Pyrene derivative and synthetic method and application thereof
A technology of pyrene derivatives and reactions, applied in the detection field of copper ions, achieving the effect of simple synthesis steps, high yield and low detection limit
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[0023] Pyrene derivative P is a compound represented by Formula 1.
[0024] Preparation of pyrene derivative P: put 1mM ethyl o-hydroxybenzoate and hydrazine hydrate of 5 times molar amount in 30mL of absolute ethanol, reflux at 75-80°C for 4h, cool to room temperature, filter the precipitated solid, and pass the solid through After washing with absolute ethanol and drying, the resulting intermediate compound was directly used in the next step. 1mM intermediate in absolute ethanol, react with pyrene formaldehyde at a molar ratio of 1:1 at 75-80°C for 4 hours, after cooling, filter the precipitated solid with suction, wash with a large amount of water and absolute ethanol in turn, and dry to obtain a light yellow solid Pure product P, productive rate 85% (see figure 1 and figure 2 ).
[0025] Depend on figure 1 and 2 The molecular ion peak and the chemical shift of H can be seen in the middle to know the generation of pyrene derivative P.
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