Production method of nanometer submicron spherical silicon powder

A production method and technology of spherical silicon, applied in the fields of nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., can solve the problems of high cost, low production efficiency, large pollution, etc., to achieve increased output and moderate investment , the effect of reducing energy consumption

Active Publication Date: 2018-09-28
甘肃纳微先导基材科技有限公司
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AI Technical Summary

Problems solved by technology

[0005] In order to solve the problems of low production efficiency, large particle size, low purity, small output, high cost, and large pollution in the current production methods of nano-micron spherical silicon powder at home and abroad, the invention provides a new directed energy gasification production method

Method used

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Embodiment Construction

[0026] The present invention will be further described below in conjunction with non-limiting examples.

[0027] Embodiment: select 6N polysilicon block material or polysilicon leftovers, select materials, wash, dry, crush and grind or directly select silicon powder as a by-product of polysilicon production. Vacuumize the spherical silicon powder production device, then fill it with argon, and continuously send the material to the melting furnace for high-temperature melting through the conveying pipeline, and the silicon liquid flows into the laser gasification platform, and the laser generator is turned on to focus the laser on the molten silicon for radiation heating , so that the silicon material quickly reaches the boiling point temperature above 2355 ° C and begins to gasify into silicon vapor. The gasification speed of the material is adapted to the feeding speed to form a continuous gasification process. The silicon vapor is quickly pushed away from the gasification po...

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Abstract

The invention belongs to the technical field of inorganic non-metallic nano-micron powder material, and specifically relates to a production method of nanometer submicron silicon powder; nanometer spherical silicon is highly used for a high-energy-density silicon carbon negative electrode material of a lithium ion battery, so that energy ratio of the lithium ion battery is improved; therefore, forsolving the problems of low yield per unit, high cost and low quality of the existing nanometer silicon powder production method, particularly the problem in nanocrystallization of the silicon material in the high-energy-density silicon carbon negative electrode material of the lithium ion battery, a novel high-temperature gasification physical production method is provided; according to the method, polysilicon, monocrystal silicon or metal silicon powder are selected as the raw materials, and the nanoscale or submicron-scale spherical silicon powder is obtained through electric power heating-laser composite heating, high-temperature gasification, silicon evaporation high-temperature growth, cooling and collecting. By adoption of the production process, high-purity and high-quality nanometer silicon powder can be produced, wherein the grain diameter is in nanoscale (5-100nm) and submicron scale (0.1-10[mu]m), and the granularity can be accurately controlled; and in addition, the production process is less in waste gas, free of waste water and solid waste emission, and meanwhile, the production method is moderate in investment, high in yield and can be applicable to large scale production.

Description

technical field [0001] The invention belongs to the technical field of inorganic non-metallic nano-micron powder materials, and in particular relates to a production method of nano-submicron spherical silicon powder. technical background [0002] Nano-spherical silicon powder is mainly used as silicon-carbon anode material for high-energy-density lithium-ion batteries. In terms of the application of anode materials for lithium-ion batteries, silicon is considered to be the most promising anode material for a new generation of high-capacity lithium-ion batteries. Silicon-carbon composite materials are ideal for improving battery energy density and are the preferred choice for anode materials for high-energy density lithium-ion batteries. most preferred material. With the development of the three major fields of consumer batteries, power batteries and energy storage batteries, especially the rapid development of the new energy vehicle industry - in recent years, national poli...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01M4/38H01M10/0525B82Y30/00B82Y40/00
CPCH01M4/386H01M10/0525B82Y30/00B82Y40/00Y02E60/10
Inventor 刘培佳刘音娜刘亮
Owner 甘肃纳微先导基材科技有限公司
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