Essential oil and preparation method thereof
A technology for essential oil and argyi leaf essential oil, which is applied in the directions of essential oil/spice, fat production, deodorization, etc., can solve the problems of complex extraction method, poor effect and high cost, and achieves high production efficiency, avoiding damaging effects and high extraction efficiency. Effect
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[0022] The preparation method of the Artemisia argyi essential oil is to dry the Artemisia argyi leaves until the moisture content is lower than 1%, and then crush them with a mechanical crusher until the particle size of the material is 0.1-0.2mm, then pour the powder into a sealed container, and pass in CO 2 , the mass ratio of powder to carbon dioxide is 1:2-3, the temperature is cooled to minus 50°C to minus 40°C, and the pressure is 6-7 atmospheres, so that CO 2 becomes a liquid, the powder is fully infiltrated into the liquid CO 2 After 1-2 hours, release the pressure suddenly to normal pressure, collect the powder, add potassium hydrogen phosphate solution to mix, and adjust the pH of the solution to 4-5, then add cellulase, mix thoroughly, and maintain the temperature at 35- 40°C, after reacting for 4-6 hours, add n-pentane, mix and stir for 15-20min at a temperature of 20-30°C and a pressure of 2-3 atmospheres, and then carry out standing and layering, and the obtaine...
Embodiment 1
[0027] An essential oil, which is composed of 70% mint essential oil, 10% mugwort essential oil, 16% borneol solution and 4% medical alcohol with a volume ratio of 15%.
[0028] Add mint essential oil, mugwort essential oil, borneol solution and medical alcohol into the blender, stir evenly at high speed, and obtain it through precision filtration. The preparation method of the mint essential oil is to dry the mint until the moisture content is lower than 1%. Then use a mechanical crusher to crush the material to a particle size of 0.3mm, then pour the powder into a sealed container, and pass in CO 2 , the mass ratio of powder to carbon dioxide is 1:2.4, the temperature is cooled to minus 45°C, and the pressure is 6.6 atmospheres, so that CO 2 becomes a liquid, the powder is fully infiltrated into the liquid CO 2 After 1.6 hours, release the pressure suddenly to normal pressure, collect the powder, add potassium hydrogen phosphate solution to mix, and adjust the pH of the sol...
Embodiment 2
[0034] The essential oil is composed of 69.5% mint essential oil, 11% mugwort essential oil, 14% borneol solution and 5.5% medicinal alcohol with a volume ratio of 10-20%.
[0035] Add mint essential oil, mugwort essential oil, borneol solution and medical alcohol into the blender, stir evenly at high speed, and obtain it through precision filtration. The preparation method of the mint essential oil is to dry the mint until the moisture content is lower than 1%. Then use a mechanical crusher to crush the material to a particle size of 0.35mm, then pour the powder into a sealed container, and pass in CO 2 , the mass ratio of powder to carbon dioxide is 1:2.4, the temperature is cooled to minus 46°C, and the pressure is 6.5 atmospheres, so that CO 2 becomes a liquid, the powder is fully infiltrated into the liquid CO 2 After 1.7 hours, release the pressure suddenly to normal pressure, collect the powder, add potassium hydrogen phosphate solution to mix, and adjust the pH of the...
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