A kind of engine lubricating oil antiwear agent and its preparation method and application
A technology of anti-wear agent and lubricating oil, which is applied in the field of lubricating oil, can solve the problem that friction reducer and anti-wear agent can not fully meet the performance of anti-friction and anti-wear, and achieve the effect of improving service life, reasonable compatibility and good compatibility
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Embodiment 1
[0043] The embodiment of the present invention provides a kind of preparation method of engine lubricating oil antiwear agent, comprises the following steps:
[0044] (1) Mix 3 parts of nano-copper oxide with 12 parts of octadecaborate polyoxyethylene ether and stir for 12 hours under the condition of 2500 r / min to prepare modified copper oxide.
[0045] (2) 15 parts of polyimide, 25 parts of polyphenylparaben (molecular weight of 70,000, particle size of 5um), 5 parts of soluble polytetrafluoroethylene ultrafine powder (50nm), 3 parts of anion Fluorocarbon surfactant, 10 parts of nonionic fluorocarbon surfactant, 10 parts of vinyl silicone oil (500CST), 20 parts of dimethyl silicone oil (500CST) and the modified copper oxide obtained in step (1) were heated at 32°C and 4000r / min under the condition of stirring for 30min to prepare the anti-wear agent.
Embodiment 2
[0047] The embodiment of the present invention provides a kind of preparation method of engine lubricating oil antiwear agent, comprises the following steps:
[0048] (1) Mix 1 part of nano-copper oxide with 10 parts of octadecaborate polyoxyethylene ether and stir for 12 hours under the condition of 2500 r / min to prepare modified copper oxide.
[0049] (2) Mix 10 parts of polyimide, 25 parts of polyphenylparaben (molecular weight of 50,000, particle size of 4um), 3 parts of soluble polytetrafluoroethylene ultrafine powder (10nm), 0.5 parts of anion Fluorocarbon surfactant, 5 parts of non-ionic fluorocarbon surfactant, 3 parts of vinyl silicone oil (500CST), 4 parts of dimethyl silicone oil (500CST) and the modified copper oxide obtained in step (1) at 25°C, 5000r / min under the condition of stirring for 60min to prepare the anti-wear agent.
Embodiment 3
[0051] The embodiment of the present invention provides a kind of preparation method of engine lubricating oil antiwear agent, comprises the following steps:
[0052] (1) Mix 5 parts of nano-copper oxide with 15 parts of octadecaborate polyoxyethylene ether and stir for 16 hours under the condition of 3000 r / min to prepare modified copper oxide.
[0053] (2) Mix 20 parts of polyimide, 35 parts of polyphenylparaben (molecular weight of 200,000, particle size of 10um), 6 parts of soluble polytetrafluoroethylene ultrafine powder (100nm), 5 parts of anion Fluorocarbon surfactant, 10 parts of non-ionic fluorocarbon surfactant, 10 parts of vinyl silicone oil (500CST), 4 parts of dimethyl silicone oil (500CST) and the modified copper oxide obtained in step (1) at 45 ° C, 3000r / min under the condition of stirring for 60min to prepare the anti-wear agent.
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