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Preparation of olive oil derivative rich in balanced unsaturated fatty acid and application

A technology of unsaturated fatty acids and olive oil, which is applied in the field of oleochemicals, can solve the problems of short shelf life, meet daily needs, improve bioabsorption efficiency, and improve antioxidant performance

Active Publication Date: 2019-09-17
青岛中科潮生生物技术有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The olive oil derivatives prepared by the invention not only increase the edible value of olive oil, but also improve its antioxidant properties, thereby solving the problem of the shelf life of the compound oil rich in polyunsaturated fatty acids under the premise of not adding exogenous antioxidants too short issue, providing technical support for the marketization of the product, with great economic prospects

Method used

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  • Preparation of olive oil derivative rich in balanced unsaturated fatty acid and application
  • Preparation of olive oil derivative rich in balanced unsaturated fatty acid and application
  • Preparation of olive oil derivative rich in balanced unsaturated fatty acid and application

Examples

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Embodiment 1

[0027] Example 1: Preparation of Olive Oil Derivatives Rich in Balanced Unsaturated Fatty Acids

[0028] 1) Mix four kinds of oils in proportion by weight: 50 parts of olive oil, 25 parts of palm oleic acid oil, 20 parts of ARA oil, and 20 parts of DHA algae oil are mixed evenly to obtain the primary mixed oil.

[0029] 2) Mix the mixed oil, soybean lecithin, and Burkholderia complex enzyme solution in a weight ratio of 3:1:8, and react at 35°C for 4 hours to obtain phospholipids rich in functional fatty acids crude product. Use high-purity nitrogen with a purity of 99.999% as the protective gas.

[0030] 3) dissolve the phospholipid crude product in dehydrated alcohol, filter and remove insolubles after mixing uniformly to obtain extract A, in the extract A, add dropwise a concentration of 70% zinc sulfate aqueous solution at a rate of 60 drops per minute to control the pH is 6.0, and the reaction time is 40 minutes. After the reaction, the aqueous phase was removed to obtai...

Embodiment 2

[0037] Example 2: Preparation of Olive Oil Derivatives Rich in Balanced Unsaturated Fatty Acids

[0038] 1) Mix four kinds of oils in proportion by weight: 70 parts of olive oil, 35 parts of palm oleic acid oil, 30 parts of ARA oil, and 30 parts of DHA algae oil are mixed evenly to obtain the initial mixed oil.

[0039] 2) Mix the mixed oil, soybean lecithin, and Burkholderia complex enzyme solution in a weight ratio of 5:1:10, and react at 45°C for 2 hours to obtain phospholipids rich in functional fatty acids crude product. Use high-purity nitrogen with a purity of 99.999% as the protective gas.

[0040] 3) dissolving the phospholipid crude product in absolute ethanol, and filtering to remove the insolubles after mixing uniformly to obtain extract A, in the extract A, add 50% zinc sulfate aqueous solution dropwise at a rate of 120 drops per minute, and control the pH to be 7.5 , the reaction time is 60 minutes. After the reaction, the aqueous phase was removed to obtain e...

Embodiment 3

[0047] Example 3: Preparation of Olive Oil Derivatives Rich in Balanced Unsaturated Fatty Acids

[0048] 1) Mix four kinds of oils in proportion by weight: 60 parts of olive oil, 30 parts of palm oil, 25 parts of ARA oil, and 25 parts of DHA algae oil are mixed evenly to obtain the primary mixed oil.

[0049] 2) Mix the mixed oil, soybean lecithin, and Burkholderia complex enzyme solution in a weight ratio of 4:1:9, and react at 40°C for 3 hours to obtain phospholipids rich in functional fatty acids crude product. Use high-purity nitrogen with a purity of 99.999% as the protective gas.

[0050] 3) Dissolving the crude phospholipid product in absolute ethanol, mixing evenly and filtering to remove the insoluble matter to obtain extract A, adding 60% zinc sulfate aqueous solution dropwise at a rate of 90 drops per minute to the extract A, controlling the pH to be 7.0 , the reaction time is 50 minutes. After the reaction, the aqueous phase was removed to obtain extract B. Use...

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Abstract

The invention provides a preparation method of an olive oil derivative rich in balanced unsaturated fatty acid. The preparation method comprises the following steps of (1) thoroughly mixing olive oil with palmitoleic acid fat, ARA fat and DHA algae oil so as to obtain primary mixed fat; (2) uniformly mixing the mixed fat with soybean lecithin and Burkholderia complex enzyme liquid, and performing a reaction at 35-45 DEG C for 2-4 hours so as to obtain a phosphatide coarse product; (3) enabling the phosphatide coarse product to dissolve in ethanol, performing mixing, removing insoluble substances to obtain an extraction solution A, adding a zinc sulfate aqueous solution dropwise to the extraction solution A, and after a reaction is completed, removing a water phase so as to obtain a extraction solution B; and (4) performing ultrasonic incubation on the extraction solution B for 20-30 minutes, and performing extraction so as to obtain the olive oil derivative rich in balanced unsaturated fatty acid. According to the olive oil derivative disclosed by the invention, the dietary value of the olive oil is increased, the antioxygenic property of the olive oil is increased, the problem that the storage life of compounded fat rich in polyunsaturated fatty acid is too short under the premise that no exogenous antioxidant is added is solved, and the olive oil derivative has great market application prospects.

Description

technical field [0001] The invention belongs to the field of oleochemical industry and relates to the preparation and application of an olive oil derivative, in particular to the preparation and application of a multipurpose olive oil derivative rich in balanced unsaturated fatty acids. Background technique [0002] Olive oil is directly cold-pressed from fresh olives, without heating and chemical treatment, and retains natural nutrients. Olive oil is rich in monounsaturated fatty acid - oleic acid, as well as vitamin A, vitamin B, vitamin D, vitamin E, vitamin K and antioxidants; it is considered to be the most suitable for human nutrition among the oils found so far of grease. The outstanding feature of olive oil is that it contains a large amount of monounsaturated fatty acids. As we all know, monounsaturated fatty acids can adjust the ratio of high and low-density lipoprotein cholesterol in human plasma, increase the level of high-density lipoprotein HDL (good choleste...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23D9/04A23D9/06A61K8/36A61K8/37A61K8/55A61K8/66A61K8/92A61Q19/00
CPCA23D9/04A23D9/06A61K8/922A61K8/37A61K8/361A61K8/66A61K8/553A61Q19/00A61K2800/522
Inventor 崔球邓煜宋晓金刘婷
Owner 青岛中科潮生生物技术有限公司