Neodymium iron boron magnet permeated by heavy rare earth and method for permeating heavy rate earth on surface of neodymium iron boron magnet
A technology of neodymium iron boron and heavy rare earth, applied in the field of magnet preparation, can solve the problems of uneven thickness of heavy rare earth, poor consistency of magnetic properties of products, heavy rare earth layer easy to fall off, etc.
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[0067] The present invention also provides a method for preparing an NdFeB magnet as described in any one of the above technical solutions, that is, a method for infiltrating heavy rare earth on the surface of an NdFeB magnet, comprising the following steps:
[0068] 1) Under the condition of the working gas, the metal raw material and the NdFeB magnet blank are subjected to the first vapor deposition to obtain the NdFeB magnet blank with a metal layer on the surface;
[0069] 2) Under the condition of working gas, the heavy rare earth or heavy rare earth alloy raw material, and the NdFeB magnet blank with a metal layer on the surface obtained in the above steps, after the second vapor deposition, obtain a heavy rare earth layer on the surface Or NdFeB magnet blank with heavy rare earth alloy layer;
[0070]3) Under vacuum conditions, the NdFeB magnet blank with the heavy rare earth layer or heavy rare earth alloy layer on the surface obtained in the above steps is heat-treate...
Embodiment 1
[0110] The 1.8mm thick 50M magnet is subjected to grain boundary infiltration heat treatment after magnetron sputtering aluminum and terbium aluminum alloy plating
[0111] Take a 50M magnet with a specification of 50-20-1.8mm, degrease it with a degreasing solution, clean it with dilute nitric acid and dry it, put it into a sputtering furnace, and evacuate it to 4.0*10 -3 Pa, and turn on the heating to keep the furnace at 200°C. Fill with high-purity argon gas, turn on the power to perform secondary ion cleaning on the magnetic steel and activate the surface for 5 minutes. After activation, turn on the intermediate frequency power supply to sputter aluminum onto the surface of the substrate. The thickness of the aluminum coating is 2 μm. Turn on the power supply to sputter terbium aluminum alloy onto the surface of the magnet. The intermediate frequency power supply is set to 10A, the voltage is 350V, and the sputtering time is 1.5h. A terbium aluminum alloy coating with a t...
Embodiment 2
[0117] The 1.8mm thick 50M magnet is sequentially coated with aluminum and terbium composite coatings by magnetron sputtering, alloyed and then subjected to grain boundary penetration heat treatment
[0118] Take a 50M magnet with a specification of 50-20-1.8mm, degrease it with a degreasing solution, clean it with dilute nitric acid and dry it, put it into a sputtering furnace, and evacuate it to 4.0*10 -3 Pa, and turn on the heating to keep the furnace at 200°C. Fill with high-purity argon gas, turn on the power to perform secondary ion cleaning on the magnetic steel and activate the surface for 5 minutes. After activation, turn on the intermediate frequency power supply to sputter aluminum metal onto the surface of the magnet. The intermediate frequency power supply is set to 10A, the voltage is 350V, and the sputtering time is 0.5h to obtain an aluminum coating with a thickness of 1 μm. Turn on the intermediate frequency power supply to sputter terbium onto the surface of ...
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Abstract
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