A kind of 3D printing ceramic nanopowder and preparation method thereof
A 3D printing and nano-powder technology, applied in the field of 3D printing materials, can solve the problems of poor compatibility between inorganic particles and polymer bodies, low mechanical properties and low curing shrinkage, and achieve low curing shrinkage, high mechanical properties and performance. stable effect
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Embodiment 1
[0024] The 3D printing ceramic nanopowder of present embodiment, raw material comprises following components: sodium silicate solution and photothermal initiator, and the mixed solution of trimethylolpropane triacrylate and acrylic acid; The quality of described sodium silicate solution The concentration is 1%; the quality of the photothermal initiator is 0.3% of the quality of the sodium silicate solution, and the mass content of trimethylolpropane triacrylate in the mixed solution of trimethylolpropane triacrylate and acrylic acid 50%.
[0025] The photothermal initiator is a mixture of 1-hydroxycyclohexyl phenyl ketone and 2,4,6-trimethylbenzoyl-diphenylphosphine oxide, 1-hydroxy cyclohexyl phenyl ketone and 2, The mass ratio of 4,6-trimethylbenzoyl-diphenylphosphine oxide is 1:1.
[0026] The preparation method of the 3D printing ceramic nanopowder of this embodiment is:
[0027] Step 1. Add sodium silicate to deionized water, heat and stir to dissolve the sodium silicat...
Embodiment 2
[0033] The 3D printing ceramic nanopowder of present embodiment, raw material comprises following components: sodium silicate solution and photothermal initiator, and the mixed solution of trimethylolpropane triacrylate and acrylic acid; The quality of described sodium silicate solution The concentration is 25%; the quality of the photothermal initiator is 0.5% of the quality of the sodium silicate solution, and the mass content of trimethylolpropane triacrylate in the mixed solution of trimethylolpropane triacrylate and acrylic acid was 33.3%.
[0034] The photothermal initiator is a mixture of 1-hydroxycyclohexyl phenyl ketone and 2,4,6-trimethylbenzoyl-diphenylphosphine oxide, 1-hydroxy cyclohexyl phenyl ketone and 2, The mass ratio of 4,6-trimethylbenzoyl-diphenylphosphine oxide is 1:0.05.
[0035] The preparation method of the 3D printing ceramic nanopowder of this embodiment is:
[0036] Step 1. Add sodium silicate to deionized water, heat and stir to dissolve the sodi...
Embodiment 3
[0042] The 3D printing ceramic nanopowder of present embodiment, raw material comprises following components: sodium silicate solution and photothermal initiator, and the mixed solution of trimethylolpropane triacrylate and acrylic acid; The quality of described sodium silicate solution The concentration is 50%; the quality of the photothermal initiator is 5% of the quality of the sodium silicate solution, and the mass content of trimethylolpropane triacrylate in the mixed solution of trimethylolpropane triacrylate and acrylic acid 25%.
[0043] The photothermal initiator is a mixture of 1-hydroxycyclohexyl phenyl ketone and 2,4,6-trimethylbenzoyl-diphenylphosphine oxide, 1-hydroxy cyclohexyl phenyl ketone and 2, The mass ratio of 4,6-trimethylbenzoyl-diphenylphosphine oxide is 1:3.
[0044] The preparation method of the 3D printing ceramic nanopowder of this embodiment is:
[0045] Step 1. Add sodium silicate to deionized water, heat and stir to dissolve the sodium silicate t...
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