Application of compound notoginsenoside Ft1 in preparation of drugs for treatment of Parkinson's disease
A Parkinson's disease, notoginseng saponin technology, applied in the application field of medicine and functional food, can solve the application and report of notoginseng saponin Ft1 that has not been discovered, the patient cannot be cured, and the report of the application of the compound has not been found, etc.
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Embodiment 1
[0016] Preparation of notoginseng saponin Ft1:
[0017] The stems and leaves of notoginseng are extracted with 10 times the amount of 1% HCl solution, extracted twice, each time for 2 hours, the filtrates are combined, the pH is adjusted to 7 with 3% NaOH solution, concentrated and dried to obtain a dry paste. Dry paste 100g, mix sample with silica gel (200-300 mesh) and carry out silica gel column chromatography, use chloroform: methanol: water (8:2:0.2) as eluent, thin layer chromatography checks and merges the same color point Fractions, Fr1-5 fractions were obtained. Fr4 (5g) was subjected to repeated silica gel column chromatography and reversed-phase silica gel RP-18 column chromatography (methanol: water / 7:3) with chloroform: methanol: water (8:2:0.2) as the eluent to obtain three Heptasaponin Ft1 (0.12 g).
[0018] Structural identification of notoginseng saponin Ft1:
[0019] Instrument: mass spectrometry (MS) is measured with VGAutopec-3000 mass spectrometer; nucl...
Embodiment 2
[0026] Activity experiment of notoginseng saponin Ft1 in treating PD function:
[0027] 1. Materials
[0028] 1.1 Animal source
[0029] SPF grade C57 / BL6J mice, male, 22-24 g, 12-14 weeks, provided by Chengdu Dashuo Experimental Animal Co., Ltd. Animal production license number: SCXK (Sichuan) 2015-030. The mice were kept in the IVC animal laboratory at a temperature of 20-25°C (daily temperature difference ≤3°C); humidity 40%-70%; lighting 12h: 12h alternating light and dark, illumination 150-300lx; noise ≤60dB. Experimental animal use license: SYXK (Dian) K2013-0002, issuing unit: Kunming Science and Technology Bureau.
[0030] 1.2 Drugs and reagents
[0031] Notoginseng saponin ft1 (supplement); 1-methyl-4-phenyl-1,2,3,6-tetrahydropyridine (MPTP) was purchased from Sigma, USA, product number M0896; TH Rabbit Polyclonal antibody was purchased from proteintech, product number : 25859-1-AP, DAB staining solution (enhanced polymer method) kit was provided by Fuzhou Maixin...
Embodiment 3
[0059] Dissolve notoginseng saponin Ft1 in sterile water for injection to dissolve, then filter through a sterile funnel, fine filter, potting, and sterilize,
[0060] Made into injection.
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