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Method for performing localized crystallization of zinc silicate on ceramic plane and preparing ceramic

A technology of zinc silicate and ceramics, which is applied in the field of zinc silicate positioning crystallization and preparation of ceramics, which can solve problems such as poor product stability and repeatability, difficult crystal distribution and quantity, and difficulties in commercial production, and achieve the solution of crystal sizes. , flexible and convenient crystallization, good crystallization effect

Active Publication Date: 2019-07-09
GUANGDONG DABU CERAMIC IND RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Crystalline glaze is regarded as a kind of luxurious decorative porcelain, which endows ceramic products with elegant and unrepetitive pictures, but because of its narrow firing range, it is easy to flow glaze, and it is often difficult to artificially control the distribution and distribution of crystals in the glaze. The quantity makes the stability and repeatability of this kind of products extremely poor, which brings difficulties to commercial production

Method used

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  • Method for performing localized crystallization of zinc silicate on ceramic plane and preparing ceramic
  • Method for performing localized crystallization of zinc silicate on ceramic plane and preparing ceramic
  • Method for performing localized crystallization of zinc silicate on ceramic plane and preparing ceramic

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preparation example Construction

[0027] (1) Preparation of crystalline glaze: Weigh the raw materials according to the following percentages by weight: feldspar 15-25%, quartz 5-10%, talc 5-10%, calcite 5-10%, kaolin 2-5%, oxidized 30-40% zinc, 10-20% glass powder, 1.5-2.5% iron red; put the weighed raw materials into a ball mill for grinding. When grinding, the ratio of material: ball: water is 1:1.5-2.5:0.6 ~1.2, grind until the fineness of the slurry is 0.1-0.2% after passing through a 300-mesh sieve, and the water content of the surface glaze slurry obtained after grinding is 45-50%, and set aside.

[0028] Under different viscosities, the speed of crystal growth is different. The growth of crystals is restricted by the viscosity of the melt, and the size of the viscosity directly binds the diffusion and migration of crystal-forming particles in the melt. Generally, the high temperature viscosity of crystalline glaze is small, the main reason is that Na 2 O and other flux content is high, while Al 2 o ...

Embodiment 1

[0040] A method for performing positional crystallization of zinc silicate on a ceramic plane and preparing ceramics, the method comprising the steps of:

[0041] (1) Preparation of crystalline glaze: Weigh the raw materials respectively according to the following percentages by weight: 15% feldspar, 10% quartz, 10% talc, 10% calcite, 5% kaolin, 30% zinc oxide, 18.5% glass powder, iron Red 1.5%; Put the weighed raw materials into a ball mill for grinding. When grinding, the ratio of material: ball: water is 1:1.5:0.6, and the fineness of the slurry is 0.1-0.2% after passing through a 300-mesh sieve. , the surface glaze slurry obtained after grinding has a water content of 45% to 50%, and is set aside.

[0042] (2) To make colored glaze, each raw material is weighed respectively according to the following percentages by weight: 90% of transparent feldspar glaze, 10% of wrapped red agent; the two raw materials are mixed and stirred evenly, and cross 100 sieves to prepare semi-fi...

Embodiment 2

[0049] A method for performing positional crystallization of zinc silicate on a ceramic plane and preparing ceramics, the method comprising the steps of:

[0050] (1) Preparation of crystalline glaze: Weigh raw materials respectively according to the following weight percentages: feldspar 22%, quartz 10%, talc 10%, calcite 10%, kaolin 4%, zinc oxide 32%, glass powder 10%, iron Red 2%; Put the weighed raw materials into a ball mill for grinding. When grinding, the ratio of material: ball: water is 1:1.8:0.8, and the fineness of the slurry is 0.1-0.2% after passing through a 300-mesh sieve. , the surface glaze slurry obtained after grinding has a water content of 45% to 50%, and is set aside.

[0051] (2) To make colored glaze, take each raw material respectively by the following weight percentages: transparent feldspar glaze 92%, wrapping red agent 8%; Mix and stir the two kinds of raw materials, cross 100 sieves and prepare semi-finished products; weigh again The flux of 10% ...

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Abstract

The invention discloses a method for performing localized crystallization of zinc silicate on a ceramic plane and preparing ceramic, and belongs to the technical field of preparation of planar crystalline glaze ceramic. The technical points of the method include the following steps: (1) preparing crystalline glaze, (2) preparing colored glaze, (3) preparing seed crystals, (4) making a planar ceramic embryo body or a ceramic embryo body with a plane, drawing patterns on the plane part, and applying a separant in the patterns, (5) coating the colored glaze on the parts, with the coated separant,of the embryo body, and (6) tearing the separant off after drying of the glaze surface, applying the crystalline glaze in the patterns, then performing planting the seed crystals on the crystalline glaze surface, performing retouching and drying sequentially, and finally performing sintering so as to obtain the finished product. The invention aims to provide a method for performing localized crystallization of zinc silicate on the ceramic plane and preparing the ceramic, and the method has an original preparation process, clear patterns, and a good artistic effect, and is suitable for mass production; and the method can be used for preparing planar crystalline glaze ceramic products.

Description

technical field [0001] The invention relates to a method for preparing ceramics, more specifically, a method for performing orientation crystallization of zinc silicate on a ceramic plane and preparing ceramics. Background technique [0002] Crystalline glaze is a kind of precious art glaze with strong decorative properties. Its fundamental feature different from ordinary glaze is that the glaze contains a certain number of visible crystals. The molten crystalline glaze (glass) partially crystallizes during cooling, forming crystals of different compositions, sizes, colors and shapes. Zinc silicate crystalline glaze is an art glaze that uses zinc oxide as a crystallizing agent to form crystals under a certain firing system. Its crystalline mineral is willemite, which has good crystallization performance, stable crystal state, and round crystal flowers. radial features. Zinc silicate crystalline glaze has low viscosity at high temperature, low fluidity, fast crystal growth,...

Claims

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Application Information

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IPC IPC(8): C03C8/00C04B41/89C04B41/86
CPCC03C8/00C04B41/52C04B41/89C04B41/86C04B41/504C04B41/5022
Inventor 黄南兴严权坤蓝天旺邓秋玲黄萌柱
Owner GUANGDONG DABU CERAMIC IND RES INST