Lithium battery special anti-warping adhesive and preparation method and anti-warping tab tape
A lithium battery and adhesive technology, which is applied in the manufacture of electrolyte batteries, adhesives, and adhesive additives, etc., can solve the problems of unwinding and degumming, large unwinding force, etc., and achieve the effect of improving the anti-lifting performance.
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Embodiment 1
[0022] Example 1, it is an adhesive with excellent anti-warping performance for lithium batteries, which is prepared by the following steps. In step 1, an adhesive with excellent anti-warping performance for lithium batteries is synthesized, and 40 parts of isooctyl acrylate ( EHA), 10 parts of lauryl acrylate (LA), 4 parts of itaconic acid, 3 parts of 4-methacryloxyethyl trimellitic anhydride (4-META), 5 parts of methyl acrylate (MMA) , 2 parts of tetrahydrofuran acrylate (THFA), 0.02 parts of free radical initiator azobisisobutyronitrile (AIBN), 0.2 parts of copper chloride, 0.3 parts of 2,2'-bipyridine and 100 parts of toluene After mixing, nitrogen deoxygenation was carried out for 90 minutes, the temperature was controlled at 75°C, and the reverse atom transfer radical polymerization (R-ARTP) polymerization reaction was carried out under the protection of nitrogen for 10 hours. The number average molecular weight (Mn) was controlled to 455100, and the molecular weight The...
Embodiment 2
[0025] Example 2, which is an adhesive with excellent anti-warping performance for lithium batteries, which is prepared by the following steps. In step 1, an adhesive with excellent anti-warping performance for lithium batteries is synthesized, and 30 parts of isooctyl acrylate ( EHA), 20 parts of lauryl acrylate (LA), 5 parts of itaconic acid, 5 parts of 4-methacryloxyethyl trimellitic anhydride (4-META), 8 parts of methyl acrylate (MMA) , 1 part of tetrahydrofuran acrylate (THFA), 0.04 part of free radical initiator azobisisobutyronitrile (AIBN), 0.2 part of copper chloride, 0.4 part of 2,2'-bipyridine and 80 parts of acetic acid After mixing the ethyl esters, deoxygenate with nitrogen for 50 minutes, control the temperature at 80°C, and carry out reverse atom transfer radical polymerization (R-ARTP) polymerization reaction under the protection of nitrogen for 8 hours, and the number average molecular weight (Mn) is controlled to 321500 , the molecular weight polydispersity ...
Embodiment 3
[0028] Embodiment 3, which is an adhesive with excellent anti-warping performance for lithium batteries, which is prepared by the following steps. Step 1 synthesizes an adhesive with excellent anti-warping properties for lithium batteries, and 40 parts of isooctyl acrylate ( EHA), 10 parts of lauryl acrylate (LA), 2 parts of itaconic acid, 4 parts of 4-methacryloxyethyl trimellitic anhydride (4-META), 5 parts of methyl acrylate (MMA) , 2 parts of tetrahydrofuran acrylate (THFA), 0.08 parts of free radical initiator azobisisobutyronitrile (AIBN), 0.1 part of copper chloride, 0.2 parts of 2,2'-bipyridine and 70 parts of acetic acid After mixing the ethyl esters, carry out nitrogen deoxygenation for 100 minutes, control the temperature at 75°C, and carry out the reverse atom transfer radical polymerization (R-ARTP) polymerization reaction under the protection of nitrogen for 20 hours, and the number average molecular weight (Mn) is controlled at 205200 , the molecular weight poly...
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