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Isooctyl palmitate preparation device with alcohol removal effect

A technology for isooctyl palmitate and a preparation device, which is applied in the field of isooctyl palmitate preparation devices, can solve problems such as affecting product quality and reducing the scope of use, and achieves improved output per unit time, convenient operation and high reaction conversion rate Effect

Inactive Publication Date: 2018-03-09
枝江市楚怡化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The traditional preparation method of isooctyl palmitate uses the product of esterification reaction between palmitic acid and isooctyl alcohol, but isooctyl alcohol remains in the product during the esterification process, and isooctyl alcohol will cause the product to emit peculiar smell. The method of octanol is distillation, but there are certain defects in the distillation method, which seriously affects the quality of the product, resulting in a narrower range of use

Method used

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  • Isooctyl palmitate preparation device with alcohol removal effect

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Embodiment Construction

[0019] The embodiments of the present invention will be further described below in conjunction with the drawings.

[0020] participate figure 1 , A device for preparing isooctyl palmitate with the effect of removing alcohol, characterized in that it includes a reaction tower 2, and the top of the reaction tower 2 is connected with an exhaust pipe 6, an isooctyl alcohol recovery pipe 10, and a palmitic acid inlet 1. The exhaust pipe 6 is connected to an isooctyl alcohol receiving tank 7, a condenser 8 is provided outside the isooctyl alcohol receiving tank 7, and the isooctyl alcohol receiving tank 7 is connected to a No. 1 oil-water separator 9. The oil outlet of the No. oil-water separator 9 is connected to the isooctyl alcohol recovery pipe 10, the outlet of the No. 1 oil-water separator 9 is connected to the No. 1 water receiving tank 11, and the side of the reaction tower 2 is connected with isooctyl alcohol and a catalyst inlet 12. The outlet of the reaction tower 2 is conn...

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Abstract

The invention relates to a device for preparing isooctyl palmitate with the effect of removing alcohol, which comprises a reaction tower, and the top of the reaction tower is connected with an exhaust pipe, an isooctyl alcohol recovery pipe and a palmitic acid inlet, and the exhaust pipe is connected with The isooctyl alcohol receiving tank, the isooctyl alcohol receiving tank is connected to the No. 1 oil-water separator, the side of the reaction tower is connected with isooctyl alcohol and the catalyst inlet, and the discharge port of the reaction tower is connected to the No. 2 oil-water separator. The finished product outlet of the No. 2 oil-water separator is connected with the finished product heating tank, and the other outlet of the No. 2 oil-water separator is connected with the catalyst recovery tank, and the catalyst recovery tank is connected with the isooctyl alcohol and the catalyst inlet through the No. 1 pump; the heat exchange There is an alcohol removal device connected to the device. This preparation system can efficiently and quickly prepare isooctyl palmitate, improve its preparation efficiency, and at the same time have the function of removing alcohol, thereby improving product quality and purity, and reducing production costs.

Description

Technical field [0001] The invention relates to the field of packaging equipment, in particular to a preparation device of isooctyl palmitate with the effect of removing alcohol. Background technique [0002] Isooctyl palmitate, good permeability, antiperspirant effect, strong affinity with the skin, is a dry breathable oil, widely used in skin care products and cosmetics, is an excellent skin softener, its performance is stable, not easy to oxidize or produce The peculiar smell can make the skin soft and smooth without greasy feeling. It has good permeability and is often used in various skin creams. [0003] The traditional preparation method of isooctyl palmitate uses palmitic acid and isooctyl alcohol to carry out the esterification reaction product, but in the esterification reaction process, there is isooctyl alcohol remaining in the product, and isooctyl alcohol will cause the product to emit peculiar smell. The method of octanol is distillation, but the distillation method...

Claims

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Application Information

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IPC IPC(8): C07C67/08C07C67/48C07C67/54C07C69/24C07C29/74C07C29/80C07C31/125
CPCC07C67/08C07C29/74C07C29/80C07C67/48C07C67/54C07C69/24C07C31/125
Inventor 刘海波江海
Owner 枝江市楚怡化工有限公司