal, 10-20 parts of plant ash, 3-5 parts of EM bacterial powder and 8-10 parts of polyvinyl alcohol. The invention also discloses a preparation method of the above soil-improving continuous-cropping-resistant compound fertilizer for vegetables. The compound fertilizer has rich nutrients. through cooperation of organic fertilizer, carbonized rice husk, peat, attapulgite, EM bacterial powder and polyvinyl alcohol, the product helps improve soil, adjust soil pH and maintain soil fertility from three aspects of water retention, air permeability and fertilizer efficiency maintenance. With the cooperation of the Chinese medicine residue, the product helps inhibit and kill insect disease, promote healthy growth of vegetables and avoid continuous-cropping and insufficient nutrition of vegetables.
Owner:ANHUI SIERTE FERTILIZER IND

Preparation method for efficient chain transfer agent trithiocarbonate used for RAFT (reversible addition-fragmentation chain transfer) polymerization

The invention belongs to the field of polymer nano biological medicinal materials, particularly relates to a preparation method for efficient chain transfer agent trithiocarbonate used for RAFT polymerization. The method is characterized in that the chemical formula of the trithiocarbonate is C17H32O2S3, and comprises the following steps: adding potassium phosphate, a solvent and carbon bisulfide into a round-bottom flask for reaction 1-3 hours; adding do-decyl mercaptans to conduct addition reaction for 1-3 hours; and finally adding 2-bromine isobutyric acid to conduct esterification reaction for 13-24 hours. The brilliant orange trithiocarbonate can be obtained from the reacted solvent subjected to procedures of reduced pressure distillation for removal, dissolution, extraction, and washing, wherein the mass ratio of the potassium phosphate to the carbon bisulfide is 1:(1-3), as well as the mass ratio of the do-decyl mercaptans to the carbon bisulfide, and the mass ratio of the 2-bromine isobutyric acid to the carbon bisulfide are also 1: (1-3). According to the method provided by the invention, the synthesizing is simple, the purification is convenient, and the stability of the product is good. Moreover, the RAFT polymerization has an efficient chain transfer effect. Therefore, the method is favorable for advancing the RAFT large-scale industrial production, and has an extensive application prospect.
Owner:TONGJI UNIV

Process for producing potassium phosphate with wet phosphoric acid

The invention relates to a process for producing potassium phosphate with wet phosphoric acid. The process comprises the following steps that: 1) wet phosphoric acid is put into an ultrasonic reactor for ultrasonication at the temperature of 2-80 degree centigrade with the reaction time of 10-120 minutes; then the product is cooled to be at room temperature and precipitates are leached, thus obtaining a filter liquor; 2) potassium hydroxide, potassium carbonate or potassium bicarbonate is used to regulate the PH value of the filter liquor and generate precipitates, and a new filter liquor obtained after filtering is concentrated, evaporated, crystallized and then separated, thus obtaining potassium phosphate. The process is characterized in that wet phosphoric acid with low purity, purity and cost, lead-bearing material and potassium chloride are used as raw materials to react and generate potassium phosphate, which reduces production cost. Impurities in the raw materials interact and generate insoluble precipitates, and the insoluble precipitates can be easily separated. In the simple process, products are generated only by concentrating and crystallizing a neutralizer; potassium phosphate is directly prepared by utilizing phosphoric acid with the concentration of 5-40%, which solves the problems of low consistency of wet phosphoric acid and high energy consumption for concentration.
Owner:WUHAN INSTITUTE OF TECHNOLOGY

Production method of microbial fermented seaweed fertilizer

The invention relates to a production method of a microbial fermented seaweed fertilizer. The production method comprises the following steps: soaking dried seaweed, taking the liquid supernatant and filtering by use of an ion exchange resin, thereby obtaining a solution A; returning the solution A to a reaction kettle, adding one or two of potassium citrate, potassium oxalate, potassium pyrophosphate and the like in a certain weight ratio for softening and digesting the seaweed at a certain temperature, and performing centrifugal separation on the clear liquid obtained after processing to obtain the filtrate, namely a solution B; supplementing water to the centrifuged seaweed residue and regulating the Ph, next, adding microorganisms and a culture medium, fermenting at a certain temperature, and performing centrifugal separation after fermentation to obtain a solution C after centrifuging; mixing the solution B and the solution C and then mixing with nitrogen fertilizer, phosphatic fertilizer, potash fertilizer, chelate medium trace elements and the like in a certain weight ratio to obtain the microbial fermented seaweed fertilizer. The microbial fermented seaweed fertilizer produced by the production method is capable of improving the growing environment of crop root systems and solving the problem of soil hardening so that the soil is loose, good in moisture and fertility preservation property and excellent in air permeability; as a result, crops can grow healthily in a good environment.
Owner:烟台嘉特生物技术有限公司
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