Preparation method of champagne phenol cigarette

A technology for betel phenol and cigarettes, which is applied in the field of preparation of betel phenol cigarettes, can solve the problems of inability to satisfy the physiological habits of smoking addicts, inability to improve the risk of oral cancer, acceptance of refractory smokers, etc. The harm to human health and the effect of reducing smoking

Inactive Publication Date: 2019-01-04
许启太
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Patent CN104026727B discloses a betel nut-type chewing tobacco product, but it pays attention to the addition of tobacco ingredients in betel nut, which still cannot improve the risk of oral mucosal ulcers and oral cancer caused by betel nut due to its hard fiber and strong alkalinity
Patent CN103829369B discloses a

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The preparation method of betel phenol cigarette of the present invention comprises the following steps:

[0025] (1) Preparation of betel nut: clean 1000g of fresh betel nuts sorted, dry at 35°C, pulverize after drying, and pass through a 30-mesh sieve to obtain betel nut dry powder; % ethanol, add 0.06% cellulose compound enzyme of betel nut dry powder weight for biological cracking, adjust pH5.5, let stand for 2h, assisted by ultrasonic wave 300W, extract at 50°C for 1h, multi-stage separation, and filter to obtain extract; The column with arecoline molecule imprinted polymer was separated to obtain a solution, and the solvent was recovered under reduced pressure to obtain an extract. The extract was dried at 55° C. and crushed at 80 mesh to obtain 101 mg of arecoline, with an extraction rate of 10.1%;

[0026] (2) Betel is added to cigarettes: get betel and be dissolved in 55% ethanol for subsequent use, and the consumption of betel is 0.1% of shredded tobacco weigh...

Embodiment 2

[0030] The preparation method of betel phenol cigarette of the present invention comprises the following steps:

[0031] (1) Preparation of betel nut: get fresh betel nut 1000g, clean up, dry under the condition of 45 ℃, pulverize after drying, pass through 50 mesh sieves, obtain betel nut dry powder; betel nut dry powder is added the concentration 75% ethanol of 6 times of betel nut weight, Add 0.1% cellulose compound enzyme by weight of betel nut dry powder for biological cracking, adjust the pH to 5.0, let it stand for 1.5h, assisted by ultrasonic wave 250W, extract at 55°C for 45min, multi-stage separation, and filter to obtain the extract; Separation was carried out on the column of sub-alkaline molecular imprinted polymer to obtain a solution, and the solvent was recovered under reduced pressure to obtain an extract, which was dried at 55°C and pulverized at 100 mesh to obtain 120 mg of betelol, with an extraction rate of 12%;

[0032] (2) Betel is added to cigarettes: g...

Embodiment 3

[0036] The preparation method of betel phenol cigarette of the present invention comprises the following steps:

[0037] (1) Preparation of betel nut: clean 1000g of fresh betel nuts sorted, dry at 55°C, pulverize after drying, and pass through a 60-mesh sieve to obtain betel nut dry powder; add betel nut dry powder 8 times its weight Concentration of 75% ethanol, adding 0.15% of betel nut dry powder weight cellulose complex enzyme for biological cracking, adjusting pH 5.5, standing for 3 hours, ultrasonic 200W assisted, 55 ℃ extraction for 45 minutes, multi-stage separation, filtration, to obtain the extract; extract Separation was carried out through a column equipped with arecoline molecular imprinted polymers to obtain a solution, and the solvent was recovered under reduced pressure to obtain an extract, which was dried at 55°C and crushed at 120 mesh to obtain 128 mg of arecoline, with an extraction rate of 12.8%;

[0038] (2) Betel is added to cigarettes: get betel and d...

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PUM

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Abstract

The invention discloses a preparation method of a champagne phenol cigarette. The fresh areca nut is dried at 30-60 DEG C and crushed to obtain areca nut dry powder. Ethanol and areca nut special enzyme are added into that areca nut dry powder for carry out biological cleavage, extraction, multi-stage separation, filtration to obtain an extracted solution; the extracted solution is separated through a column filled with arecoline molecularly imprinted polymer to obtain a solution, and the solvent is recovered under reduced pressure to obtain an extract; the extract is dried below 60 DEG C, dried extract is crushed to obtain champagne phenol. The champagne phenol is dissolved in a 45 to 90 percent ethanol to obtain a champagne phenol solution; and the champagne solution is sprayed evenly onthe shredded tobacco. The invention effectively extracts champagne phenol from fresh or dried betel nut through an innovative extraction preparation process, and the extraction rate is as high as 6%-18%. The combination of champagne phenol and cigarette of the invention can improve the excitement and taste of cigarette, not only reduce the dry prickle and irritation of cigarette, but also improvethe comfort degree of cigarette mouthfeel and the smoking quality of cigarette.

Description

technical field [0001] The invention belongs to the technical field of cigarette processing, and in particular relates to a preparation method of betel phenol cigarettes. Background technique [0002] As smoking and health problems become more and more prominent, people's requirements for the quality of cigarettes are also increasing. They not only hope to refresh and relax through smoking, but also hope to reduce the harm of smoking to the human body. [0003] Betel nut is the mature fruit of Areca catechu L. in the palm family. It has been planted in my country for 2,000 years. It is the first of the four major southern medicines in my country. Anti-fatigue, anti-migraine and other functions. Betel nut chewing can produce miraculous effects of heating, flushing, slightly drunk, anti-fatigue, and excitement. It is the world's four major hobbies after cigarettes, alcoholic beverages, and coffee. There are about 700 million people chewing betel nuts in the world at present. ...

Claims

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Application Information

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IPC IPC(8): A24D1/00A24B3/12
CPCA24B3/12A24D1/002
Inventor 许启太
Owner 许启太
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