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Preparation method of rigid polyurethane foam heat insulation and energy saving material

A thermal insulation and energy-saving material, polyurethane rigid foam technology, applied in the field of building construction, can solve the problems of thermal insulation performance impact, high cost, insufficient stability, etc., to achieve the effect of improving thermal insulation performance, uniform cells, and enhancing overall stability

Inactive Publication Date: 2018-08-24
GUANGXI JISHUN ENERGY TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, the current polyurethane materials need to use more chemical solvents, the cost is high, and the stability is not good enough, which has a certain impact on the thermal insulation performance

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A preparation method of polyurethane rigid foam thermal insulation and energy-saving material includes the following steps:

[0020] S1. Prepare black material and white material. The weight ratio of black material and white material is 1.15:1. The black material is isocyanate. The white material is made by mixing the following raw materials in parts by weight: 90 parts of polyether polyol, deionized 16 parts of water, 8 parts of expanded vermiculite, 5 parts of acrylic resin, 2.5 parts of silicone oil foam stabilizer, 5 parts of rock wool fiber, 5 parts of bagasse fiber, 8 parts of nano calcium carbonate, N,N-dimethylcyclohexylamine 0.2 parts, 5 parts of modified tin catalyst;

[0021] S2. Mix the white material uniformly in advance, then mix the black material and the white material, use a high-pressure foaming machine to foam and inject it into the mold, and form the polyurethane rigid foam insulation and energy-saving material.

[0022] Among them, the preparation method ...

Embodiment 2

[0026] A preparation method of polyurethane rigid foam thermal insulation and energy-saving material includes the following steps:

[0027] S1. Prepare black material and white material. The weight ratio of black material and white material is 1.1:1. The black material is isocyanate. The white material is made by mixing the following raw materials in parts by weight: 70 parts of polyether polyol, deionized 15 parts of water, 6 parts of expanded vermiculite, 3 parts of acrylic resin, 2 parts of silicone oil foam stabilizer, 3 parts of rock wool fiber, 2 parts of bagasse fiber, 5 parts of nano calcium carbonate, N,N-dimethylcyclohexylamine 0.1 part, 4 parts of modified tin catalyst;

[0028] S2. Mix the white material uniformly in advance, then mix the black material and the white material, use a high-pressure foaming machine to foam and inject it into the mold, and form the polyurethane rigid foam insulation and energy-saving material.

[0029] Among them, the preparation method of t...

Embodiment 3

[0033] A preparation method of polyurethane rigid foam thermal insulation and energy-saving material includes the following steps:

[0034] S1. Prepare black material and white material, the weight ratio of black material and white material is 1.2:1, the black material is isocyanate, and the white material is made by mixing the following raw materials in parts by weight: 95 parts of polyether polyol, deionized 25 parts of water, 9 parts of expanded vermiculite, 6 parts of acrylic resin, 3 parts of silicone oil foam stabilizer, 6 parts of rock wool fiber, 6 parts of bagasse fiber, 9 parts of nano calcium carbonate, N,N-dimethylcyclohexylamine 0.3 parts, 6 parts of modified tin catalyst;

[0035] S2. Mix the white material uniformly in advance, then mix the black material and the white material, use a high-pressure foaming machine to foam and inject it into the mold, and form the polyurethane rigid foam insulation and energy-saving material.

[0036] Among them, the preparation method...

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Abstract

The invention provides a preparation method of a rigid polyurethane foam heat insulation and energy saving material. The preparation method comprises the following steps of S1, preparing a black material and a white material with the weight ratio being (1.1-1.2) to 1, wherein the black material is isocyanate, and the white material is prepared by mixing the following raw materials in parts by weight: 70-95 parts of polyether polyol, 15-25 parts of deionized water, 6-9 parts of expanded vermiculite, 3-6 parts of acrylic resin, 2-3 parts of organosilicon oil foam stabilizer, 3-6 parts of rock wool fiber, 2-6 parts of bagasse fiber, 5-9 parts of nanometer calcium carbonate, 0.1-0.3 part of N,N-dimethyl cyclohexyl amine and 4-6 parts of modified tin catalyst; and S2, uniformly mixing the whitematerial in advance, then mixing the black material and the white material, foaming a mixture with a high-pressure foaming machine, injecting a foamed product into a die, and performing formation toobtain the rigid polyurethane foam heat insulation and energy saving material. The preparation method can reduce use of a chemical solvent and improves the heat insulation performance of a whole polyurethane material at the same time.

Description

Technical field [0001] The invention relates to the field of building construction, in particular to a preparation method of a polyurethane rigid foam thermal insulation and energy-saving material. Background technique [0002] Polyurethane has the advantages of good waterproof performance, good heat preservation performance, and good adhesion performance, and has excellent mechanical properties, good electrical properties, acoustic properties and chemical resistance. It is particularly remarkable that its thermal conductivity is the lowest among all organic materials. Therefore, it has a very wide range of applications, almost being applied to all sectors of the national economy. It currently covers many engineering fields such as furniture, automotive interiors, building insulation, home appliances, etc., especially in terms of building insulation, due to the world's energy shortage and energy-saving goals. In terms of construction, it is not only widely used in industrial buil...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L75/08C08L33/04C08L5/16C08L97/02C08K13/04C08K7/12C08K7/26C08K3/26C08G18/66C08G18/48C08G18/32C08G18/24C08J9/08C08G101/00
CPCC08G18/24C08G18/3203C08G18/48C08G18/6674C08K2003/265C08K2201/003C08K2201/004C08K2201/011C08L75/08C08L2205/035C08L2205/16C08L2312/00C08G2110/0025C08G2110/0083C08L33/04C08L5/16C08L97/02C08K13/04C08K7/12C08K7/26C08K3/26
Inventor 刘建麟周帆黎明煌王戈陈少东张立颖吴定超邓克汉李晖赵克菲周洪生李猛邓颖成
Owner GUANGXI JISHUN ENERGY TECH
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