Application of graphene in preparing soybean protein fiber and fabric
A soybean protein fiber, soybean protein technology, applied in the direction of fiber chemical characteristics, single-component protein rayon, rayon manufacturing, etc., can solve the problem that soybean protein fiber has poor moisture resistance, soybean protein is not resistant to high temperature, and has not been widely promoted, etc. problems, to achieve the effect of increasing added value, excellent bulkiness, and excellent electrical conductivity
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[0035] Correspondingly, the present invention also provides a kind of preparation method of modified soybean protein fiber, comprising the following steps:
[0036] After oxidizing graphene with a sheet structure of less than 10 layers with an oxidant, it is dispersed in an organic solvent to form a graphene oxide mixture;
[0037] In the presence of hydroiodic acid, the graphene oxide mixed solution is mixed with the soybean protein spinning solution, and the modified soybean protein fiber is obtained by wet spinning.
[0038] The invention mainly studies the spinning technology of graphene in soybean protein fiber, and successfully prepares soybean protein fiber containing graphene, which has a good application prospect.
[0039] In the embodiment of the present invention, liquid graphene derivatives are first prepared: graphene→graphene oxide (GO)→polar solvent dispersion to obtain a graphene oxide mixture, namely liquid graphene oxide (referred to as liquid graphene).
[00...
Embodiment 1
[0071] (1) Liquid graphene derivatives: select graphene powder within 10 layers, purity>99%, layer thickness 0.7-1.2nm, metal content<10ppm, adjust pH=4 to oxidize with 1% owf potassium permanganate Monolayer graphene oxide is prepared, dispersed in 95% ethanol solvent, and adjusted according to the mass ratio of 1:1 to obtain graphene oxide mixed liquid (also called liquid graphene).
[0072] (2) Soybean protein fiber (containing graphene): 1% owf liquid graphene, 10% soy protein, 0.5% owf hydroiodic acid, 1% owf alginate, 0.8% owf sodium caseinate, 1.5% owf fruit The glue is mixed with the remaining amount of polyvinyl alcohol, degreased, separated, dried, adjusted to pH = 10, and wet-spun at a spinning speed of 25 m / min to obtain fibers.
[0073] Using conventional standard methods in this field, the obtained fibers were tested for strength, electrical conductivity and other indicators. The results show that the fineness of the obtained fiber is 1.2dtex, the length is 18mm...
Embodiment 2
[0082] (1) Liquid graphene derivatives: select graphene powder within 10 layers, purity>99%, layer thickness 0.7-1.2nm, metal content<10ppm, adjust pH=5 to oxidize with 3% owf potassium permanganate Monolayer graphene oxide is prepared, dispersed in 95% ethanol solvent, and adjusted according to the mass ratio of 1:1 to obtain liquid graphene.
[0083] (2) Soybean protein fiber (including graphene): 2% owf liquid graphene, 15% soy protein, 0.5% owf hydroiodic acid, 1.5% owf alginate, 0.8% owf sodium caseinate, 1% owf fruit The glue is mixed with the remaining amount of polyvinyl alcohol, degreased, separated, dried, adjusted to pH = 10, and wet-spun at a spinning speed of 55m / min to obtain fibers, and the ethanol polar solvent is recovered.
[0084] The resulting fiber fineness: 1.1dtex, length 29mm, specific gravity 1.03g / m 3 , fiber moisture regain 6%, breaking strength (dry): 4.1 (cN / dtex), breaking strength (wet): 2.9 (cN / dtex), breaking elongation (dry): 14%, breaking el...
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