Heated non-burning cigarette and preparation method thereof
A technology for heating non-combustion and cigarettes, applied in the field of the tobacco industry, can solve the problems of easy moisture absorption, limited addition amount, etc., and achieve the effects of simple steps, uniform particle size, and simple device
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Embodiment 1
[0081] 12 g of polyvinyl alcohol was weighed and dissolved in 400 mL of deionized water at 80° C. to obtain a polyvinyl alcohol solution.
[0082] 3 g of polylactic acid particles were weighed and dissolved in 30 mL of dichloromethane to obtain a polylactic acid solution.
[0083] The polylactic acid solution and propylene glycol were put into syringes, placed on two syringe pumps, and connected to a coaxial double-needle reactor. The flow rates of the two syringe pumps were 5mL / h (the flow of propylene glycol) and 6mL / h (poly The flow rate of lactic acid solution) was dropped into the polyvinyl alcohol solution, mechanically stirred for 6h, the stirring speed was 250r / min, the product was vacuum filtered, washed with deionized water, and then collected to obtain polylactic acid functional capsules. The particle size of the capsules was measured to be 3.3 mm.
Embodiment 2
[0085] 12 g of polyvinyl alcohol was weighed and dissolved in 400 mL of deionized water at 80° C. to obtain a polyvinyl alcohol solution.
[0086] 3.6 g of polylactic acid particles were weighed and dissolved in 30 mL of dichloromethane to obtain a polylactic acid solution.
[0087] The polylactic acid solution and deionized water were put into the syringes, placed on two syringe pumps, and connected to the coaxial double-needle reactor. The flow rates of the two syringe pumps were 5mL / h (water flow) and 6mL / h respectively. h (flow rate of polylactic acid solution), drop into polyvinyl alcohol solution, stir mechanically for 6h, stirring speed is 250r / min, filter the product under reduced pressure, wash with deionized water, and then collect to obtain water-in-polylactic acid capsules . The measured particle size of the water-filled capsule is 3.5 mm (see image 3 -a).
Embodiment 3
[0089] Compared with Example 2, the main difference is that the PLA solubility of the wall material solution is 0.15g / mL; the details are as follows:
[0090] 12 g of polyvinyl alcohol was weighed and dissolved in 400 mL of deionized water at 80° C. to obtain a polyvinyl alcohol solution.
[0091] 4.5 g of polylactic acid particles were weighed and dissolved in 30 mL of dichloromethane to obtain a polylactic acid solution.
[0092] Put the polylactic acid solution and deionized water into the syringe respectively, place them on two syringe pumps, and connect the coaxial double-needle reactor. The flow rates of the two syringe pumps are 5mL / h (flow rate of water) and 6mL / h respectively. (flow rate of polylactic acid solution); drop into polyvinyl alcohol solution, stir mechanically for 6h, stirring speed is 250r / min, filter the product under reduced pressure, wash with deionized water, and then collect to obtain water-in-polylactic acid capsules. The particle size of the water...
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