Composite crease-resistant and pilling-resistant finishing agent and preparation method thereof

A treatment agent and anti-pilling technology, which is applied in fiber treatment, wear-resistant fibers, textiles and papermaking, etc. It can solve problems such as easy pilling, strong damage to fabrics, stiff and rough hand feeling, etc., to improve wrinkle resistance and reduce slippage. Move, improve the effect of pilling resistance

Active Publication Date: 2018-04-13
广州先盈生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this kind of finishing agent also has certain disadvantages, such as high price, easy to pollute the environment, yellowing of the fabric, and serious damage to the strength of the fabric.
[0006] The fabric treated with anti-wrinkle finishing agent endows it with elasticity and resilience, but the handle becomes stiff and r

Method used

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  • Composite crease-resistant and pilling-resistant finishing agent and preparation method thereof
  • Composite crease-resistant and pilling-resistant finishing agent and preparation method thereof
  • Composite crease-resistant and pilling-resistant finishing agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A composite anti-wrinkle and anti-fluff treatment agent, comprising the following components in mass percentage, ethyl hydrogen-containing silicone oil 10%, sorbitan fatty acid ester S-20 2%, secondary alcohol polyoxyethylene ether S-50 2%, Maleic anhydride 10%, water-soluble azo initiator V-50 0.2%, viscosity 1000cPs polydimethylsiloxane 12%, polyglycidyl ether 10%, polyoxyethylene sorbitan fatty acid ester T-20 4%, diethylene glycol monobutyl ether 1%, polyvinyl alcohol 2%, and the rest is deionized water.

[0028] Above-mentioned polyvinyl alcohol selects the polyvinyl alcohol of medium viscosity that molecular weight is 110000 for use.

[0029] The preparation method of the composite anti-wrinkle and anti-fluff treatment agent comprises the following steps: 1) preparing each component according to the above-mentioned mass percentage for future use.

[0030] Preparation of component A: Add sorbitan fatty acid ester S-20, secondary alcohol polyoxyethylene ether S-50 ...

Embodiment 2

[0042] A composite anti-wrinkle and anti-fluff treatment agent, comprising the following components in mass percentage, ethyl hydrogen-containing silicone oil 12%, sorbitan fatty acid ester S-40 3%, secondary alcohol polyoxyethylene ether S-70 2.5%, Cyclopentetate anhydride 12%, water-soluble azo initiator VA-044 0.3%, viscosity 2000cPs polydimethylsiloxane 10%, polyglycidyl ether 8%, polyoxyethylene sorbitan fatty acid ester T -40 3%, diethylene glycol monobutyl ether 0.8%, polyvinyl alcohol 1.5%, and the rest is deionized water.

[0043] Above-mentioned polyvinyl alcohol selects the polyvinyl alcohol of medium viscosity that molecular weight is 120000 for use.

[0044] The preparation method of the composite anti-wrinkle and anti-fluff treatment agent comprises the following steps: 1) preparing each component according to the above-mentioned mass percentage for future use.

[0045] Preparation of component A: Add sorbitan fatty acid ester S-40, secondary alcohol polyoxyethy...

Embodiment 3

[0055] A compound anti-wrinkle and anti-pilling treatment agent, comprising the following components in mass percentage, 15% of hydroxyl hydrogen-containing silicone oil, 4% of sorbitan fatty acid ester S-60, 3% of secondary alcohol polyoxyethylene ether S-70, cyclo Glutaric anhydride 15%, water-soluble azo initiator VA-044 0.3%, viscosity 4000cPs polydimethylsiloxane 10%, polyglycidyl ether 7%, polyoxyethylene sorbitan fatty acid ester T- 60 3%, diethylene glycol monobutyl ether 0.7%, polyvinyl alcohol 1%, and the rest is deionized water.

[0056] Above-mentioned polyvinyl alcohol selects the polyvinyl alcohol of medium viscosity that molecular weight is 130000 for use.

[0057] The preparation method of the composite anti-wrinkle and anti-fluff treatment agent comprises the following steps: 1) preparing each component according to the above-mentioned mass percentage for future use.

[0058] Preparation of component A: Add sorbitan fatty acid ester S-60, secondary alcohol po...

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Abstract

The invention discloses a composite crease-resistant and pilling-resistant finishing agent which comprises, in weight percent, 10-20% of hydrogen-containing silicone oil, 2-5% of sorbitan fatty acid ester, 2-4% of secondary alcohol ethoxylate, 10-20% of acid anhydride, 0.2-0.5% of initiating agents, 6-12% of polydimethylsiloxane, 5-10% of polyglycidyl ether, 2-4% of polyoxyethylene sorbitan fattyacid ester, 0.5-1% of diethylene glycol monobutyl ether, 0.5-2% of polyvinyl alcohol and the rest deionized water. Active Si-H bonds in the hydrogen-containing silicone oil and high-electron-withdrawing acid anhydride are synthesized into copolymers through free-radical addition mechanisms under the action of the initiating agents, esterification reaction among the copolymers and hydroxyl on fibermacromolecules can be achieved, crease-resist effects can be acquired, and softness effects can also be acquired. The copolymers and pilling-resistant finishing liquid are synergistically compounded,a soft and toughened thin film is formed on the surfaces of fibers, sliding of the fibers is reduced, so that fiber ends are adhered onto yarns, plush is not easily formed by friction, the pilling resistance of fabrics is effectively improved, and the composite crease-resistant and pilling-resistant finishing agent is prepared.

Description

technical field [0001] The invention relates to the technical field of textile auxiliaries, in particular to a composite anti-wrinkle and anti-fluff treatment agent and a preparation method thereof. Background technique [0002] During the wearing process of the fabric, due to the factors of the fabric itself and various external forces and external frictions, it is easy to produce wrinkles and pilling before obvious damage occurs, which affects the appearance and wearing performance. Therefore, it is necessary to carry out anti-wrinkle and anti-pilling finishing on the fabric to improve the wearing comfort and quality of the fabric. [0003] The anti-wrinkle and anti-pilling treatment currently on the market is basically completed in two steps, one is anti-pilling finishing, and the other is anti-wrinkle finishing. There are many kinds of additives used, the process is complicated, and the cost is high. [0004] In addition, the breaking strength, elongation at break, and...

Claims

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Application Information

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IPC IPC(8): D06M15/643D06M15/53D06M15/333D06M101/06
CPCD06M15/333D06M15/53D06M15/643D06M15/6433D06M2101/06D06M2200/20D06M2200/35
Inventor 姚宾燕章数龙陈妃状李钢
Owner 广州先盈生物科技有限公司
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