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Preparation method of special coating ink inkjet printing adhesive

A technology of inkjet printing and adhesives, which is applied in the direction of application, ink, dyeing, etc., to achieve the effect of improving the color fastness of printing

Inactive Publication Date: 2018-01-16
HEFEI JUHE RADIAL CHEM TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, most polyacrylate emulsions on the market contain a certain amount of N-methylolacrylamide, which will release formaldehyde during baking and storage and add to the defects of the prior art

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0013] The invention provides a technical solution: a preparation method of inkjet printing adhesive specially used for paint ink, the steps of which are as follows:

[0014] Add 0.5-2% wt of the emulsifier mixed with fatty acid polyoxyethylene ether sodium sulfate and tridecyl polyoxyethylene ether (accounting for the total amount of adhesive, the same below) into 20-25% wt of distilled water and stir evenly, then Add 28-33%wt of butyl acrylate, 2-5% of styrene, and 2-5% of acrylonitrile. Use an emulsifier to emulsify at 1000r / min for 15-20mins to obtain pre-emulsified monomers. Take out 5-8% of pre-emulsified monomers. Add 0.5-1% IBMA to the body, and use an emulsifier to emulsify at 1000r / min for 5mins.

[0015] Dissolve 0.1-0.15% ammonium persulfate in 3-4% water, add 25-35% distilled water and 0.2-0.5% itaconic acid into a 1L four-neck flask equipped with a stirrer, a constant pressure dropping funnel and a thermometer, Initially add 5% pre-emulsified monomer and 10% amm...

Embodiment 1

[0018] Add a total of 8g of emulsifier mixed with fatty acid polyoxyethylene ether sodium sulfate and tridecyl polyoxyethylene ether (accounting for the total amount of adhesive, the same below) into 270g of distilled water and stir evenly, then add 300g of butyl acrylate, styrene 30g, 30g of silicone oil, emulsified at 1000r / min for 15mins using an emulsifier to obtain pre-emulsified monomers, took out 50g of pre-emulsified monomers, added 5g of IBMA, and emulsified at 1000r / min for 5mins with an emulsifier.

[0019] Dissolve 1.2g of ammonium persulfate in 40% water, add 300g of distilled water and 2g of itaconic acid into a 1L four-neck flask equipped with a stirrer, a constant pressure dropping funnel and a thermometer, initially add 40g of pre-emulsified monomer and 15g of Stir ammonium persulfate solution in a water bath at 80-85°C, add the remaining pre-emulsified monomer and ammonium persulfate dropwise, and control the dropping time for 150mins. The pH of the emulsion ...

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PUM

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Abstract

The present invention discloses a preparation method of a special coating ink inkjet printing adhesive, the method is as follows: adding 0.5-2 wt % of a fatty acid polyoxyethylene ether sulfate sodiumand tridecyl polyoxyethylene ether mixed emulsifier into 20-25 wt % of distilled water, stirring evenly, adding 28-33 wt % of butyl acrylate, 2-5% of styrene and 2-5% of acrylonitrile, using an emulsifying machine for emulsifying at 1000r / min for 15-20mins, taking 5-8% of a pre-emulsified monomer out, adding 0.5-1% of IBMA, using the emulsifying machine for emulsifying at 1000r / min for 5mins,dissolving 0.1-0.15% of ammonium persulfate in 3-4% of water, adding 25-35% of distilled water and 0.2-0.5% of itaconic acid into a flask, first adding 5% of the pre-emulsified monomer and 10% of anammonium persulfate solution, stirring, dropwise adding the remaining pre-emulsified monomers and ammonium persulfate, thermally insulating for reaction for 1-1.5h, adjusting emulsion pH to 6.5-7.5 with ammonium hydroxide, filtering and discharging. The special coating ink inkjet printing adhesive has no formaldehyde release. When applied to coating ink ink-jet printing process, the special coating ink inkjet printing adhesive can improve the printing color fastness and obtain soft hand feeling. The special coating ink inkjet printing adhesive product has a small particle size, can pass through EPSON, star and other nozzles, and has no nozzle blocking problem.

Description

technical field [0001] The invention relates to the technical field of an environmentally friendly fine-grained acrylic resin special adhesive for paint and ink for inkjet printing of fabrics, in particular to a preparation method of an inkjet printing special adhesive for paint and ink. Background technique [0002] With the improvement of the overall level of the world economy, people's demand for clothing and textiles is becoming more and more individualized and diversified, which requires the traditional textile industry to change to the direction of multi-variety and small-batch production. Textile digital inkjet printing technology is characterized by high-quality and short-process printing, and the production response process is short and fast, which can well meet the requirements of immediate delivery. At present, the research and development of digital inkjet printing technology mainly focuses on printing machines, inks and processes. Inkjet printing ink can be div...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F220/18C08F212/08C08F220/44C08F220/58C08F2/30C08F2/26C09D11/30D06P1/52
Inventor 张清润吴昊天王冬
Owner HEFEI JUHE RADIAL CHEM TECH
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