PTFE (polytetrafluoroethylene) separation material
A technology of polytetrafluoroethylene and separation materials, applied in the direction of semi-permeable membrane separation, total evaporation, membrane, etc., can solve the problems of short service life, high cost of use, easy damage, etc., achieve strong fiber form, and improve durability , the effect of preventing collapse
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Embodiment 1
[0019] The polytetrafluoroethylene separation material of this embodiment has a three-dimensional interconnected pore structure, and is characterized in that the stems surrounding the pores have stem holes. The pore diameter is 100-1000nm, the stem diameter is 50-300nm, and the stem pore diameter is not less than 30nm and less than 100nm. The porosity of the pores is 50%-95%, and the porosity of the stem pores is 15-65%.
[0020] Pore diameter, stem diameter, and porosity were detected by nano-CT.
[0021] The preparation method of described PTFE material, comprises the following steps:
[0022] (1) Preparation of spinning solution: dissolve polyvinyl alcohol in water, add polytetrafluoroethylene emulsion, and mix well;
[0023] (2) Spinning: use high-voltage electrospinning equipment for electrospinning to obtain a uniform nanofiber precursor film;
[0024] (3) Sintering: ①Raise the temperature from room temperature to 90-120°C while maintaining a vacuum state. The vacuu...
Embodiment 2
[0027] The polytetrafluoroethylene separation material in this embodiment has a three-dimensional penetrating pore structure, with stem holes surrounding the pore, the pore diameter is 200±100nm, the stem diameter is 125±75nm, and the stem pore diameter is 50±20nm.
[0028] Wherein (I) the porosity of the pores is 60±10%, the porosity of the stem pores is 55±10%; the total surface area of the stems, stem area:stem hole area=1-15:1.
[0029] Or (II) the porosity of the pores is 60±10%, and the porosity of the stem pores is 55±10%; the total surface area of the stem, stem area:stem hole area=16-30:1.
[0030] Or (Ⅲ) the porosity of the pores is 80±10%, and the porosity of the stem pores is 30±15%; the total surface area of the stem, stem area:stem hole area=1-15:1.
[0031] Or (IV) The porosity of the pores is 80±10%, and the porosity of the stem pores is 30±15%; the total surface area of the stem, stem area:stem hole area=16-30:1.
[0032] Stem surface area image analy...
Embodiment 3
[0040] The polytetrafluoroethylene separation material in this embodiment has a three-dimensional penetrating pore structure, with stem holes surrounding the pore, the pore diameter is 200±10nm, the stem diameter is 125±10nm, and the stem pore diameter is 45±5nm.
[0041] Wherein (I) the porosity of the pores is 60%, and the porosity of the stem pores is 55%; the total surface area of the stem, stem area:stem hole area=7:1.
[0042] Or (II) the porosity of the pores is 60%, and the porosity of the stem pores is 55%; the total surface area of the stem, stem area:stem hole area=23:1.
[0043] Or (Ⅲ) The porosity of the pores is 80%, and the porosity of the stem pores is 30%; the total surface area of the stem, stem area:stem hole area=7:1.
[0044]Or (IV) The porosity of the pores is 80%, and the porosity of the stem pores is 30%; the total surface area of the stem, stem area:stem hole area=23:1.
[0045] Porosity of material = porosity of pores + (1 - porosity of pores...
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