Sustained-release gel composition containing mesoporous silicon
A slow-release gel and mesoporous silicon technology, which is applied in separation methods, dispersed particle separation, chemical instruments and methods, etc., can solve problems such as pollution, harm to human adolescents, and difficulty in eliminating volatile organic compounds, etc., and is beneficial to Adsorption, the effect of improving the stability of hydrogen bond adsorption
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[0028] Preparation of bismuth vanadate
[0029] Dissolve 0.0015 mol of sodium vanadate and 0.006 mol of bismuth nitrate in deionized water respectively, drop the sodium vanadate solution into the bismuth nitrate solution drop by drop, stir for 30 minutes, let it stand for 5 hours, and put it in a constant temperature drying box After reacting at 160 degrees Celsius for 12 hours, after cooling to room temperature, continue to keep stirring and add 0.01 mol of hydrogen peroxide, filter with suction, wash and dry to obtain bismuth vanadate powder.
[0030] At room temperature, 8 parts by weight of tantalum pentachloride were dissolved in 100 parts by weight of absolute ethanol to obtain a tantalum pentachloride ethanol solution, which was left to stand for 15 minutes; 15 parts by weight of bismuth vanadate, 0.08 parts by weight of sulfurous acid Add sodium hydrogen to seal the HDI into the tantalum pentachloride ethanol solution, and combine evenly to obtain the first mixed solut...
Embodiment 1
[0032] In a container, dissolve 5 parts by weight of polyacrylic acid X1 and 0.8 parts by weight of polyisobutylene succinimide in 100 parts by weight of water; add 0.08 parts by weight of mesoporous silicon (Shanghai carboxyphenanthrene, MSNs-90) container, and heated up to 55 degrees Celsius, and kept for 24 hours; cooled to normal temperature, added 2 parts by weight of imidazolidinone and 0.04 parts by weight of nano-modified tantalum oxide photocatalytic oxidant, mixed evenly, adjusted the pH value to 7, and obtained slow release gel.
Embodiment 2
[0034] In a container, dissolve 2 parts by weight of polyacrylic acid X2 and 0.6 parts by weight of polyisobutylene succinimide in 100 parts by weight of water; add 0.05 parts by weight of mesoporous silicon (Shanghai carboxyphenanthrene, MSNs-90) In the container, heat up to 55 degrees Celsius and keep for 24 hours; cool to normal temperature, add 2 parts by weight of imidazolidinone and 0.05 parts by weight of nano-modified tantalum oxide photocatalytic oxidant, mix well, adjust the pH value to 7, and obtain slow release gel.
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