Environment-friendly and fireproof building sound insulation material and preparation method thereof
A technology of fire-proof building and sound-proof material, which is applied in the field of building sound-proofing, can solve the problems such as unsatisfactory fire-proof and sound-proof performance, achieve the effects of improving fire-proof and sound-proof performance, preventing moisture absorption and storage decomposition, and improving fire-proof performance
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Embodiment 1
[0022] A sound-insulating material for an environment-friendly fireproof building, the preparation method of which comprises the following steps:
[0023] (1), Weigh 7.5 parts of acrylic acid, 23 parts of bisphenol A epoxy acrylate, 9.9 parts of water, 7 parts of SR-10 emulsifier and 0.5 parts of 819 photoinitiator and add them to the reaction kettle, the stirring speed is 95r / min , keep the system temperature at 33 °C for 15 minutes, add 59 parts of amylopectin to the reaction kettle at 0.04 parts / min, raise the temperature of the reaction kettle to 58 °C and continue the reaction for 27 minutes, and the product is illuminated by a 2000W high-pressure mercury lamp for 5 seconds , transfer the product to a ball mill, maintain the ball milling temperature at 38°C, and the cylinder rotation speed at 17r / min for ball milling reaction for 50min. Under the protection of nitrogen, transfer the product to a muffle furnace. The product is heat-treated at 100°C for 1 hour, and heat-trea...
Embodiment 2
[0029] A sound-insulating material for an environment-friendly fireproof building, the preparation method of which comprises the following steps:
[0030](1), Weigh 6 parts of acrylic acid, 16 parts of bisphenol A epoxy acrylate, 8 parts of water, 6 parts of SR-10 emulsifier and 0.4 parts of 819 photoinitiator and add them to the reaction kettle, the stirring speed is 95r / min , maintain the system temperature at 33 °C for 15 minutes, add 59 parts of amylopectin to the reactor at 0.04 parts / min, raise the temperature of the reactor to 53 °C and continue the reaction for 27 minutes, and the product is illuminated by a 2000W high-pressure mercury lamp for 3 seconds , transfer the product to a ball mill, maintain the ball milling temperature at 38°C, and the cylinder rotation speed at 17r / min for ball milling reaction for 50min. Under the protection of nitrogen, transfer the product to a muffle furnace. The product is heat-treated at 100°C for 1 hour, and heat-treated at 200°C. 2h...
Embodiment 3
[0036] A sound-insulating material for an environment-friendly fireproof building, the preparation method of which comprises the following steps:
[0037] (1), Weigh 9 parts of acrylic acid, 30 parts of bisphenol A epoxy acrylate, 15 parts of water, 10 parts of SR-10 emulsifier and 1 part of 819 photoinitiator and add them to the reaction kettle, the stirring speed is 95r / min , keep the system temperature at 33 °C for 15 minutes, add 59 parts of amylopectin to the reaction kettle at 0.04 parts / min, raise the temperature of the reaction kettle to 66 °C and continue the reaction for 27 minutes, and the product is illuminated by a 2000W high-pressure mercury lamp for 8 seconds , transfer the product to a ball mill, maintain the ball milling temperature at 38°C, and the cylinder rotation speed at 17r / min for ball milling reaction for 50min. Under the protection of nitrogen, transfer the product to a muffle furnace. The product is heat-treated at 100°C for 1 hour, and heat-treated a...
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