Method for preparing novel magnesium-based composite by ultrasonic assisted mechanical mixing
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A technology of auxiliary machinery and composite materials, which is applied in the field of magnesium alloys, can solve the problems of carbon nanotube surface inactivity, weak bonding, and fragile interface, and achieve the effects of increasing stirring speed, preventing oxidative combustion, and reducing pores and inclusions
Inactive Publication Date: 2018-05-29
HARBIN UNIV OF SCI & TECH
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[0006] As we all know, the main obstacle restricting the application of carbon nanotube-reinforced composite materials is that it is difficult to uniformly disperse in the matrix material, because carbon nanotubes are easy to form larger agglomerations, the surface structure of carbon nanotubes is relatively complete, and there are fewer active groups, so in It is difficult to dissolve in various solvents. Because the surface of carbon nanotubes is not active, chemical reactions are not easy to occur, and the interface with the matrix alloy is relatively fragile and the combination is not firm.
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[0018] The present invention is further illustrated in conjunction with specific examples of implementation as follows, the Mg-Al-Si-Sb-Ca alloy is composed of the following components in weight percentage: 8%Al, 2%Si, 0.75%Sb, 0.5%Ca, and the balance is magnesium , the added reinforcement is 1% carbon nanotubes.
[0019] Its preparation method is:
[0020] (1) Calculate and weigh the carbon nanotubes into the alcohol, add a certain amount of chemical dispersant, then use the stirrer to stir the carbon nanotube alcohol solution, and then put the carbon nanotube alcohol solution into the ultrasonic pool for ultrasonic Treat for 3 hours until a stable suspension of carbon nanotubes is obtained, add an appropriate amount of magnesium chips to the carbon nanotube alcohol solution, stir for 3 hours, and finally dry naturally in a fume hood.
[0021] (2) Clean the impurities on the melting tools such as graphite crucible, stirring paddle, ultrasonic tool rod, etc., and put them int...
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Abstract
The invention provides a method for preparing a carbon-nanotube strengthened magnesium-based composite. According to the method, carbon nanotubes are evenly distributed in a magnesium matrix through aseries of technical processes, and the strengthened magnesium-based composite is obtained; and an alloy is composed of, by weight percentage, 8% of Al, 2% of Si, 0.75% of Sb, 0.5% of Ca, 1% of the carbon nanotubes and the balance Mg, and the raw materials comprise a pure magnesium ingot, an aluminum ingot, an antimony ingot, an Mg-10Al-27Ca master alloy, an Al-50Si master alloy, magnesium chips and the carbon nanotubes. The method comprises the specific implementation and processing steps of (1), pre-dispersion of the carbon nanotubes, (2), alloy melting and semisolid mixing and (3), ultrasonic dispersion. By the adoption of the technology, the problem of the bad wettability of the matrix and the composite is solved, the defects of micropores, shrinkage porosity and the like in the compositing process are overcome effectively, the alloy structure is refined, and the mechanical performance is improved.
Description
technical field [0001] The invention belongs to the field of magnesium alloys, and in particular relates to a method for preparing novel magnesium-based composite materials by ultrasonic-assisted mechanical stirring. Background technique [0002] Since entering the 21st century, resources and the environment have become the primary issues of human sustainable development. Therefore, the current trend of world industrial development is to save energy, resources and green production. As the lightest metal material for engineering structures, magnesium alloy has many excellent unique properties, such as high specific strength, high specific modulus, good electrical and thermal conductivity, good damping and shock absorption and electromagnetic shielding performance, easy to process and form, good Magnesium alloys have been widely used in automobiles, communication equipment, aviation and other fields due to their advantages such as regeneration and reuse. Therefore, magnesium ...
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