Preparation method of environment-friendly lead-cadmium-free red glass and product prepared by the same

A cadmium red, environment-friendly technology, which is applied in glass manufacturing equipment, glass molding, manufacturing tools, etc., can solve the problems of complex melting process and unstable color of antimony red glass, and achieve efficient production and preparation methods Simple and easy to use, promotes the effect of color development

Active Publication Date: 2019-05-31
JINGDEZHEN CERAMIC INSTITUTE
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The object of the present invention is to overcome the deficiencies of the prior art, and provide an environment-friendly preparation method of lead-free cadmium red glass, by performing low-temperature pretreatment on the colorant, to effectively solve the problem of complex melting process of antimony red glass in the prior art, color instability problem

Method used

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  • Preparation method of environment-friendly lead-cadmium-free red glass and product prepared by the same

Examples

Experimental program
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Effect test

Embodiment 1

[0026] The preparation method of a kind of environment-friendly lead-free cadmium red glass of this embodiment, its steps are as follows:

[0027] (1) Pretreatment of stable colorants

[0028] According to the composition of the stable coloring agent in parts by mass, it is Sb 2 o 3 1.50 parts, 2.63 parts of S, 0.38 parts of C, 0.011 parts of CuO; after mixing the components of the above-mentioned stable colorant evenly, the stable colorant according to the mass ratio: sodium silicate water glass=1:9, mixed with sodium silicate water glass Uniformly form a semi-solid mixture; then place it in a low-temperature oven at 90°C to dry to constant weight, pass through a 200-mesh standard sieve after crushing, and obtain a pretreated stable colorant;

[0029] (2) Preparation of mixed raw materials

[0030] According to the composition of the basic components in parts by mass, it is SiO 2 48.81 parts, Na 2 CO 3 22.72 copies, K 2 CO 3 11.08 parts, CaCO 3 10.84 copies, H 3 BO ...

Embodiment 2

[0037] The preparation method of a kind of environment-friendly lead-free cadmium red glass of this embodiment, its steps are as follows:

[0038] (1) Pretreatment of stable colorants

[0039] According to the composition of the stable coloring agent in parts by mass, it is Sb 2 o 3 2.51 parts, 2.27 parts of S, 0.46 parts of C, and 0.015 parts of CuO; after mixing the components of the above-mentioned stable colorant evenly, the stable colorant according to the mass ratio: sodium silicate water glass=1:11, mixed with sodium silicate water glass Uniformly form a semi-solid mixture; then place it in a low-temperature oven at 130°C and dry it to constant weight, pass through a 200-mesh standard sieve after crushing, and obtain a pretreated stable colorant;

[0040] (2) Preparation of mixed raw materials

[0041] According to the composition of the basic components in parts by mass, it is SiO 2 46.45 parts, Na 2 CO 3 20.61 copies, K 2 CO 3 12.07 parts, CaCO 3 12.56 copies...

Embodiment 3

[0048] The preparation method of a kind of environment-friendly lead-free cadmium red glass of this embodiment, its steps are as follows:

[0049] (1) Pretreatment of stable colorants

[0050] According to the composition of the stable coloring agent in parts by mass, it is Sb 2 o 3 1.77 parts, 1.95 parts of S, 1.07 parts of C, 0.015 parts of CuO; after mixing the components of the above-mentioned stable colorant evenly, the stable colorant according to the mass ratio: sodium silicate water glass=1:13, mixed with sodium silicate water glass Uniformly form a semi-solid mixture; then place it in a low-temperature oven at 150°C to dry to constant weight, pass through a 200-mesh standard sieve after crushing, and obtain a pretreated stable colorant;

[0051] (2) Preparation of mixed raw materials

[0052] According to the composition of the basic components in parts by mass, it is SiO 2 49.22 parts, Na 2 CO 3 24.71 copies, K 2 CO 3 9.67 parts, CaCO 3 8.93 copies, H 3 BO ...

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Abstract

The invention discloses a preparation method of environment-friendly lead-cadmium-free red glass. Basic components and a stable colorant are used as raw materials. The method includes the steps that firstly, the stable colorant and sodium silicate are mixed evenly and subjected to low-temperature pretreatment, and then the mixture and the basic components are mixed evenly to obtain a mixed raw material; the mixed raw material is molten at a rising temperature to form a melt, and after temperature reduction, forming and natural cooling to the room temperature, basic glass is obtained; the basicglass is calcined for secondary color development, and then the environment-friendly lead-cadmium-free red glass is obtained. Besides, the invention discloses the product prepared by the preparationmethod of the environment-friendly lead-cadmium-free red glass. The preparation method is simple and easy to implement, the technological process is stable and reliable, the problems that in the priorart, a founding technology is complex and color development is not stable are effectively solved, and the obtained product has high visible light transmittance and can be widely applied to many fields such as building materials, artistic decoration and optical application.

Description

technical field [0001] The invention relates to the technical field of glass materials, in particular to a method for preparing an environment-friendly lead-cadmium-free red glass suitable for the fields of building materials, art decoration, and optical applications, and the prepared product. Background technique [0002] Red is the color of celebration. Red glass is not only commonly used in building materials and optical applications, but is also currently used in art decoration, jewelry necklace products, imitation rubies and other fields. It has very broad application prospects and market potential. However, as people pay more and more attention to environmental protection issues, traditional red glass has attracted more and more attention regardless of its material, components or production process. As we all know, in order to obtain bright red glass, it is necessary to add a colorant to the components of the glass to achieve stable coloring of the glass. At present, ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C3/089C03B19/02C03B25/00
Inventor 肖卓豪石旭海肖晓东孔令兵罗文艳
Owner JINGDEZHEN CERAMIC INSTITUTE
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