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Amino acid shampoo composition and preparation method thereof

A composition and shampoo technology, applied in the field of low-cost thickening cleaning compositions, can solve the problems of difficulty in thickening, defoaming, and high cost, and achieve the effects of improving stability, reducing costs, and reducing working hours

Active Publication Date: 2021-01-15
GUANGZHOU KENENG COSMETICS RES CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Mainly due to the high cost of amino acid surface activity, the cheapest one costs more than 12 yuan / kg, and the expensive one is even nearly 100 yuan / kg
The foam height of amino acid surfactants is lower than that of commonly used sulfate surfactants, and the biggest problem with amino acid surfactants is that it is difficult to thicken. Conventional shampoo thickeners often cannot thicken effectively, or there will be Obvious defoaming, such as cocamide MEA, PEG-150 distearate, PEG-120 methyl glucose dioleate, acrylic acid (ester) copolymer, the thickening effect is very limited
In recent years, in order to solve the problem of difficult thickening in the corresponding market, such as PEG-120 methyl glucose triisostearate, PEG-150 pentaerythritol tetrastearate, acrylic acid (ester) / C10- 30 alkanol acrylate crosslinked polymers and other products that effectively thicken amino acid surface activity, but they have various problems such as high cost, defoaming, need for heating, and complicated process
[0003] In addition, in the prior art, only amphoteric surfactants are used to thicken amino acid surfactants. For example, Lu Haiwei studied the compounding of amino acid / amphophoteric surfactants, and found that cocamide betaine is effective for different amino acid surfactants. The surface activity and thickening effect are different. It has a thickening effect on sodium lauryl sarcosinate and sodium cocoyl alaninate, but it has a thickening effect on sodium lauryl glutamate, sodium cocoyl methyl taurate and coconut oil. Sodium oleoyl glycinate has no effective thickening effect (Lu Haiwei. Amino acid / amphoteric surfactant compound thickening system and rheological research [D]. East China University of Science and Technology, 2013.)

Method used

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  • Amino acid shampoo composition and preparation method thereof
  • Amino acid shampoo composition and preparation method thereof
  • Amino acid shampoo composition and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0055] Example 1 verifies the synergistic thickening of amino acid surfactants of different weight percentages of betaine surfactants and different weight percentages of sodium α-olefin sulfonate

[0056] In order to verify the effects of different weight percentage components and different amino acid types on foaming and thickening effects, the inventors designed the following three schemes. Wherein from scheme 1 to scheme 3, the percentage by weight of betaine surfactant and sodium α olefin sulfonate increases gradually, for each scheme, also designed the different kinds of amino acid surfactant on foaming and thickening effect etc. Influence. See below for specific plans:

[0057]

[0058] Table 1. Physicochemical properties of combinations prepared by different amino acid surfactants in scheme 1

[0059]

[0060]

[0061] Table 2. Physicochemical properties of combinations prepared by different amino acid surfactants in scheme 2

[0062]

[0063] NOTE: Sodiu...

Embodiment 2

[0074] Example 2 Verify the effect of different amounts of amphoteric betaine surface activity and the ratio of sodium α-olefin sulfonate on the thickening effect of amino acid surface activity, and the influence of pH on the viscosity of the system

[0075] Table 4.

[0076]

[0077]

[0078] The thickening ability of composition changes with the ratio of sodium α-olefin sulfonate and amino acid surface activity, and the change of viscosity occurs. Through experiments and experience of the inventor, when sodium α-olefin sulfonate and betaine surface activity The weight ratio of the agent is 0.8-1.2:1.8-2.4, and the formula has a higher viscosity at this time. In addition, it can be seen from the above table that the change of pH will affect the viscosity. Different amino acids have different main surface activities, and their highest viscosity points are different. The highest viscosity of sodium sarcosinate is around 6.0, and a parabola appears with different pH, and ...

Embodiment 4

[0080] Preparation and testing of some amino acid shampoos of embodiment 4

[0081] Prepare some shampoos according to the formulas of Table 5, Table 6, and Table 7.

[0082] Preparation method: S1: Add appropriate amount of water at low temperature, add cationic conditioner, and disperse well;

[0083] S2: Add betaine surfactant, stir for 1 minute, add amino acid surfactant, and then add sodium α-olefin sulfonate;

[0084] S3: Add the rest of the raw materials in the formula, stir until uniform and then discharge.

[0085] Table 5. Sodium Cocamide Taurate Shampoo

[0086]

[0087]

[0088] Table 6. Monosodium glutamate shampoo

[0089]

[0090] Table 7. Sodium Sarcosinate Shampoo

[0091]

[0092] Table 8 Properties of Different Amino Acid Shampoos

[0093] Viscosity mPA·s Foam height mm Effect Shampoos in Table 5 15000 150 soft and smooth Shampoos in Table 6 4500 140 Lightweight, good wet combing effect Shampoos in Table...

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Abstract

The invention relates to a cleaning composition and a preparation method thereof, belonging to the technical field of cosmetics. The composition comprises, by weight, 15 to 50% of an amino acid surfactant, 10 to 30% of sodium alpha-olefinsulfonate and 15 to 50% of a betaine surfactant. The composition provided by the invention effectively overcomes the problem of difficulty in thickening of conventional products with the amino acid surfactant as a main surfactant, realizes thickening mainly through complex formulation of an anionic surfactant and an ampholytic surfactant, and constructs a micelle from sodium C14-16 olefin sulfonate and the betaine surfactant in a proper ratio so as to realize system thickening; other thickening agent is not needed; cold preparation can be realized, so production time is substantially reduced; and the prepared cleaning composition has abundant and fine foam, is greatly saved in cost and overcomes the problem of difficulty in thickening of the amino acidsurfactant and the problem of low foam of the amino acid surfactant.

Description

technical field [0001] The invention belongs to the field of cosmetics and relates to a low-cost thickened cleaning composition. Background technique [0002] Amino acid shampoos generally have problems of high cost and low foam in the market. The main reason is that the cost of amino acid surface activity is high, the cheapest is more than 12 yuan / kg, and the expensive one is even nearly 100 yuan / kg. The foam height of amino acid surfactants is lower than that of commonly used sulfate surfactants, and the biggest problem with amino acid surfactants is that it is difficult to thicken. Conventional shampoo thickeners often cannot thicken effectively, or there will be Obvious defoaming, such as cocamide MEA, PEG-150 distearate, PEG-120 methyl glucose dioleate, acrylic acid (ester) copolymer, the thickening effect is very limited. In recent years, in order to solve the problem of difficult thickening in the corresponding market, such as PEG-120 methyl glucose triisostearate, ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K8/46A61K8/44A61K8/04A61Q5/02A61Q19/10
CPCA61K8/046A61K8/44A61K8/442A61K8/447A61K8/466A61K2800/48A61K2800/592A61Q5/02A61Q19/10
Inventor 张伟雄阮景波周晓璐金淑芳张伟杰张楚标
Owner GUANGZHOU KENENG COSMETICS RES CO LTD
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