Fruit and vegetable preservative and preparation method and application thereof
The technology of a fruit and vegetable preservative and attapulgite clay is applied in the field of fruit and vegetable preservative and its preparation, which can solve the problems of structure collapse in contact with water and reduced adsorption performance, so as to slow down the decay progress, reduce the ethylene content, and delay the climacteric time. Effect
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Embodiment 1
[0022] Attapulgite clay was purified and crystal beam dispersed by conventional methods of purification, acid activation, and homogenization, and it was ready for use.
[0023] Measure 94.7 mL of N,N-dimethylformamide (DMF) into a 250 mL flat-bottomed single-necked flask, and add 2.0 g of Al (NO 3 ) 3 9H 2 O. 1.0 g of 2,5-dihydroxyterephthalic acid (DHTA) and 7.0 g of attapulgite clay, stir and disperse for 10 minutes after feeding, seal the bottle mouth with tin foil and place in a constant temperature oven at 120°C for 18 hours to react. After the reaction, cool down to room temperature naturally, pour off the supernatant, wash the product with N, N-dimethylformamide, ethanol, and distilled water in sequence, and then dry it at 120°C for 4 h. The obtained solid powder is a preservative. Test its The specific surface area is 850 m 2 / g, the pore volume is 0.50 cm 3 / g at 293 K, 105 Pa, the adsorption capacity of ethylene is 5.3 mol / kg, and the adsorption capacity of hydro...
Embodiment 2
[0026] Purify and disperse the attapulgite clay according to the method described in Example 1 for later use.
[0027] Measure 94.7 mL of N,N-dimethylformamide (DMF) into a 250 mL flat-bottomed single-necked flask, and add 2.6 g of Al (NO 3 ) 3 9H 2 O. 1.4 grams of 2,5-dihydroxyterephthalic acid (DHTA) and 6.0 grams of attapulgite clay were dispersed ultrasonically for 20 minutes after feeding, sealed with tin foil and placed in a constant temperature oven at 140°C for 20 hours. After the reaction, cool down to room temperature naturally, pour off the supernatant, wash the product with N, N-dimethylformamide, ethanol, and distilled water in turn, and then dry it at 120°C for 4 hours. The obtained solid powder is a preservative. Test its The specific surface area is 1060 m 2 / g, the pore volume is 0.46 cm 3 / g at 293 K, 105 Pa, the adsorption capacity of ethylene is 5.7 mol / kg, and the adsorption capacity of hydrogen sulfide is 2.5 mol / kg.
[0028] According to the method ...
Embodiment 3
[0030] Purify and disperse the attapulgite clay according to the method described in Example 1 for later use.
[0031] Measure 94.7 mL of N,N-dimethylformamide (DMF) into a 250 mL flat-bottomed single-necked flask, and add 3.9 g of Al (NO 3 ) 3 9H 2 O. 2.1 grams of 2,5-dihydroxyterephthalic acid (DHTA) and 4.0 grams of attapulgite clay were dispersed ultrasonically for 20 minutes after feeding, sealed with tin foil and placed in a constant temperature oven at 100°C for 24 hours. After the reaction, cool down to room temperature naturally, pour off the supernatant, wash the product with N,N-dimethylformamide, ethanol, and distilled water in turn, and then dry it at 120°C for 3 h. The obtained solid powder is a preservative. Test its The specific surface area is 1180 m 2 / g, the pore volume is 0.41 cm 3 / g at 293 K, 105 Pa, the adsorption capacity of ethylene is 5.1 mol / kg, and the adsorption capacity of hydrogen sulfide is 2.0 mol / kg.
[0032] According to the method descr...
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