A kind of nano flake bioi and its application as electrode material
A technology of nanosheets and electrode materials, applied in the field of chemistry, can solve the problem that no one has reported the electrochemical performance of BiOI electrode materials.
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Embodiment 1
[0018] Example 1: Nano flake BiOI
[0019] A nano-flaky BiOI is prepared by the following method: first, add bismuth nitrate and potassium iodide to ethylene glycol, stir for 1 h, add 1.3 mmol bismuth nitrate and 8 mmol potassium iodide per 20 mL of ethylene glycol; then, transfer the solution Put it into the polytetrafluoroethylene lining for hydrothermal reaction, and react at a constant temperature of 170 ° C for 6 hours; finally, take it out to cool, centrifuge, wash, and dry to obtain nano-flaky BiOI.
[0020] figure 1 is the scanning electron microscope (SEM) image of the prepared BiOI, by figure 1 It can be seen that the BiOI prepared by this method is a relatively regular nano-sheet structure.
[0021] figure 2 X-ray diffraction (XRD) figure of the prepared BiOI, by figure 2 It can be seen that the BiOI prepared by this method is a pure BiOI crystal, and the standard card is JCPDS:73-2062.
Embodiment 2
[0022] Example 2: Nano flake BiOI
[0023] A nano-flaky BiOI is prepared by the following method: first, add bismuth nitrate and potassium iodide to ethylene glycol, stir for 0.5h, add 1.2mmol bismuth nitrate and 7.5mmol potassium iodide per 20mL of ethylene glycol; then, the The solution was transferred to a polytetrafluoroethylene liner for hydrothermal reaction at a constant temperature of 160°C for 6.5 hours; finally, it was taken out to cool, centrifuged, washed, and dried to obtain nano-flaky BiOI. The BiOI prepared in this example has the same morphology as the BiOI obtained in Example 1.
Embodiment 3
[0024] Example 3: Nano flake BiOI
[0025] A nano-flaky BiOI is prepared by the following method: first, add bismuth nitrate and potassium iodide to ethylene glycol, stir for 1.5h, add 1.4mmol bismuth nitrate and 8.5mmol potassium iodide per 20mL of ethylene glycol; then, the The solution was transferred to a polytetrafluoroethylene lining for hydrothermal reaction at a constant temperature of 180°C for 5.5 hours; finally, it was taken out to cool, centrifuged, washed, and dried to obtain nano-flaky BiOI. The BiOI prepared in this example has the same morphology as the BiOI obtained in Example 1.
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