Preparation method for high polymer composite zirconia mobile phone back cover
A technology of composite zirconia and mobile phone back cover, which is applied in the field of ceramics, can solve the problems of improving toughness and molding characteristics, and achieve the effects of increasing toughness and molding characteristics, reducing energy efficiency loss, and lowering sintering temperature
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Embodiment 1
[0028] A method for preparing a high polymer composite zirconia mobile phone back cover, comprising the following steps:
[0029] (1) Prepare raw materials: The raw materials and parts by weight for preparing the polymer composite zirconia mobile phone back cover include: 5 parts of mullite whiskers, 50 parts of zirconia powder, 15 parts of high polymer, 5 parts of filler Parts, 5 parts of plasticizer; High polymer is the copolymer of polyethylene terephthalate and polybutylene terephthalate; Plasticizer is methyl oxide acetyl linoleate;
[0030] (2), adding the mullite whiskers in the parts by weight into 40wt% ethylene glycol aqueous solution, stirring evenly to form a suspension with a mass fraction of 8%, and then adding the zirconia powder in the parts by weight, Mix well to form a precursor suspension;
[0031] (3) Transfer the precursor suspension formed in (2) to a hydrothermal kettle, react for 1 hour at a temperature of 160ºC and a pressure of 0.2MPa, and wash and d...
Embodiment 2
[0035] A method for preparing a high polymer composite zirconia mobile phone back cover, comprising the following steps:
[0036] (1) Prepare raw materials: The raw materials and parts by weight for preparing the polymer composite zirconia mobile phone back cover include: 8 parts of mullite whiskers, 80 parts of zirconia powder, 30 parts of high polymer, 10 parts of filler Parts, 8 parts of plasticizer; High polymer is the copolymer of polyethylene terephthalate and polybutylene terephthalate; Plasticizer is epoxy butyl furfurate;
[0037] (2), adding the mullite whiskers in the parts by weight into a 60wt% ethylene glycol aqueous solution, stirring evenly to form a suspension with a mass fraction of 10%, and then adding the zirconia powder in the parts by weight, Mix well to form a precursor suspension;
[0038] (3) Transfer the precursor suspension formed in (2) to a hydrothermal kettle, react for 2 hours at a temperature of 180ºC and a pressure of 0.8MPa, and wash and dry ...
Embodiment 3
[0042] A method for preparing a high polymer composite zirconia mobile phone back cover, comprising the following steps:
[0043] (1) Preparation of raw materials: The raw materials and parts by weight for preparing the polymer composite zirconia mobile phone back cover include: 5.5 parts of mullite whiskers, 60 parts of zirconia powder, 18 parts of high polymer, and 6 parts of filler Parts, 6 parts of plasticizer; High polymer is the copolymer of polyethylene terephthalate and polybutylene terephthalate; Plasticizer is epoxy octyl soybean oleate;
[0044] (2), adding the mullite whiskers in the parts by weight into a 50wt% aqueous solution of ethylene glycol, stirring evenly to form a suspension with a mass fraction of 9%, and then adding the zirconia powder in the parts by weight, Mix well to form a precursor suspension;
[0045] (3) Transfer the precursor suspension formed in (2) to a hydrothermal kettle, react for 1.5 hours under the conditions of temperature 170ºC and pres...
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