Cationic paraffin emulsion as well as preparation method and application thereof

A paraffin emulsion, cationic technology, applied in fiber types, textiles and papermaking, fiber processing, etc., can solve the problems of large emulsifier content, limited use of emulsified paraffin, affecting paraffin waterproofness, etc., to ensure the effect of waterproofing.

Active Publication Date: 2019-06-21
上海舜雅化工有限公司
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  • Claims
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Problems solved by technology

Another example is that the Chinese invention patent application with the notification number CN106188572A discloses a high-solid paraffin emulsion and a preparation method thereof. In the above two inventions, an aqueous solution of aluminum sulfate is introduced, which can be used in wood, leather and metal products. Used as

Method used

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  • Cationic paraffin emulsion as well as preparation method and application thereof
  • Cationic paraffin emulsion as well as preparation method and application thereof
  • Cationic paraffin emulsion as well as preparation method and application thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0047] Embodiment 1: A kind of cationic paraffin emulsion, comprising 25.6Kg of distilled water, 20Kg of No. 56 paraffin, 0.7Kg of hydrogenated tallow amine-2EO, 0.1Kg of 99% glacial acetic acid by weight.

[0048] Its preparation method is: with 25.6Kg of distilled water, No. 56 paraffin wax of 20Kg, 0.7Kg of hydrogenated tallow amine-2EO (that is, hydrogenated tallow amine polyoxyethylene ether containing two ethylene oxide EO), 0.1Kg weight percent is Add 99% glacial acetic acid into the pressure emulsification kettle, and seal the pressure emulsification kettle; then directly heat it to 90±10°C, keep it warm for 3 hours until the No. 56 paraffin and hydrogenated tallow amine-2EO in the pressure emulsification kettle are all Melt, then carry out temperature-controlled stirring at a stirring speed of 50r / min. After stirring for 10 minutes, the temperature in the pressure emulsification tank reaches 75°C. At this time, under a homogenizing pressure of 30MPa, the material is ho...

Embodiment 2

[0049] Embodiment 2: a cationic paraffin emulsion, comprising 25.6Kg of pure water, 20Kg of No. 75 microcrystalline paraffin, 1Kg of tallow amine-2EO, 0.1Kg of 99% glacial acetic acid by weight.

[0050] Its preparation method is: with the pure water of 25.6Kg, No. 75 microcrystalline paraffin of 20Kg, the tallow amine-2EO of 1Kg (promptly containing the tallow amine polyoxyethylene ether of two ethylene oxide EOs), 0.1Kg weight percentage is Add 99% glacial acetic acid into the pressure emulsification kettle, and seal the pressure emulsification kettle; then directly heat to 102.5±2.5°C, keep warm for 4 hours until the No. 75 microcrystalline paraffin and tallow amine-2EO in the pressure emulsification kettle All melted, followed by temperature-controlled stirring at a stirring speed of 60r / min. After stirring for 12 minutes, the temperature in the pressure emulsification tank reached 95°C. At this time, under a homogenizing pressure of 35MPa, the material was homogenized and ...

Embodiment 3

[0051] Embodiment 3: a cationic paraffin emulsion, including 25.6Kg of tap water, 20Kg of No. 75 medical white petrolatum, 0.6Kg of dodecylamine-5EO, and 0.03Kg of 99% glacial acetic acid by weight.

[0052] The preparation method is as follows: 25.6Kg of tap water, 20Kg of No. 75 medical white vaseline, 0.6Kg of dodecylamine-5EO (that is, dodecylamine polyoxyethylene ether containing five ethylene oxide EOs), 0.03Kg of weight Add glacial acetic acid with a percentage of 99% into the pressure emulsification kettle, and seal the pressure emulsification kettle; then directly heat it to 75±5°C and keep it warm for 3.5 hours until all the dodecylamine-5EO in the pressure emulsification kettle melts , and then carry out temperature-controlled stirring at a stirring speed of 70r / min. After stirring for 13 minutes, the temperature in the pressure emulsification tank reaches 70°C. At this time, under a homogenizing pressure of 35MPa, the material is homogeneously discharged through a h...

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Abstract

The invention discloses a cationic paraffin emulsion as well as a preparation method and an application thereof and belongs to the technical field of paraffin emulsion processing. The cationic paraffin emulsion is technically characterized by being prepared from components in percentage by weight as follows: 42%-43.5% of paraffin, 1.3%-2.15% of fatty amine polyoxyethylene ether, 0.01%-0.22% of glacial acetic acid and 54.5%-55.0% of water. The preparation method of the cationic paraffin emulsion comprises operation steps as follows: step 1, water, paraffin, fatty amine polyoxyethylene ether andglacial acetic acid are added to a reaction kettle, and the reaction kettle is sealed; step 2, the reaction kettle is heated to 80-105 DEG C, a thermal insulation reaction is performed for 1-5 h until the paraffin and the fatty amine polyoxyethylene ether in the reaction kettle are fully melt; step 3, stirring is started and the temperature in the reaction kettle is controlled at 70-95 DEG C; step 4, homogenization and discharging are performed, a product is cooled to the room temperature, and the cationic paraffin emulsion can be obtained. According to the cationic paraffin emulsion, the total content of fatty amine polyoxyethylene ether is lower; the paraffin is waterproof, but an emulsifier is not waterproof, so that the waterproof property and the lubrication performance of paraffin are guaranteed to the greatest extent.

Description

technical field [0001] The invention belongs to the technical field of paraffin emulsion processing, more specifically, it relates to a cationic paraffin emulsion and its preparation method and application. Background technique [0002] Paraffin wax emulsion is a waxy and water-containing homogeneous fluid made by physical modification of various waxes including petroleum wax; it is made of paraffin wax and several emulsifiers of different types and performances and appropriate regulators through emulsification reactions. A stable emulsion of solid-oil-water multiphase dispersion system. [0003] It is understood that paraffin is the most widely used wax. In emulsion, paraffin is often used as waterproofing agent, lubricant and release agent. Cationic paraffin emulsions are often used in cationic systems, which are suitable for areas with negative surface charges, such as fabrics, paper fibers, etc. [0004] The current technologies can be roughly divided into two categor...

Claims

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Application Information

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IPC IPC(8): C08J3/03C08L91/06C08L71/02C08K5/09D06M15/01D06M101/06D06M101/32D06M101/34
Inventor 周德春刘松
Owner 上海舜雅化工有限公司
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