MoS2-SnO2-carbon fiber composite material and preparation method thereof

A mos2-sno2-, composite material technology, applied in carbon fiber, fiber processing, textiles and papermaking, etc., can solve the problems of limited material properties and applications, high temperature environment, cumbersome preparation process, etc., to achieve accelerated carrier mobility, The effect of increasing the specific surface area and increasing the effective sites

Active Publication Date: 2018-06-19
NORTHWEST UNIV(CN)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The preparation process is relatively cumbersome, and the reaction requires a high-temperature environment. The most important thing is that there are safety hazards in the process; in addition, this method only prepares composite powder materials, which does not address the shortcomings of pure powder materials in photocatalysis. solution, which greatly limits the properties and applications of the material

Method used

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  • MoS2-SnO2-carbon fiber composite material and preparation method thereof
  • MoS2-SnO2-carbon fiber composite material and preparation method thereof
  • MoS2-SnO2-carbon fiber composite material and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0049] First, in this experiment, tin tetrachloride (SnCl 4 ·5H 2 O) and sodium hydroxide (NaOH) as reaction source materials to prepare SnO on a flexible substrate carbon cloth 2 . The specific operation process is as follows: use an electronic balance to weigh a certain amount of tin tetrachloride (SnCl 4 ·5H 2 O) and sodium hydroxide (NaOH), respectively configure 0.04mol / L tin tetrachloride solution and 0.56mol / L NaOH solution, and then slowly titrate the prepared NaOH solution into the tin tetrachloride solution to make it Mix well and finally form a stable and uniform precursor solution. Slowly pour the solution into a 50ml autoclave containing carbon cloth, place it in an oven, and react at 200°C for 16 hours. After the reaction is over, take out the carbon cloth and wash it with deionized water several times. Arrange the carbon to dry at 60℃ to obtain SnO 2 Coated carbon fiber composite material.

[0050] SnO 2 -The carbon fiber membrane material is washed several times ...

Embodiment 2

[0053] First, in this experiment, tin tetrachloride (SnCl 4 ·5H 2 O) and sodium hydroxide (NaOH) as reaction source materials to prepare SnO on a flexible substrate carbon cloth 2 . The specific operation process is as follows: use an electronic balance to weigh a certain amount of tin tetrachloride (SnCl 4 ·5H 2 O) and sodium hydroxide (NaOH), respectively configure 0.04mol / L tin tetrachloride solution and 0.56mol / L NaOH solution, and then slowly titrate the prepared NaOH solution into the tin tetrachloride solution to make it Mix well and finally form a stable and uniform precursor solution. Slowly pour the solution into a 50ml autoclave containing carbon cloth, place it in an oven, and react at 200°C for 16 hours. After the reaction is over, take out the carbon cloth and wash it with deionized water several times. Arrange the carbon to dry at 60℃ to obtain SnO 2 Coated carbon fiber composite material.

[0054] SnO 2 -The carbon fiber membrane material is washed several times ...

Embodiment 3

[0057] First, in this experiment, tin tetrachloride (SnCl 4 ·5H 2 O) and sodium hydroxide (NaOH) as reaction source materials to prepare SnO on a flexible substrate carbon cloth 2 . The specific operation process is as follows: use an electronic balance to weigh a certain amount of tin tetrachloride (SnCl 4 ·5H 2 O) and sodium hydroxide (NaOH), respectively configure 0.04mol / L tin tetrachloride solution and 0.56mol / L NaOH solution, and then slowly titrate the prepared NaOH solution into the tin tetrachloride solution to make it Mix well and finally form a stable and uniform precursor solution. Slowly pour the solution into a 50ml autoclave containing carbon cloth, place it in an oven, and react at 200°C for 16 hours. After the reaction is over, take out the carbon cloth and wash it with deionized water several times. Arrange the carbon to dry at 60℃ to obtain SnO 2 Coated carbon fiber composite material.

[0058] SnO 2 -The carbon fiber membrane material is washed several times ...

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Abstract

The invention discloses a MoS2-SnO2-carbon fiber composite material and a preparation method thereof, wherein the preparation method comprises that a SnO2 nanometer material grows on a carbon fiber material in a coated manner and a MoS2 nanometer material is subjected to secondary growth at the SnO2-carbon fiber by using a two-step hydrothermal method. According to the present invention, during the hydrothermal preparation, any templates and catalysts are not required, and the method has advantages of simple process, high yield and low cost, and is suitable for mass production; and the MoS2 nanometer material directly grows on the SnO2 coated carbon cloth, and the prepared nanometer composite material has the sandwich structure, has characteristics of tight coating and clear layering, andcan be used as photocatalysis materials, electrocatalysis materials, solar cell materials, flexible sensor materials, field emission materials and lithium ion battery negative electrode materials.

Description

Technical field [0001] The invention belongs to the field of nanomaterials and relates to a MoS 2 -SnO 2 -Carbon fiber composite material and its preparation method. Background technique [0002] With the continuous development of science and technology, electronic products and smart devices have begun to develop in the direction of miniaturization and light weight. Flexible electronic products have been applied to various areas of people's lives, such as wearable electronic devices and flexible display devices. Because of its good flexibility, carbon fiber is woven into carbon cloth, which can be widely used as a flexible electrode in various batteries, supercapacitors and other fields, and will be widely used in the next generation of nanoelectronic devices and other fields. [0003] MoS 2 Is an important semiconductor functional material, MoS 2 Nanomaterials are widely used as solar cells, sensitive devices, optoelectronic devices, lithium ion battery anode materials, photocatal...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/46D06M11/53D06M101/40
CPCD06M11/46D06M11/53D06M2101/40
Inventor 闫军锋贾仕隆许曼章贠江妮张志勇赵武翟春雪马晓龙张适师毓菲
Owner NORTHWEST UNIV(CN)
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