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Oil suspended agent for preventing fruit dropping as well as preparation method and application thereof

An oil suspension and suspending agent technology, applied in the field of preparations to prevent fruit drop, can solve the problems of closed field orchards, unrecorded production, and reduced effect of 1-methylcyclopropene, etc., to maintain effective action time, emulsification The effect of excellent dispersibility and excellent thermal storage stability

Active Publication Date: 2018-10-26
CHINA AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If directly process citrus with 1-methylcyclopropene, because the type of preparation directly used by 1-methylcyclopropene is a fumigant, the effect of the fumigant as spraying is very unsatisfactory; if it is made into a preparation, but the patent document There is no record of what type of preparation was made, let alone what advantages or technical problems it overcomes when making this type of preparation for spraying citrus
[0006] In short, on the one hand, for 1-methylcyclopropene fumigant, the 1-methylcyclopropene fumigant is put into water, the active ingredient 1-methylcyclopropene is released in a closed environment, and the target crops are treated in a closed environment. , and when it is used as spraying, it is impossible to seal the field orchard, which will greatly reduce the effect of 1-methylcyclopropene and greatly reduce the economic value; on the other hand, 1-methylcyclopropene fumigant has no special excipient The agent cannot be applied with oil or water, and excellent suspension performance and dispersion performance cannot be obtained, resulting in uneven distribution of the agent, clogging of the nozzle, etc.

Method used

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  • Oil suspended agent for preventing fruit dropping as well as preparation method and application thereof
  • Oil suspended agent for preventing fruit dropping as well as preparation method and application thereof
  • Oil suspended agent for preventing fruit dropping as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] Embodiment 1: 0.033% 1-methylcyclopropene microcapsule oil dispersion oil suspension

[0048] The selection and ratio of the original drug and additives are: 1-methylcyclopropene microcapsules 1%, dispersant fatty alcohol polyether phosphate 3%, thickener organic bentonite 3%, stabilizer 2,6-di Tert-butyl-4-methylphenol 1%, liquid carrier methyl oleate 92%.

[0049] Preparation methods, including:

[0050] 1) Sanding: 1% of 1-methylcyclopropene microcapsules, 3% of dispersant fatty alcohol polyether phosphate, 3% of thickener organic bentonite, 1% of stabilizer 2,6- Di-tert-butyl-4-methylphenol is mixed with 92% liquid carrier methyl oleate, dispersed and emulsified by a high-speed shearing machine, and then sand-milled in a sand mill, and filtered to obtain a highly dispersed and stable oil suspension system;

[0051] 2) Detection: through the determination of control indicators, the final product viscosity is 420mP·s, the particle size (D90) is 1.642 μm, the pH val...

Embodiment 2

[0052] Embodiment 2: 0.330% 1-methylcyclopropene microcapsule oil dispersion oil suspension

[0053] The selection and ratio of original drug and additives are: 1-methylcyclopropene microcapsule granule 10%, dispersant alkylphenol polyether phosphate 3%, thickener fumed silica 3%, stabilizer tert-butyl 1% p-hydroxyanisole, liquid carrier soybean oil 83%.

[0054] Preparation methods, including:

[0055] 1) Sanding: 10% of 1-methylcyclopropene microcapsules, 3% of dispersant alkylphenol polyether phosphate, 3% of thickener fumed silica, 1% of stabilizer Butylated hydroxyanisole is mixed with 83% soybean oil as a liquid carrier, dispersed and emulsified by a high-speed shearing machine, and then sanded in a sand mill, and filtered to obtain a highly dispersed and stable oil suspension system;

[0056] 2) Detection: through the determination of control indicators, the final product viscosity is 540mP·s, the particle size (D90) is 1.985 μm, the pH value is 6.56, and the content ...

Embodiment 3

[0057] Embodiment 3: 0.660% 1-methylcyclopropene microcapsule oil dispersion oil suspension

[0058] The selection and ratio of the original drug and additives are: 1-methylcyclopropene microcapsules 20%, dispersant arylphenol polyether phosphate 3%, thickener xanthan gum 3%, stabilizer propyl gallate Ester 1%, Liquid Carrier Mineral Oil 73%.

[0059] Preparation methods, including:

[0060] 1) sanding: with 20% 1-methylcyclopropene microcapsules, 3% dispersant arylphenol polyether phosphate, 3% thickener xanthan gum, 1% stabilizer gallic acid Propyl ester is mixed with 73% liquid carrier mineral oil, dispersed and emulsified by a high-speed shearing machine, then sanded in a sand mill, and filtered to obtain a highly dispersed and stable oil suspension system;

[0061] 2) Detection: through the determination of control indicators, the final product viscosity is 630mP·s, the particle size (D90) is 2.364 μm, the pH value is 6.89, and the content of 1-methylcyclopropene is 0.6...

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Abstract

The invention discloses an oil suspended agent for preventing fruit dropping as well as a preparation method and application thereof. The oil suspended agent for preventing the fruit dropping comprises the following components by weight percent: 1 to 40 percent of 1-methyl cyclopropene microcapsule granules, 1 to 10 percent of dispersing agent, 0.1 to 10 percent of thickening agent, 0.1 to 10 percent of stabilizing agent, and the balance of liquid carrier, wherein the content of 1-methyl cyclopropene in the oil suspended agent is 0.01 to 2 percent. The oil suspended agent has small particle size, and excellent emulsification performance, dispersity, spreading performance, viscosity, suspension rate and shelf life stability under the joint effect of the additives dispersing agent, thickening agent, stabilizer and the liquid vector; after being applied, the chemical effect can be continuously played in a given time, the chemical liquid is uniform in distribution in an open orchard environment, the acting time is ensured, the effect for preventing the dropping of fruits in a fruit picking period is good, and the harvesting time can be prolonged.

Description

technical field [0001] The invention relates to a preparation for preventing fruit drop, in particular to an oil suspension for preventing fruit drop and its preparation method and application. Background technique [0002] In order to reduce the loss of the fruit industry, relevant work can be carried out from two aspects of preventing fruit drop and post-preservation. At present, the method of preventing fruit drop mainly starts from two aspects: one is the cultural method, which suppresses the balance between plant growth and reproductive growth through fertilizer and water control, thinning flower buds, flowering girdling, etc.; the other is the use of plant growth regulation to To regulate the physiological state of fruit trees, it is generally used in the current production to spray gibberellin on the orchard before and after flowering and spray NAA before harvest. However, although spraying gibberellin can prevent flower and fruit drop, it will make the weight of the...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N27/00A01N25/04A01N25/22A01N25/02A01P21/00
Inventor 吴学民郭鑫宇张振华逄森赵锐
Owner CHINA AGRI UNIV