High thermal conductivity thermal conduction silica gel gasket and preparation method thereof
A technology of thermally conductive silica gel and high thermal conductivity, which is applied in the field of thermal interface materials. It can solve the problems of limited dispersion and addition amount, low thermal conductivity of gaskets, and inability to form thermal conduction paths, etc., to achieve good operability, increase filling volume, The effect of reducing viscosity
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Embodiment 1
[0036] The components used in the preparation process of the thermally conductive silicone gasket with high thermal conductivity are as follows: (A) 20 parts by weight of methyl vinyl silicone oil with a viscosity of 800mPa·s; (B) 2 parts by weight of hydrogen-containing silicone oil with a hydrogen content of 0.25% ; (C) 80 parts by weight of n-hexane; (D) 450 parts by weight of spherical heat-conducting alumina powder filler, the particle size of large particle size alumina is 130 μm, and the particle size of small particle size alumina is 4 μm, wherein the ratio of large and small particle sizes is 350 parts by weight : 100 parts by weight; 4 parts by weight of (E) KH-570 coupling agent; 2 parts by weight of (F) catalyst; 2 parts by weight of (G) inhibitor. Preparation process: (1) heat the (D) in vacuum to remove excess water; (2) stir the (A)-(D) at a low speed with a planetary mixer at a stirring speed of 800 rpm for 25 minutes. Preliminary mixture; (3) The ultrasonic ca...
Embodiment 2
[0038]The components used in the preparation process of the thermally conductive silicone gasket with high thermal conductivity are as follows: (A) 20 parts by weight of methyl vinyl silicone oil with a viscosity of 200mPa·s; (B) 5 parts by weight of hydrogen-containing silicone oil with a hydrogen content of 0.15% (C) 200 parts by weight of n-hexane; (D) 500 parts by weight of spherical heat-conducting alumina powder filler, the particle size of large-sized alumina is 140 μm, and the particle size of small-sized alumina is 2 μm, wherein the ratio of large and small particle sizes is 380 parts by weight : 120 parts by weight; 3 parts by weight of (E) KH-560 coupling agent; 2 parts by weight of (F) catalyst; 2 parts by weight of (G) inhibitor. Preparation process: (1) heat the (D) in vacuum to remove excess water; (2) stir the (A)-(D) at a low speed with a planetary mixer at a stirring speed of 600 rpm for 25 minutes Preliminary mixture; (3) The ultrasonic cavitation working fr...
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