Preparation method of champagne phenol cigarette
A technology for betel phenol and cigarettes, which is applied in the field of preparation of betel phenol cigarettes, can solve the problems of inability to satisfy the physiological habits of smoking addicts, inability to improve the risk of oral cancer, acceptance of refractory smokers, etc. The harm to human health and the effect of reducing smoking
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Embodiment 1
[0024] The preparation method of betel phenol cigarette of the present invention comprises the following steps:
[0025] (1) Preparation of betel nut: clean 1000g of fresh betel nuts sorted, dry at 35°C, pulverize after drying, and pass through a 30-mesh sieve to obtain betel nut dry powder; % ethanol, add 0.06% cellulose compound enzyme of betel nut dry powder weight for biological cracking, adjust pH5.5, let stand for 2h, assisted by ultrasonic wave 300W, extract at 50°C for 1h, multi-stage separation, and filter to obtain extract; The column with arecoline molecule imprinted polymer was separated to obtain a solution, and the solvent was recovered under reduced pressure to obtain an extract. The extract was dried at 55° C. and crushed at 80 mesh to obtain 101 mg of arecoline, with an extraction rate of 10.1%;
[0026] (2) Betel is added to cigarettes: get betel and be dissolved in 55% ethanol for subsequent use, and the consumption of betel is 0.1% of shredded tobacco weigh...
Embodiment 2
[0030] The preparation method of betel phenol cigarette of the present invention comprises the following steps:
[0031] (1) Preparation of betel nut: get fresh betel nut 1000g, clean up, dry under the condition of 45 ℃, pulverize after drying, pass through 50 mesh sieves, obtain betel nut dry powder; betel nut dry powder is added the concentration 75% ethanol of 6 times of betel nut weight, Add 0.1% cellulose compound enzyme by weight of betel nut dry powder for biological cracking, adjust the pH to 5.0, let it stand for 1.5h, assisted by ultrasonic wave 250W, extract at 55°C for 45min, multi-stage separation, and filter to obtain the extract; Separation was carried out on the column of sub-alkaline molecular imprinted polymer to obtain a solution, and the solvent was recovered under reduced pressure to obtain an extract, which was dried at 55°C and pulverized at 100 mesh to obtain 120 mg of betelol, with an extraction rate of 12%;
[0032] (2) Betel is added to cigarettes: g...
Embodiment 3
[0036] The preparation method of betel phenol cigarette of the present invention comprises the following steps:
[0037] (1) Preparation of betel nut: clean 1000g of fresh betel nuts sorted, dry at 55°C, pulverize after drying, and pass through a 60-mesh sieve to obtain betel nut dry powder; add betel nut dry powder 8 times its weight Concentration of 75% ethanol, adding 0.15% of betel nut dry powder weight cellulose complex enzyme for biological cracking, adjusting pH 5.5, standing for 3 hours, ultrasonic 200W assisted, 55 ℃ extraction for 45 minutes, multi-stage separation, filtration, to obtain the extract; extract Separation was carried out through a column equipped with arecoline molecular imprinted polymers to obtain a solution, and the solvent was recovered under reduced pressure to obtain an extract, which was dried at 55°C and crushed at 120 mesh to obtain 128 mg of arecoline, with an extraction rate of 12.8%;
[0038] (2) Betel is added to cigarettes: get betel and d...
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