Device and method for preparing graphene from carbon material in laser shock liquid medium

A liquid medium, laser shock technology, applied in graphene, nanocarbon and other directions

Active Publication Date: 2018-01-16
JIANGSU UNIV
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  • Abstract
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  • Claims
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However, tiny graphene cannot really exert its superior properties. Therefore, re

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  • Device and method for preparing graphene from carbon material in laser shock liquid medium

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[0018] The technical solutions of the present invention will be described in more detail below with reference to the accompanying drawings, but are not intended to limit the present invention.

[0019] like figure 1 As shown, it includes a laser generating system and a reaction vessel 27 located below the laser generating system. Both sides of the bottom of the reaction vessel 27 are provided with lead screws 25 in the Y-axis direction. Driven by the second motor 21, the plate 17 can move back and forth in the Y-axis direction on the lead screw 25. A second rotating shaft 24 and a first rotating shaft 18 are mounted on the support plate 17, and the second rotating shaft 24 is mounted on the support plate 17. A copper foil 23 is wound, a first motor 20 is mounted on the first rotating shaft 18 , and the copper foil 23 is rotated from the second rotating shaft 24 to the first rotating shaft by the rotation of the first motor 20 . 18, the first motor 20 is connected with the rig...

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Abstract

The invention relates to a device and a method for massively preparing graphene from a carbon material in a laser shock liquid medium. The device comprises a system for preparing graphene through laser, and a system for transferring the graphene on different substrates. Laser generated by a high-power pulse laser generator is reflected by a light mirror, the obtained laser beam is vertically focused in a proper position of the upper surface of a graphite block target material in an aqueous solution medium, a direct current electric field with the voltage being direct current 24 V is applied totwo ends of the graphite target material, one electrode of the electric field is a copper plate fixed at one end of a reaction tank, the other end of the reaction tank adopts copper foil, a motor drives the copper foil to move at a constant speed, a high-temperature and high-voltage plasma is formed between the graphite and the aqueous medium at the moment of shocking the graphite with the laser,the plasma adheres to the surface of the copper foil under the driving of the electric field, the plasma is continuously adhered, and the copper foil continuously moves in order to finally achieve the purpose of continuous massive preparation of the graphene.

Description

technical field [0001] The invention belongs to the high-efficiency preparation of graphene technology, in particular to a device and method for preparing graphene by laser shocking carbon materials in a liquid medium. Background technique [0002] Graphene has attracted the attention of researchers in the past ten years. It is a new type of carbon nanomaterial with only a single atomic layer thickness, and the thickness of a single layer is only 0.3554nm. Graphene not only has the unique properties of nanomaterials, but also has extremely high hardness. It is the strongest material we know in the world today, with a tensile strength of 125GPa and an elastic modulus as high as 1.1TPa. Moreover, the thermal conductivity of graphene under normal environmental conditions is 5x103W / (mK), which is an order of magnitude higher than that of copper under the same conditions. Graphene has excellent optical transparency (light absorption rate is only 2.3%), high electrical conductivi...

Claims

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Application Information

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IPC IPC(8): C01B32/19
Inventor 任旭东贾唯马服辉王冕
Owner JIANGSU UNIV
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