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Gel for detecting formaldehyde in air and water solution

An aqueous solution and gel technology, which is applied in the direction of analyzing materials through chemical reactions and material analysis through observing the impact on chemical indicators, can solve the problems of short shelf life of working fluids and inability to produce single-component products. Achieve the effect of being conducive to observing discoloration, fast detection speed, and easy detection operation

Inactive Publication Date: 2017-12-26
赵东育
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Commonly used formaldehyde detection methods include: phenol reagent method, phloroglucinol method, Schiff reagent, chromotropic acid and other common methods. production
At present, there is no portable single-component product on the market that has a shelf life of 12-18 months at room temperature and is suitable for rapid qualitative detection of formaldehyde in both air and water environments.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The preparation method of one-component formaldehyde detection gel, it comprises the steps:

[0025] Take 99 parts by mass of distilled water and heat to 85°C, add 1 part by mass of basic fuchsin, stir to dissolve, filter while hot to obtain a 1% concentration of basic fuchsin solution, cool to room temperature for later use;

[0026] Get 5 mass parts of basic fuchsin solution of the above-mentioned 1% concentration, add 70 mass parts of distilled water and start stirring, then add 10 mass parts of 10% sodium sulfite solution, stir for 30 minutes, add 10 mass parts of 4% sulfuric acid solution, stir for 30 minutes Minutes, add 0.5 parts by mass of activated carbon, stir for 10 minutes, let stand overnight, filter to obtain a colorless and transparent detection reagent for subsequent use;

[0027] Take 70 parts by mass of the detection reagent, sieve into 0.3 parts by mass of polyacrylic acid resin powder as a thickening gel, stir and disperse evenly to obtain a detectio...

Embodiment 2

[0031] The preparation method of one-component formaldehyde detection gel, it comprises the steps:

[0032] Take 99 parts by mass of distilled water and heat to 85°C, add 1 part by mass of basic fuchsin, stir to dissolve, filter while hot to obtain a 1% concentration of basic fuchsin solution, cool to room temperature for later use;

[0033] Get 5 mass parts of basic fuchsin solution of the above-mentioned 1% concentration, add 80 mass parts of distilled water and start to stir, then add 10 mass parts of 10% sodium sulfite solution, stir for 30 minutes, add 10 mass parts of 4% sulfuric acid solution, stir for 30 minutes minutes, add 0.1 parts by mass of activated carbon, stir for 10 minutes, let stand overnight, filter to obtain a colorless and transparent detection reagent for subsequent use;

[0034] Take 70 parts by mass of the detection reagent, add 4 parts by mass of the thickening gel agent Carboresin, stir and disperse evenly to obtain a detection solution for later use...

Embodiment 3

[0038] The preparation method of one-component formaldehyde detection gel, it comprises the steps:

[0039] Take 99 parts by mass of distilled water and heat to 85°C, add 1 part by mass of basic fuchsin, stir to dissolve, filter while hot to obtain a 1% concentration of basic fuchsin solution, cool to room temperature for later use;

[0040] Get 5 mass parts of basic fuchsin solution of the above-mentioned 1% concentration, add 80 mass parts of distilled water and start to stir, then add 10 mass parts of 10% sodium sulfite solution, stir for 30 minutes, add 10 mass parts of 4% sulfuric acid solution, stir for 30 minutes minutes, add 0.1 parts by mass of activated carbon, stir for 10 minutes, let stand overnight, filter to obtain a colorless and transparent detection reagent for subsequent use;

[0041] Take 70 parts by mass of the detection reagent, add 10 parts by mass of a thickening gel superabsorbent resin, stir and disperse evenly to obtain a detection solution for use; t...

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PUM

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Abstract

The invention relates to detection gel, and in particular to one-component gel for detecting formaldehyde in air and water solutions, which is applicable to the field of environment detecting. A preparation method of the gel is as follows: taking 99 mass parts of distilled water, heating to 85 DEG C, adding 1 mass part of basic fuchsin, and stirring. The gel for detecting the formaldehyde in the air and the water solutions is characterized in that the preparation method comprises the following steps: taking 5 mass parts of 1% basic fuchsin solution, adding 70 to 80 mass parts of distilled water, starting stirring, then adding 10 mass parts of 10% sodium sulphite solution, adding 10 mass parts of 4% sulfuric acid solution, adding 0.1 to 0.5 mass part of active carbon, stirring, standing, and filtering to obtain a colorless and transparent detection reagent for later use; taking 70 mass parts of the detection reagent, adding 0.3 to 10 mass parts of thickening gel, uniformly stirring and dispersing, so as to obtain a detection solution for later use; then taking 0.1 to 0.5 mass part of polyamino acid coenzyme to be dissolved in 10 mass parts of distilled water, gradually dropwise adding an obtained solution into the detection solution, and gradually gelling the solution to a paste, adding distilled water to 100 mass parts, uniformly stirring, thus obtaining the toothpaste-shaped formaldehyde-detecting gel.

Description

technical field [0001] The invention relates to a detection gel, in particular to a single-component formaldehyde detection gel in air and aqueous solution, which is suitable for the field of environmental detection. Background technique [0002] Formaldehyde is a widely used chemical raw material, and it is also the main pollutant of indoor air pollution after room decoration. The national GB50325-2010 standard stipulates that the indoor formaldehyde concentration shall not exceed 0.1 (mg / m³). There are also some businesses that add or spray formaldehyde solution to seafood, vegetables and other foods to achieve the purpose of keeping fresh. Consumers and regulators, in the field, need a convenient, rapid, semi-quantitative reagent to detect the presence of formaldehyde in air and water. [0003] At present, the rapid detection products such as formaldehyde detection boxes and test strips sold on the market are all two-component or three-component, and the operation proces...

Claims

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Application Information

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IPC IPC(8): G01N21/78
Inventor 赵东育
Owner 赵东育
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