Preparation method of special coating ink inkjet printing adhesive
A technology of inkjet printing and adhesives, which is applied in the direction of application, ink, dyeing, etc., to achieve the effect of improving the color fastness of printing
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preparation example Construction
[0013] The invention provides a technical solution: a preparation method of inkjet printing adhesive specially used for paint ink, the steps of which are as follows:
[0014] Add 0.5-2% wt of the emulsifier mixed with fatty acid polyoxyethylene ether sodium sulfate and tridecyl polyoxyethylene ether (accounting for the total amount of adhesive, the same below) into 20-25% wt of distilled water and stir evenly, then Add 28-33%wt of butyl acrylate, 2-5% of styrene, and 2-5% of acrylonitrile. Use an emulsifier to emulsify at 1000r / min for 15-20mins to obtain pre-emulsified monomers. Take out 5-8% of pre-emulsified monomers. Add 0.5-1% IBMA to the body, and use an emulsifier to emulsify at 1000r / min for 5mins.
[0015] Dissolve 0.1-0.15% ammonium persulfate in 3-4% water, add 25-35% distilled water and 0.2-0.5% itaconic acid into a 1L four-neck flask equipped with a stirrer, a constant pressure dropping funnel and a thermometer, Initially add 5% pre-emulsified monomer and 10% amm...
Embodiment 1
[0018] Add a total of 8g of emulsifier mixed with fatty acid polyoxyethylene ether sodium sulfate and tridecyl polyoxyethylene ether (accounting for the total amount of adhesive, the same below) into 270g of distilled water and stir evenly, then add 300g of butyl acrylate, styrene 30g, 30g of silicone oil, emulsified at 1000r / min for 15mins using an emulsifier to obtain pre-emulsified monomers, took out 50g of pre-emulsified monomers, added 5g of IBMA, and emulsified at 1000r / min for 5mins with an emulsifier.
[0019] Dissolve 1.2g of ammonium persulfate in 40% water, add 300g of distilled water and 2g of itaconic acid into a 1L four-neck flask equipped with a stirrer, a constant pressure dropping funnel and a thermometer, initially add 40g of pre-emulsified monomer and 15g of Stir ammonium persulfate solution in a water bath at 80-85°C, add the remaining pre-emulsified monomer and ammonium persulfate dropwise, and control the dropping time for 150mins. The pH of the emulsion ...
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