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A kind of aluminum-titanium aluminum intermetallic compound-alumina composite material and its preparation method and application

A composite material and titanium oxide technology, applied in the field of aluminum-titanium-aluminum intermetallic compound-alumina composite material and its preparation, can solve the problems of reducing material properties, affecting material properties, agglomeration, etc., and achieving excellent room temperature and high temperature performance, The effect of fine aluminum grain size and excellent mechanical properties

Active Publication Date: 2020-08-07
WUHAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The problems existing in these preparation methods are: TiAl in the obtained composite materials 3 particles and Al 2 o 3 The particle content is low, which affects the improvement of material performance; the original TiO 2 When there are many nanoparticles, it is difficult to disperse, and it is easy to cause agglomeration, which in turn leads to the formation of new TiAl 3 Particles and Al 2 o 3 Particle agglomeration reduces material properties; high cost severely limits process development and further optimization

Method used

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  • A kind of aluminum-titanium aluminum intermetallic compound-alumina composite material and its preparation method and application
  • A kind of aluminum-titanium aluminum intermetallic compound-alumina composite material and its preparation method and application
  • A kind of aluminum-titanium aluminum intermetallic compound-alumina composite material and its preparation method and application

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] Titanium oxide nanoparticles are used as reinforcements, and pure aluminum flakes are used as substrates. The size of the pure aluminum sheet used in this embodiment is 300 mm in length, 100 mm in width and 0.2 mm in thickness. Titanium oxide nanoparticles have a size of 55 nm. A precision rolling mill is adopted, and the rolling speed is set at 187mm / min.

[0040] First, cut the original pure aluminum sheet into a size of 100*20*0.2mm, take 10 pieces as the original substrate, and polish and ultrasonically clean the surface to remove oil, impurities and oxides on the surface, and the obtained pure The aluminum sheet is designated as aluminum sheet A.

[0041] After calculation, the titanium oxide nanoparticles are added into an appropriate amount of ethanol, and ultrasonically dispersed, so that the titanium oxide nanoparticles are uniformly dispersed in the ethanol to form a titanium oxide-ethanol suspension. Pour the titanium oxide-ethanol suspension evenly on 9 p...

Embodiment 2

[0045] Titanium oxide nanoparticles are used as reinforcements, and pure aluminum flakes are used as substrates. The size of the pure aluminum sheet used in this embodiment is 300 mm in length, 100 mm in width, and 0.2 mm in thickness, and the size of titanium oxide nanoparticles is 55 nm. A precision rolling mill is adopted, and the rolling speed is set at 187mm / min.

[0046] First, cut the original pure aluminum sheet into a size of 100*20*0.2mm, take 10 pieces as the original substrate, and polish and ultrasonically clean the surface to remove oil, impurities and oxides on the surface, and the obtained pure The aluminum sheet is designated as aluminum sheet A.

[0047] After calculation, the TiO 2 The nanoparticles are added into an appropriate amount of ethanol, and dispersed ultrasonically to form a titanium oxide-ethanol suspension. Pour the titanium oxide-ethanol suspension evenly on 9 pieces of aluminum, and place it for a certain period of time. After the ethanol i...

Embodiment 3

[0052] Titanium oxide nanoparticles are used as reinforcements, and pure aluminum flakes are used as substrates. The size of the pure aluminum sheet used in this embodiment is 300 mm in length, 100 mm in width, and 0.2 mm in thickness, and the size of titanium oxide nanoparticles is 55 nm. A precision rolling mill is adopted, and the rolling speed is set at 187mm / min.

[0053] First, cut the original pure aluminum sheet into a size of 100*20*0.2mm, take 10 pieces as the original substrate, and polish and ultrasonically clean the surface to remove oil, impurities and oxides on the surface, and the obtained pure aluminum sheet is recorded as Make aluminum sheet A.

[0054] After calculation, the TiO 2 The nanoparticles are added into an appropriate amount of ethanol, and dispersed ultrasonically to form a titanium oxide-ethanol suspension. Pour the titanium oxide-ethanol suspension evenly on 9 pieces of aluminum, and place it for a certain period of time. After the ethanol is...

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Abstract

The invention discloses an aluminum-titanium aluminum intermetallic compound-aluminum oxide composite material and a preparing method and application thereof. Firstly, nano TiO2 particles and an aluminum sheet are subjected to accumulative pack rolling into an Al-TiO2 composite material prefabricated body; then, the Al-TiO2 composite material prefabricated body is arranged in the high-temperatureand high-pressure condition, the in-situ chemical reaction is induced, and TiAl3 and Al2O3 mixed particles are generated; and then, a sample is heated to the temperature at the aluminum melting pointor above, heat extrusion treatment is conducted, and a final Al-TiAl3-Al2O3 composite material is obtained. According to the technology, the low initial TiO2 particle volume fraction is utilized, through the chemical reaction of Al-TiO2 and aluminum selective heat extrusion, the content of target particles is greatly adjusted, the total volume fraction of generated TiAl3 particles and Al2O3 particles is 3.6-9.9 times of the initial TiO2 particle volume fraction, the microscopic structure is fine, and particle distribution is uniform. The prepared Al-TiAl3-Al2O3 composite material is excellentin mechanical performance, the hardness reaches up to 532.8HV to the maximum degree and is 21.7 times of the hardness of pure aluminum, the room-temperature compression strength reaches up to 1311.9 MPa to the maximum degree, the compression strength reaches up to 918.6 MPa to the maximum degree at 300 DEG C, the compression strength reaches up to 564.6 MPa to the maximum degree at 600 DEG C, andthe compression strength is 225.2 MPa at 700 DEG C.

Description

technical field [0001] The invention relates to an aluminum-titanium aluminum intermetallic compound-alumina composite material and a preparation method and application thereof, belonging to the field of composite material preparation. Background technique [0002] With the development of industry and science and technology, the application of material properties in practical situations is becoming more and more important, and the requirements and standards are getting higher and higher, especially in cutting-edge fields such as aerospace and military. It is gradually difficult for single metals and alloys to meet the actual requirements, which leads to the rapid and rapid development of metal matrix composites. Compared with traditional pure metal and alloy materials, metal matrix composites can not only play a coordinated role between matrix and reinforcement, but also adjust the type and content of matrix and reinforcement to obtain materials with different properties acc...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C1/10C22C21/00C22C32/00
CPCC22C1/1026C22C21/00C22C32/0036
Inventor 梅青松张高攀陈峰马烨杨向阳梅鑫明惠涵煜李菊英
Owner WUHAN UNIV
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