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Neodymium iron boron magnet permeated by heavy rare earth and method for permeating heavy rate earth on surface of neodymium iron boron magnet

A technology of neodymium iron boron and heavy rare earth, applied in the field of magnet preparation, can solve the problems of uneven thickness of heavy rare earth, poor consistency of magnetic properties of products, heavy rare earth layer easy to fall off, etc.

Inactive Publication Date: 2018-05-15
金力永磁(宁波)科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are still problems such as uneven thickness of heavy rare earth, poor bonding force, easy fall off of heavy rare earth layer, resulting in poor consistency of magnetic properties of the product

Method used

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  • Neodymium iron boron magnet permeated by heavy rare earth and method for permeating heavy rate earth on surface of neodymium iron boron magnet

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preparation example Construction

[0067] The present invention also provides a method for preparing an NdFeB magnet as described in any one of the above technical solutions, that is, a method for infiltrating heavy rare earth on the surface of an NdFeB magnet, comprising the following steps:

[0068] 1) Under the condition of the working gas, the metal raw material and the NdFeB magnet blank are subjected to the first vapor deposition to obtain the NdFeB magnet blank with a metal layer on the surface;

[0069] 2) Under the condition of working gas, the heavy rare earth or heavy rare earth alloy raw material, and the NdFeB magnet blank with a metal layer on the surface obtained in the above steps, after the second vapor deposition, obtain a heavy rare earth layer on the surface Or NdFeB magnet blank with heavy rare earth alloy layer;

[0070]3) Under vacuum conditions, the NdFeB magnet blank with the heavy rare earth layer or heavy rare earth alloy layer on the surface obtained in the above steps is heat-treate...

Embodiment 1

[0110] The 1.8mm thick 50M magnet is subjected to grain boundary infiltration heat treatment after magnetron sputtering aluminum and terbium aluminum alloy plating

[0111] Take a 50M magnet with a specification of 50-20-1.8mm, degrease it with a degreasing solution, clean it with dilute nitric acid and dry it, put it into a sputtering furnace, and evacuate it to 4.0*10 -3 Pa, and turn on the heating to keep the furnace at 200°C. Fill with high-purity argon gas, turn on the power to perform secondary ion cleaning on the magnetic steel and activate the surface for 5 minutes. After activation, turn on the intermediate frequency power supply to sputter aluminum onto the surface of the substrate. The thickness of the aluminum coating is 2 μm. Turn on the power supply to sputter terbium aluminum alloy onto the surface of the magnet. The intermediate frequency power supply is set to 10A, the voltage is 350V, and the sputtering time is 1.5h. A terbium aluminum alloy coating with a t...

Embodiment 2

[0117] The 1.8mm thick 50M magnet is sequentially coated with aluminum and terbium composite coatings by magnetron sputtering, alloyed and then subjected to grain boundary penetration heat treatment

[0118] Take a 50M magnet with a specification of 50-20-1.8mm, degrease it with a degreasing solution, clean it with dilute nitric acid and dry it, put it into a sputtering furnace, and evacuate it to 4.0*10 -3 Pa, and turn on the heating to keep the furnace at 200°C. Fill with high-purity argon gas, turn on the power to perform secondary ion cleaning on the magnetic steel and activate the surface for 5 minutes. After activation, turn on the intermediate frequency power supply to sputter aluminum metal onto the surface of the magnet. The intermediate frequency power supply is set to 10A, the voltage is 350V, and the sputtering time is 0.5h to obtain an aluminum coating with a thickness of 1 μm. Turn on the intermediate frequency power supply to sputter terbium onto the surface of ...

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Abstract

The invention provides a neodymium iron boron magnet permeated by heavy rare earth. The neodymium iron boron magnet is obtained by a neodymium iron boron magnet blank of which the surface is compounded by a plating through thermal treatment; the neodymium iron boron magnet blank of which the surface is compounded by the plating comprises the neodymium iron boron magnet, a metal layer compounded onthe surface of the neodymium iron boron magnet and a heavy rare earth layer or a heavy rare earth alloy layer compounded on the surface of the metal layer again. Firstly, the uniform and dense metalplating is formed on the surface of a neodymium iron boron substrate, so that the surface of the substrate is flat and dense, afterwards, a heavy rare earth plating or a heavy rare earth alloy platingis formed on the surface of the metal plating, then metal and heavy rare earth or heavy rare earth alloy is permeated inside the neodymium iron boron substrate in the mode of thermal treatment, and the purpose of improving the coercivity of neodymium iron boron is achieved. The neodymium iron boron magnet blank rare earth layer is high in binding force, the thickness is uniform and consistent, then the neodymium iron boron magnet blank rare earth layer is permeated inside the substrate through high temperature, the magnet performance can be greatly improved, and the magnet performance consistency is well kept; meanwhile, the utilization rate of heavy rare earth can be increased, and the cost is saved.

Description

technical field [0001] The invention belongs to the technical field of magnet preparation, and relates to an NdFeB magnet and a preparation method thereof, in particular to an NdFeB magnet infiltrated with heavy rare earth and a method for infiltrating the heavy rare earth on the surface of the NdFeB magnet. Background technique [0002] NdFeB magnets are rare earth permanent magnets made by sintering materials containing rare earth neodymium, iron and boron. At present, the industry often adopts the sintering method to make NdFeB permanent magnet materials. For example, Wang Wei et al. disclosed the use of sintering method to manufacture NdFeB permanent magnets in "The Influence of Key Process Parameters and Alloy Elements on the Magnetic and Mechanical Properties of Sintered NdFeB". The technological process of materials generally includes the steps of batching, smelting, ingot crushing, powder making, hydrogen crushing, jet mill ultrafine powder, powder orientation pressi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F1/057H01F41/02
CPCH01F1/057H01F41/0293
Inventor 毛华云梁礼渭
Owner 金力永磁(宁波)科技有限公司