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Process for preparing high-purity quartz sand by using composite method

A technology of high-purity quartz sand and composite method, used in wet separation, chemical instruments and methods, solid separation, etc., can solve the problems of insufficient purity of quartz sand, difficult to meet the needs of enterprises, low separation efficiency, etc., and improve the grade. , The effect of low pharmaceutical consumption and meeting process requirements

Inactive Publication Date: 2018-12-21
江苏凯达石英股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the existing production technology, there are common problems such as insufficient purity of quartz sand and low sorting efficiency, which are difficult to meet the needs of enterprises

Method used

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  • Process for preparing high-purity quartz sand by using composite method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] A process for preparing high-purity quartz sand by a composite method, comprising:

[0042] 1) Crushing: Crushing the quartz sand ore to prepare 40-180 mesh quartz sand.

[0043] 2) Magnetic separation: use a magnetic separator to rough the quartz sand, remove some magnetic impurities, and obtain a magnetically separated quartz sand coarse concentrate;

[0044] 3) Slurry: Add the magnetically separated quartz sand coarse concentrate into the slurry tank, first add a pH regulator to adjust the pH of the slurry to 6-7, and then add a collector (diethylamine sodium methoxide xanthate: xanthic acid Acrylic ester=1:1) 150g / t, after stirring for 8 minutes, add 2# oil 60g / t, after stirring for 5 minutes, pump into the flotation column for flotation; the pH regulator is one of oxalic acid, hydrochloric acid, sulfuric acid one or more kinds;

[0045] 4) Flotation: pump the quartz sand coarse concentrate slurry into the cyclone static micro-bubble flotation column for flotation...

Embodiment 2

[0050] A process for preparing high-purity quartz sand by a composite method, comprising:

[0051] 1) Crushing: Crushing the quartz sand ore to prepare 40-180 mesh quartz sand.

[0052] 2) Magnetic separation: use a magnetic separator to rough the quartz sand, remove some magnetic impurities, and obtain a magnetically separated quartz sand coarse concentrate;

[0053]3) Slurry: Add the coarse concentrate of magnetically separated quartz sand into the slurry tank, first add a pH regulator to adjust the pH of the slurry to 6, and then add a collector (diethylamine sodium methoxide xanthate: propylene xanthate =1:1) 200g / t, after stirring for 10 minutes, add 2# oil 90g / t, and after stirring for 6 minutes, pump into the flotation column for flotation; the pH regulator is one of oxalic acid, hydrochloric acid, sulfuric acid or various;

[0054] 4) Flotation: pump the quartz sand coarse concentrate slurry into the cyclone static micro-bubble flotation column for flotation, the flo...

Embodiment 3

[0059] A process for preparing high-purity quartz sand by a composite method, comprising:

[0060] 1) Crushing: Crushing the quartz sand ore to prepare 40-180 mesh quartz sand.

[0061] 2) Magnetic separation: use a magnetic separator to rough the quartz sand, remove some magnetic impurities, and obtain a magnetically separated quartz sand coarse concentrate;

[0062] 3) Slurry: Add the coarse concentrate of magnetically separated quartz sand into the slurry tank, first add a pH regulator to adjust the pH of the slurry to 6, and then add a collector (diethylamine sodium methoxide xanthate: propylene xanthate =1:1) 180g / t, after stirring for 10 minutes, add 2# oil 80g / t, and after stirring for 6 minutes, pump into the flotation column for flotation; the pH regulator is one of oxalic acid, hydrochloric acid, sulfuric acid or various;

[0063] 4) Flotation: pump the quartz sand coarse concentrate slurry into the cyclone static micro-bubble flotation column for flotation, the fl...

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PUM

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Abstract

The invention discloses a process for preparing high-purity quartz sand by using a composite method. The process for preparing the high-purity quartz sand by using the composite method comprises the steps of 1) crushing; 2) magnetic separation; 3) pulp mixing; 4) floatation: pumping quartz sand rough concentrate pulp into a floatation column to be selected through floatation so as to prepare floatation-selected quartz sand rough concentrate; 5) ultrasonic treatment; 6) acid leaching: adding ultrasonically treated floatation-selected quartz sand rough concentrate to a mixed acid liquor to be leached by the acid, and controlling the acid leaching temperature at 40-60 degrees centigrade so as to obtain an acid-leached quartz sand concentrate; and 7) washing. According to the process for preparing the high-purity quartz sand by using the composite method, by using a magnetic separation, the floatation and acid leaching combined composite process to purify the quartz sand, the content of impurities in the quartz sand concentrate can be greatly reduced to obtain the high-purity quartz sand; and through combination of three sections of processes of magnetic separation primary impurity removing, floatation purification and acid leaching impurity further-removing, the grade of the quartz sand concentrate is obviously improved. According to the process for preparing the high-purity quartz sand by using the composite method, the grade of the obtained concentrate is high, the reagent consumption is low, the treatment amount is large, and a technical requirement on preparation of the high-purity quartz sand can be satisfied.

Description

technical field [0001] The invention relates to the field of quartz sand production technology, in particular to a technology for preparing high-purity quartz sand by a composite method. Background technique [0002] Quartz sand is a hard, wear-resistant, chemically stable silicate mineral whose main chemical composition is SiO2. Quartz sandstone is the main source of quartz sand siliceous mineral raw materials for glass, ceramics, foundry and other industries. Because quartz sandstone contains impurities such as associated minerals and cement, it must be purified by mineral processing before it can be used industrially. In recent years, the glass industry and the new energy industry have developed rapidly, and the amount of quartz sand has been increasing. There is a large gap in the use of quartz sand in the glass industry, which is far from meeting the needs of economic and social development and strategic emerging industries. The unique physical and chemical properties...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B03B7/00
CPCB03B7/00
Inventor 张勋张凤凯李玉军刘祥友石坤
Owner 江苏凯达石英股份有限公司
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