Straw paint preparation method
A straw and paint technology, applied in the field of straw paint preparation, can solve the problems of low recycling rate, limited scope of recycling, and failure of straw recycling to meet market demand, and achieve huge application value and broad market prospects
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[0023] A preparation method of straw paint, comprising the steps of:
[0024] A. Stir and dissolve 10-20g straw raw materials in 100g water, stir and heat to 80°C;
[0025] B. Add 0.1-0.15g sodium dithionite, 0.4-0.6gNaHCO 3 , 0.1-0.2gNa 2 CO 3 and emulsifier, the emulsifier is formed by mixing 0.8-0.9g of nonionic surfactant x405 and 1-2g of water, and stirring for 10 minutes to obtain a mixed solution;
[0026] C. Add an initiator to the mixed solution. The initiator is mixed with 1g of potassium peroxodisulfate and 18-19g of water. First add 50% of the volume of the initiator, drop it within 10-15 minutes, and continue to stir for 15 minutes. ;
[0027] D. Add the reaction monomer to the mixed solution of step C, the reaction monomer is formed by mixing 37-38g of butyl acrylate and 31-32g of methyl methacrylate, first add the reaction monomer with a volume of 10% dropwise for 10-15 minutes After the internal dropwise addition was completed, the stirring reaction was co...
Embodiment 1
[0040] A preparation method of straw paint, comprising the steps of:
[0041] A. Stir and dissolve 10g of straw raw material in 100g of water, stir and heat to 80°C;
[0042] B. Add 0.1g sodium dithionite, 0.4gNaHCO 3 , 0.1gNa 2 CO 3 And emulsifying agent, emulsifying agent is mixed by 0.8g nonionic surfactant x405 and 2g water, stirred 10 minutes and made mixed solution;
[0043] C, adding initiator in the mixed solution, initiator is mixed by potassium peroxodisulfate 1g and 18.6g water, first adds the initiator of volume 50%, finishes dropping in 10 minutes, continues stirring reaction 15 minutes;
[0044] D. Add reaction monomer to step C mixed liquid, the reaction monomer is formed by mixing 37g of butyl acrylate and 31g of methyl methacrylate, first drop the reaction monomer of 10% by volume, and drop it within 10 minutes. Continue to stir and react for 15 minutes;
[0045] E. Add 0.2g of methacrylic acid, 0.2g of 2-hydroxypropyl methacrylate and 50% of the remainin...
Embodiment 2
[0052] A preparation method of straw paint, comprising the steps of:
[0053] A. Stir and dissolve 20g of straw raw material in 100g of water, stir and heat to 80°C;
[0054] B. Add 0.15g sodium dithionite, 0.6gNaHCO 3 , 0.2gNa 2 CO 3 And emulsifying agent, emulsifying agent is mixed by 0.9g nonionic surfactant x405 and 1g water, stirs 10 minutes and makes mixed solution;
[0055] C, adding initiator in the mixed solution, initiator is mixed by potassium peroxodisulfate 1g and 18g water, first adds the initiator of 50% of volume, adds dropwise in 15 minutes, continues stirring reaction 15 minutes;
[0056] D. Add the reaction monomer to the mixed liquid of step C, the reaction monomer is formed by mixing 38g of butyl acrylate and 32g of methyl methacrylate, first drop the reaction monomer with 10% volume, and finish the dropwise addition within 15 minutes. Continue to stir and react for 15 minutes;
[0057] E. Add 0.2g of methacrylic acid, 0.2g of 2-hydroxypropyl methacry...
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