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Flame-retardant nano composite material and preparation method thereof

A nano-composite material and nano flame retardant technology are applied in the field of flame-retardant nano-composite materials and their preparation, which can solve the problems of affecting the mechanical properties of composite materials, adding a large amount of flame-retardant additives, and a large amount of toxic fumes, so as to achieve enhanced smoke suppression. Good effect, good flame retardant effect, good anti-melting effect

Inactive Publication Date: 2018-04-20
XIHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Aiming at the above-mentioned deficiencies in the prior art, the present invention provides a flame-retardant nanocomposite material and its preparation method, which can effectively solve the problem that the large amount of flame-retardant additives used in the prior art will affect the mechanical properties of the composite material, and at the same time After the composite material is burned, a large amount of toxic smoke will be produced, the flame retardant effect is poor, and the environment is not friendly.

Method used

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  • Flame-retardant nano composite material and preparation method thereof
  • Flame-retardant nano composite material and preparation method thereof

Examples

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Effect test

Embodiment 1

[0027] A flame-retardant nano-composite material, comprising the following components by weight: 80 parts of polypropylene resin, 1 part of composite nano-flame retardant, 5 parts of nano-talc powder, 0.5 parts of flame-retardant synergist, anti-dripping agent 0.1 part, 1 part of compatibilizer, 0.1 part of antioxidant and 0.5 part of reinforcing agent;

[0028] The composite nano-flame retardant includes the following components by weight: 10 parts of modified nano-montmorillonite, 8 parts of nano-aluminum hydroxide, 2 parts of nano-aluminum tripolyphosphate and 1 part of nano-magnesium hydroxide.

[0029] The modified nano-montmorillonite is prepared by the following method: add montmorillonite to 80°C water, disperse ultrasonically for 1 hour to obtain a montmorillonite dispersion with a concentration of 10wt%, then add an intercalation agent and a protonating agent to control the temperature At 80°C, continue ultrasonic dispersion for 1 hour, then filter to obtain the firs...

Embodiment 2

[0040] A flame-retardant nano-composite material, comprising the following components by weight: 100 parts of polypropylene resin, 4 parts of composite nano-flame retardant, 15 parts of nano-talc powder, 1.5 parts of flame-retardant synergist, anti-dripping agent 0.5 parts, 4 parts of compatibilizer, 0.5 parts of antioxidant and 1.5 parts of reinforcing agent;

[0041] The composite nano-flame retardant includes the following components by weight: 20 parts of modified nano-montmorillonite, 15 parts of nano-aluminum hydroxide, 6 parts of nano-aluminum tripolyphosphate and 5 parts of nano-magnesium hydroxide.

[0042] The modified nano-montmorillonite is prepared by the following method: add montmorillonite to 80°C water, disperse ultrasonically for 1 hour to obtain a montmorillonite dispersion with a concentration of 10wt%, then add an intercalation agent and a protonating agent to control the temperature At 80°C, continue ultrasonic dispersion for 1 hour, then filter to obtain...

Embodiment 3

[0053] A flame-retardant nanocomposite material, comprising the following components by weight: 85 parts of polypropylene resin, 2 parts of composite nano-flame retardant, 8 parts of nano-talc powder, 0.8 parts of flame-retardant synergist, anti-dripping agent 0.2 parts, 2 parts of compatibilizer, 0.2 parts of antioxidant and 0.8 parts of strengthening agent;

[0054] The composite nano-flame retardant includes the following components by weight: 13 parts of modified nano-montmorillonite, 10 parts of nano-aluminum hydroxide, 3 parts of nano-aluminum tripolyphosphate and 2 parts of nano-magnesium hydroxide.

[0055] The modified nano-montmorillonite was prepared by the following method: adding montmorillonite to 80°C water and ultrasonically dispersing it for 1 hour to obtain a montmorillonite dispersion with a concentration of 6 wt%, and then adding an intercalation agent and a protonating agent to control the temperature At 80°C, continue ultrasonic dispersion for 1 hour, the...

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Abstract

The invention discloses a flame-retardant nano composite material and a preparation method thereof. The flame-retardant nano composite material comprises the following components in parts by weight: 80-100 parts of polypropylene resin, 1-4 parts of a compounded nano flame retardant, 5-15 parts of nano talcum powder, 0.5-1.5 parts of a flame-retardant synergist, 0.1-0.5 part of anti-dripping agent,1-4 parts of a compatilizer, 0.1-0.5 part of an antioxidant and 0.5-1.5 parts of a reinforcing agent. The composite material prepared by combining specific components has the advantages of good mechanical property, good flame-retardant effect, less smoke generated during combustion, good anti-dripping effect, no harm to human body and no environmental pollution; meanwhile, the preparation processis simple and convenient, the cost is low, and the composite material is suitable for industrial production.

Description

technical field [0001] The invention belongs to the technical field of flame-retardant nanocomposite materials, and in particular relates to a flame-retardant nanocomposite material and a preparation method thereof. Background technique [0002] Nanocomposite materials are a new field that develops very rapidly in material science in recent years. In general, it refers to composite materials with at least one dimension of the dispersed phase smaller than 100 nm. The special function of nanocomposites mainly comes from the small size effect of particles and numerous interfacial recombination effects. As long as a small amount of nanoparticles is added to the polymer by melt mixing or in situ polymerization, it can greatly improve the polymerization. The mechanical properties, barrier properties and flame retardant properties of the material can be obtained, and much higher heat resistance, dimensional stability and electrical conductivity can be obtained than conventional fi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/12C08L27/18C08K13/06C08K9/02C08K9/04C08K7/24C08K3/34C08K3/22C08K3/32B29B9/06B29C47/92B29C48/92
CPCB29B9/06B29C48/92B29C2948/92704C08K2003/2224C08K2003/2227C08K2003/2255C08K2003/327C08K2201/003C08K2201/011C08L23/12C08L2201/02C08L27/18C08K13/06C08K9/02C08K9/04C08K3/346C08K7/24C08K3/34C08K3/22C08K3/32
Inventor 陈宝书赵天宝李正秋廖力
Owner XIHUA UNIV
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