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Low Salt and Low Alkali Reactive Dyeing Process by Air Dyeing

A technology of alkali activity and air flow, which is applied in the fields of dyeing, textile and papermaking, and spray/jet textile material treatment. It can solve the problems of difficult sewage treatment, low dye utilization rate, waste of water resources, etc., and reduce the difficulty of sewage treatment. , The effect of improving the utilization rate of dyestuffs and reducing the water consumption of washing

Active Publication Date: 2021-07-20
ZHEJIANG MIZUDA TEXTILE PRINTING & DYEING TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the dyeing of cotton fabrics with traditional reactive dyes, the reactive groups of reactive dyes and cotton fibers are activated under alkaline conditions and then undergo addition reactions with the hydroxyl groups of fibers. The reactive groups of reactive dyes need to be consumed to activate More alkali agent, more alkali agent will cause the hydrolysis of the dye at the same time, and a large amount of salt needs to be consumed in the dyeing process, especially in air-flow dyeing, the consumption of alkali agent and salt is much greater than that of continuous dyeing. Acid neutralization is also required, and a large amount of water is consumed during washing, resulting in reduced dye utilization, waste of water resources, acid neutralization, high cost, and difficult sewage treatment.
Therefore, the reactive dyeing process of air dyeing has the problems of lower dye utilization rate, waste of water resources, need for acid neutralization, high cost, and difficult sewage treatment

Method used

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  • Low Salt and Low Alkali Reactive Dyeing Process by Air Dyeing
  • Low Salt and Low Alkali Reactive Dyeing Process by Air Dyeing
  • Low Salt and Low Alkali Reactive Dyeing Process by Air Dyeing

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Example 1. The low-salt and low-alkali active dyeing process of air dyeing comprises the following steps,

[0024] A. Choose the following dyes

[0025] For product A;

[0026] B, carry out pretreatment to all-cotton cloth according to conventional process, obtain B product;

[0027] C. Put product B into the air-flow atomization dyeing machine, connect product B end to end to form a rope, add 1.2% owf product A into the tank, the bath ratio is 1:4; The mass fraction of powder is 15%%; add soda ash until the concentration of soda ash in the tank is 2g / L; heat up to 30°C, and dye for 20min; add soda ash again until the concentration of soda ash in the tank is 5g / L; heat up to 55°C, Dyeing for 20 minutes; Drain to obtain product C;

[0028] D. Soap product C for 10 minutes and drain to obtain product D;

[0029] E. Wash and dry product D according to the conventional process to obtain a finished product.

Embodiment 2

[0030] Example 2. The low-salt and low-alkali active dyeing process of air dyeing comprises the following steps,

[0031] A. Choose the following dyes

[0032] For product A;

[0033] B. Pretreating the rayon cloth according to the conventional process to obtain product B;

[0034] C. Put product B into the air-flow atomization dyeing machine, connect product B end to end to form a rope, add 2.8% owf product A into the tank, the bath ratio is 1:3; The mass fraction of powder is 25%; add soda ash until the concentration of soda ash in the vat is 4g / L; heat up to 30°C and dye for 15min; add soda ash again until the concentration of soda ash in the vat is 8g / L; heat up to 65°C and dye 30min; Drain liquid to obtain product C;

[0035] D. Soap product C for 15 minutes and drain to obtain product D;

[0036] E. Wash and dry product D according to the conventional process to obtain a finished product.

Embodiment 3

[0037] Example 3. The low-salt and low-alkali active dyeing process of air dyeing is characterized in that: comprising the following steps,

[0038] A. Choose the following dyes

[0039] For product A;

[0040] B, carry out pretreatment to polyester-cotton cloth according to routine process, obtain B product;

[0041] C. Put product B into the air-flow atomization dyeing machine, connect product B end to end to form a rope, add 1.5% owf product A into the tank, the bath ratio is 1:4; The mass fraction of powder is 18%; add soda ash until the concentration of soda ash in the vat is 3g / L; heat up to 30°C and dye for 20min; add soda ash again until the concentration of soda ash in the vat is 6g / L; heat up to 55°C and dye 30min; Drain liquid to obtain product C;

[0042] D. Soap product C for 10 minutes and drain to obtain product D;

[0043] E. Wash and dry product D according to the conventional process to obtain a finished product.

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PUM

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Abstract

The invention discloses a low-salt and low-alkali active dyeing process for air dyeing, which comprises the following steps: A. Select a vinyl sulfone type reactive dye containing a group that activates the vinyl sulfone group, which is product A; Pretreat the fabric to obtain product B; C, put product B into the air-flow atomization dyeing machine, add product A into the vat, the bath ratio is 1:3~4; add sodium bicarbonate; add soda ash; heat up to 30°C , dye for 15-20min; then add soda ash; heat up to 55-65℃, dye for 20-30min; The conventional process washes and dries product D to obtain a finished product. The invention has the characteristics of improved dyestuff utilization rate, water resource saving, no need of acid neutralization, reduced cost and reduced sewage treatment difficulty.

Description

technical field [0001] The invention relates to the technical field of reactive dyeing by air-dyeing, in particular to a low-salt and low-alkali reactive dyeing process by air-dyeing. Background technique [0002] Reactive dyes have the characteristics of bright color, good level dyeing, simple dyeing method, high color fastness, complete color spectrum and low cost. Therefore, reactive dyeing is widely used. In the dyeing of cotton fabrics with traditional reactive dyes, the reactive groups of reactive dyes and cotton fibers are activated under alkaline conditions and then undergo addition reactions with the hydroxyl groups of fibers. The reactive groups of reactive dyes need to be consumed to activate More alkali agent, more alkali agent will cause the hydrolysis of the dye at the same time, and a large amount of salt needs to be consumed in the dyeing process, especially in air-flow dyeing, the consumption of alkali agent and salt is much greater than that of continuous d...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P1/38D06P1/673D06P1/00D06B1/02
CPCD06B1/02D06P1/0032D06P1/38D06P1/6735
Inventor 乐德忠
Owner ZHEJIANG MIZUDA TEXTILE PRINTING & DYEING TECH CO LTD
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