Preparation method for porous titanium-ceramic composite biological material

A porous material and biological technology, applied in the field of porous composite materials and medical metal materials, can solve the problems of poor biocompatibility, insufficient mechanical properties of porous titanium alloy system, etc., to improve biological activity, biocompatibility and biological activity , the effect of improving biocompatibility

Inactive Publication Date: 2017-12-22
NORTHEASTERN UNIV
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  • Abstract
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  • Claims
  • Application Information

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Problems solved by technology

[0006] The invention provides a method for preparing a titanium-ceramic composite biological porous material, which success

Method used

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  • Preparation method for porous titanium-ceramic composite biological material

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Embodiment 1

[0024] (1) Ti2448 (Ti-24Nb-4Zr-8Sn, purchased from Institute of Metals, Chinese Academy of Sciences) and nano ZrO 2 Mix the ingredients according to the mass ratio of 95:5, then add the mixed material and zirconia grinding balls into the ball milling jar according to the mass ratio of 1:2, and add alcohol to two-thirds of the ball milling jar. Mixed material in planetary ball mill 300r·min -1 Under the ball milling for 10h, stop for 1h when the ball mill reaches 5h. The ball-milled raw materials are dried in a 120°C drying oven at a constant temperature, and 10wt.% NH is added after drying 4 HCO 3 Pore-forming agent and 4wt.% polyethylene glycol binder, and fully hand-grinded in an agate mortar for 30min;

[0025] (2) Pour the raw material powder mixed uniformly through hand grinding into a stainless steel mold for compaction, and then hold it under a pressure of 200MPa for 5min to form it;

[0026] (3) Put the pressed sample into a tube-type resistance furnace, use a vacu...

Embodiment 2

[0028] (1) Ti2448 (Ti-24Nb-4Zr-8Sn, purchased from Institute of Metals, Chinese Academy of Sciences) and nano ZrO 2 Mix the ingredients according to the mass ratio of 95:5, then put the mixed material and zirconia grinding balls into the ball milling jar according to the mass ratio of 1:2, and add alcohol to two-thirds of the ball milling jar. Mixed material in planetary ball mill 300r·min -1 Under the ball milling for 10h, stop for 1h when the ball mill reaches 5h. The ball-milled raw materials are dried in a 120°C drying oven at a constant temperature, and 30wt.% NH is added after drying 4 HCO 3 Pore-forming agent and 3wt.% polyethylene glycol binder, and fully hand-grinded in an agate mortar for 30min;

[0029] (2) Pour the raw material powder mixed uniformly through hand grinding into a stainless steel mold for compaction, and then hold it under a pressure of 250MPa for 5min to form it;

[0030] (3) Put the pressed sample into a tubular muffle furnace, use a vacuum pum...

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Abstract

The invention discloses a preparation method for a porous titanium-ceramic composite biological material, and relates to the field of porous composite materials and medical metal materials. The preparation method specifically comprises the technical steps of firstly, mixing an titanium alloy and nano-oxide ceramics according to a preset ratio, carrying out ball milling and then adding a pore forming agent and a binding agent for pressing; and then, sintering a sample in a high-temperature furnace according to a preset sintering parameter and carrying out furnace cooling so as to obtain a final product. The method has the advantages that the defects of poor mechanical property, low biocompatibility, no biological activity and the like of a traditional medical titanium alloy can be overcome, the process is simple, the consumption is low, the environment can be protected, the cost is low, the economical efficiency can be achieved, and industrial production can be realized easily.

Description

technical field [0001] The invention belongs to the technical field of porous composite materials and medical metal materials, and relates to a preparation method of titanium-ceramic composite biological porous materials. Background technique [0002] With the continuous development of the economy and the continuous progress of the society, people have higher and higher requirements for the quality of life, especially in the emphasis on medical health. In recent years, the demand for biomaterials has been increasing day by day, which also reflects the future development direction of the material industry. Therefore, the development of biomedical materials that are stable, easy to use, safe and reliable, and have excellent performance is one of the important topics in the field of materials today. [0003] At present, the biometal materials that are well developed and widely used mainly include stainless steel and titanium alloys, which are mainly used in the replacement of ...

Claims

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Application Information

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IPC IPC(8): C22C1/08C22C14/00C22C32/00B22F3/11
CPCB22F3/11C22C1/08C22C14/00C22C32/001
Inventor 马北越任鑫明张博文张亚然于景坤
Owner NORTHEASTERN UNIV
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